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RESEARCH PAPER · Chemistry of Materials · 1999

Time-Resolved in Situ X-ray Powder Diffraction Study of the Formation of Mesoporous Silicates

Stephen P. O'Brien, Robin J. Francis, Andrew M. Fogg, Dermot O’Hare, Nanae Okazaki, Kazuyuki Kuroda

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Time-Resolved in Situ X-ray Powder Diffraction Study of the Formation of Mesoporous SilicatesOriginalNew directions in self-assembly:71Thin films of mesoporous silica: preparation and characterization55Determination of the kinetics of crystallisation of gibbsite using time resolved in situ energy dispersive powder X-ray diffraction32In-situ small angle x-ray scattering (SAXS) studies on the formation of mesostructured aluminophosphate / surfactant composite materials6Time-resolved in-situ X-ray diffraction study of the formation of 3D-hexagonal mesoporous silica films8Orientation of Guest Molecules and Formation of Mesoporous Silica Induced by Layered Silicate-Organic Interactions1Nonaqueous Synthesis of Mesostructured Aluminophosphate/Surfactant Composites: Synthesis, Characterization, and In-Situ SAXS Studies36The in situ phase transitions occurring during bicontinuous cubic phase formation43In Situ Investigations on Cetyltrimethylammonium Surfactant/Silicate Systems, Precursors of Organized Mesoporous MCM-41-Type Siliceous Materials129Lamellar Hexadecyltrimethylammonium Silicates Derived from Kanemite42Control of mesostructured silica particle morphology107In Situ X-ray Diffraction Studies of the Crystallization of Layered Manganese Thioantimonates(III) under Hydrothermal Conditions75An in Situ Study of Mesostructured CTAB−Silica Film Formation during Dip Coating Using Time-Resolved SAXS and Interferometry Measurements207Controlled Solubilization of Toluene by Silicate−Catanionic Surfactant Mesophases as Studied by in Situ and ex Situ XRD43Recent advances in the formation mechanisms of organized mesoporous materials172Leached Natural Saponite as the Silicate Source in the Synthesis of Aluminosilicate Hexagonal Mesoporous Materials29Controlled Synthesis and Processing of Ceramic Oxides — A Molecular Approach1Chemical Strategies To Design Textured Materials: from Microporous and Mesoporous Oxides to Nanonetworks and Hierarchical Structures1958Transformation of Layered Docosyltrimethyl- and Docosyltriethylammonium Silicates Derived from Kanemite into Precursors for Ordered Mesoporous Silicas24In-Situ SAXS Studies on the Formation of Silicate/Surfactant Mesophases with Solubilized Benzene under Acidic Conditions27An in situ study of crystallisation gradients during the hydrothermal/autoclave synthesis of zeolites8In‐situ Energy‐Dispersive X‐ray Diffraction Studies of Crystal Growth and Compound Conversion Under Solvothermal Conditions47Synthesis of Al-containing mesoporous silica (KSW-2) with semi-squared channels by incorporation of Al into the framework of kanemiteElectronic supplementary information (ESI) available: powder XRD patterns and 29Si MAS NMR spectra of kanemite and Al-kanemite, N2 adsorption isotherm of Al-KSW-2, TEM images of Al-KSW-2. See http://www.rsc.org/suppdata/jm/b2/b211073c/20Mesoporous templated silicates: an overview of their synthesis, catalytic activation and evaluation of the stability189Synchrotron X-ray diffraction–diffusion studies of the preparation of SBA-15 materials33Discovery of mesoporous silica from layered silicates13Síntesis de materiales nanoestructurados de sílice a partir de tensoactivos orgánicos iónicos y no iónicos0Silica-Based Mesostructured Materials Induced by Surfactant Assemblies in the Two-Dimensionally Limited Space of a Layered Polysilicate Kanemite16Alkali Silicates and Crystalline Silicic Acids22Alkali Silicates and Crystalline Silicic Acids8Influence of the Kind of Layered Disodium Disilicates on the Formation of Silica−Organic Mesostructured Materials15Envisaging the Physicochemical Processes during the Preparation of Supported Catalysts: Raman Microscopy on the Impregnation of Mo onto Al 2 O 3 Extrudates174Al-rich mesoporous FSM-16 materials: Synthesis, characterization and catalytic properties3In situ NMR and XRD studies of the growth mechanism of SBA-124Surfactant-templated mesostructured materials from inorganic silica85Hydroxy Double Salt Anion Exchange Kinetics: Effects of Precursor Structure and Anion Size51Characterization of the Initial Stages of SBA-15 Synthesis by in Situ Time-Resolved Small-Angle X-ray Scattering94Detailed in Situ XRD and Calorimetric Study of the Formation of Silicate/Mixed Surfactant Mesophases under Alkaline Conditions. Influence of Surfactant Chain Length and Synthesis Temperature21Formation Mechanism for Monodispersed Mesoporous Silica Spheres and Its Application to the Synthesis of Core/Shell Particles104Synthesis, characterization and catalytic properties of mesoporous Al-FSM-16 materials10Catalytic oxidation of cyclohexene over metalloporphyrin supported on mesoporous molecular sieves of FSM-16 type—Steric effects induced by nanospace constraints28ControlledSynthesisandProcessingofCeramicOxides—AMolecularApproach0In Situ Investigation on the Formation Mechanism of MCM-41 Mesoporous Silica by Microcalorimetry9Ordered Mesoporous Silica Derived from Layered Silicates72Synthesis and structural characterization of iron-modified folded sheet mesoporous materials13Observation and Isolation of Layered and Framework Ytterbium Hydroxide Phases Using In Situ Energy-Dispersive X-ray Diffraction56Catalytic performance of iron-mesoporous nanomaterials synthesized by a microwave-hydrothermal process4Formation Mechanism Studies of Phenylene-Bridged Periodic Mesoporous Organosilicas (PMOs)3In situ SAXD Studies on Phenylene- and Thiophene-Bridged Periodic Mesoporous Organosilicas (PMOs)4Structural characterization of Fe-FSM-16 prepared using a microwave–hydrothermal process3High activities of iron-FSM-16 materials synthesized by a microwave-hydrothermal process in friedel-crafts alkylations4In-Situ Raman Spectroscopy Studies of Room-Temperature and Hydrothermal Reactions1Properties and reactivity of zinc-folded sheet mesoporous materials3Properties and reactivity of Zr-incorporated folded sheet mesoporous material for alkylation of anisole using tert-butylalcohol3Synthesis Approach of Mesoporous Molecular Sieves5The vapor phase tert-Butylation of anisole with tert-butanol reaction over nickel mesoporous catalysts1Remarkable catalytic performance of H–Fe–FSM-16, synthesized by use of a microwave hydrothermal process, in the acetylation of 1,2-dimethoxybenzene0Changes in the mesostructure and properties of MCM-41 depending on the formation medium3Size Limit on the Formation of Periodic Mesoporous Organosilicas (PMOs)7Monitoring MCM-41 synthesis by X-ray mesostructure analysis15Thermoanalytical Characterization and Catalytic Conversion of Deoiled Micro Algae and Jatropha Seed Cake4Mechanistic Aspects in the Formation, Growth and Surface Functionalization of Metal Oxide Nanoparticles in Organic Solvents125Synthèse de nano-adsorbant à base d’argile, application à l’adsorption de métaux lourds et de chlorophénols0Single-micelle-directed synthesis of mesoporous materials315Panoramic (in beam) studies of materials synthesis1Fabrication of Mesoporous Silica Nanoparticles and Its Applications in Drug Delivery14

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  1. New directions in self-assembly:

    Current Opinion in Colloid & Interface Science · 1999-10-01

    Ivana Soten, Geoffrey Alan Ozin

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  2. Thin films of mesoporous silica: preparation and characterization

    Current Opinion in Colloid & Interface Science · 1999-12-01

    Svetlana Pevzner, Oren Regev, Rachel Yerushalmi‐Rozen

    Read original paper ↗ ·

  3. Determination of the kinetics of crystallisation of gibbsite using time resolved in situ energy dispersive powder X-ray diffraction

    Journal of Materials Chemistry · 2000-01-01

    Andrew M. Fogg, Stephen J. Price, Robin J. Francis, Stephen P. O'Brien, Dermot M. O'Hare

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  4. In-situ small angle x-ray scattering (SAXS) studies on the formation of mesostructured aluminophosphate / surfactant composite materials

    Studies in surface science and catalysis · 2000-01-01

    Michael Tiemann, Michael Fröba, Gert Rapp, Sérgio S. Funari

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  5. Time-resolved in-situ X-ray diffraction study of the formation of 3D-hexagonal mesoporous silica films

    MRS Proceedings · 2000-01-01

    David Grosso, Pierre‐Antoine Albouy, Heinz Wilfried Amenitsch, Ruud Balkenende, Florence Babonneau

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  6. Orientation of Guest Molecules and Formation of Mesoporous Silica Induced by Layered Silicate-Organic Interactions

    Molecular crystals and liquid crystals science technology. Section A, Molecular crystals and liquid crystals/Molecular crystals and liquid crystals science and technology. Section A, Molecular crystals and liquid crystals · 2000-04-01

    Kazuyuki Kuroda

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  7. Nonaqueous Synthesis of Mesostructured Aluminophosphate/Surfactant Composites: Synthesis, Characterization, and In-Situ SAXS Studies

    Chemistry of Materials · 2000-04-26

    Michael Tiemann, Michael Fröba, Gert Rapp, Sérgio S. Funari

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  8. The in situ phase transitions occurring during bicontinuous cubic phase formation

    Microporous and Mesoporous Materials · 2000-08-01

    Svetlana Pevzner, Oren Regev

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  9. In Situ Investigations on Cetyltrimethylammonium Surfactant/Silicate Systems, Precursors of Organized Mesoporous MCM-41-Type Siliceous Materials

    Langmuir · 2000-08-03

    Jörn Frasch, Bénédicte Lebeau, Michel Soulard, Joël Patarin, R. Zana

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  10. Lamellar Hexadecyltrimethylammonium Silicates Derived from Kanemite

    Langmuir · 2000-09-02

    Tatsuo Kimura, Daigo Itoh, Nanae Okazaki, Mizue Kaneda, Yasuhiro Sakamoto, Osamu Terasaki, Yoshiyuki Sugahara, Kazuyuki Kuroda

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  11. Control of mesostructured silica particle morphology

    Journal of Materials Chemistry · 2001-01-01

    Henry B. S. Chan, Peter M. Budd, Timothy deV. Naylor

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  12. In Situ X-ray Diffraction Studies of the Crystallization of Layered Manganese Thioantimonates(III) under Hydrothermal Conditions

    Chemistry of Materials · 2001-03-20

    Lars Engelke, M. Schaefer, Melissa J. Schur, Wolfgang Bensch

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  13. An in Situ Study of Mesostructured CTAB−Silica Film Formation during Dip Coating Using Time-Resolved SAXS and Interferometry Measurements

    Chemistry of Materials · 2002-01-11

    David Grosso, Florence Babonneau, Pierre‐Antoine Albouy, Heinz Wilfried Amenitsch, Ruud Balkenende, Aline Brunet-Bruneau, Josette Rivory

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  14. Controlled Solubilization of Toluene by Silicate−Catanionic Surfactant Mesophases as Studied by in Situ and ex Situ XRD

    Langmuir · 2002-01-18

    Anna M. Lind, Jenny Andersson, Stefan Karlsson, Patrik Ågren, Patrick Bussian, Heinz Wilfried Amenitsch, Mika Lindén

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  15. Recent advances in the formation mechanisms of organized mesoporous materials

    Current Opinion in Colloid & Interface Science · 2002-03-01

    Joël Patarin, Bénédicte Lebeau, R. Zana

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  16. Leached Natural Saponite as the Silicate Source in the Synthesis of Aluminosilicate Hexagonal Mesoporous Materials

    The Journal of Physical Chemistry B · 2002-03-30

    Thierry Linssen, Pegie Cool, Mohammed Baroudi, Kristof Cassiers, Etienne F. Vansant, Oleg I. Lebedev, Joseph Van Landuyt

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  17. Controlled Synthesis and Processing of Ceramic Oxides — A Molecular Approach

    CRC Press eBooks · 2002-08-27

    Mika Lindén, Jarl B. Rosenholm

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  18. Chemical Strategies To Design Textured Materials: from Microporous and Mesoporous Oxides to Nanonetworks and Hierarchical Structures

    Chemical Reviews · 2002-10-25

    Galo J. A. A. Soler‐Illia, Clément Sánchez, Bénédicte Lebeau, Joël Patarin

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  19. Transformation of Layered Docosyltrimethyl- and Docosyltriethylammonium Silicates Derived from Kanemite into Precursors for Ordered Mesoporous Silicas

    Langmuir · 2002-10-30

    Tatsuo Kimura, Daigo Itoh, Tetsuro Shigeno, Kazuyuki Kuroda

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  20. In-Situ SAXS Studies on the Formation of Silicate/Surfactant Mesophases with Solubilized Benzene under Acidic Conditions

    Langmuir · 2002-12-01

    Michael Tiemann, Valérie Goletto, R. Blum, Florence Babonneau, Heinz Wilfried Amenitsch, Mika Lindén

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  21. An in situ study of crystallisation gradients during the hydrothermal/autoclave synthesis of zeolites

    Physical Chemistry Chemical Physics · 2003-01-01

    David Hooper, Paul Barnes, Jeremy K. Cockcroft, Andrew C. Jupe, Simon D. M. Jacques, Stephen P. Bailey, Fabio Lupo, Martin J. Vickers, Michael Hanfland

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  22. In‐situ Energy‐Dispersive X‐ray Diffraction Studies of Crystal Growth and Compound Conversion Under Solvothermal Conditions

    European Journal of Inorganic Chemistry · 2003-01-20

    Lars Engelke, Michael Schaefer, Felix Porsch, Wolfgang Bensch

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  23. Synthesis of Al-containing mesoporous silica (KSW-2) with semi-squared channels by incorporation of Al into the framework of kanemiteElectronic supplementary information (ESI) available: powder XRD patterns and 29Si MAS NMR spectra of kanemite and Al-kanemite, N2 adsorption isotherm of Al-KSW-2, TEM images of Al-KSW-2. See http://www.rsc.org/suppdata/jm/b2/b211073c/

    Journal of Materials Chemistry · 2003-02-19

    Tetsuro Shigeno, Koji Inoue, Tatsuo Kimura, Naonobu Katada, Miki Niwa, Kazuyuki Kuroda

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  24. Mesoporous templated silicates: an overview of their synthesis, catalytic activation and evaluation of the stability

    Advances in Colloid and Interface Science · 2003-04-01

    Thierry Linssen, Kristof Cassiers, Pegie Cool, Etienne F. Vansant

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  25. Synchrotron X-ray diffraction–diffusion studies of the preparation of SBA-15 materials

    Microporous and Mesoporous Materials · 2003-11-05

    Vladimir Zholobenko, Andreï Y. Khodakov, DURAND Dominique Christiane

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  26. Discovery of mesoporous silica from layered silicates

    Studies in surface science and catalysis · 2004-01-01

    Kazuyuki Kuroda

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  27. Síntesis de materiales nanoestructurados de sílice a partir de tensoactivos orgánicos iónicos y no iónicos

    Unknown journal · 2004-01-01

    José Franco Pérez Arévalo

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  28. Silica-Based Mesostructured Materials Induced by Surfactant Assemblies in the Two-Dimensionally Limited Space of a Layered Polysilicate Kanemite

    Bulletin of the Chemical Society of Japan · 2004-03-01

    Tatsuo Kimura, Daigo Itoh, Tetsuro Shigeno, Kazuyuki Kuroda

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  29. Alkali Silicates and Crystalline Silicic Acids

    CRC Press eBooks · 2004-03-23

    Scott M. Auerbach, Kathleen A. Carrado, Prabir K. Dutta

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  30. Alkali Silicates and Crystalline Silicic Acids

    CRC Press eBooks · 2004-03-23

    Wilhelm Schwieger, G. Lagaly

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  31. Influence of the Kind of Layered Disodium Disilicates on the Formation of Silica−Organic Mesostructured Materials

    Chemistry of Materials · 2004-07-23

    Munetaka Kato, Tetsuro Shigeno, Tatsuo Kimura, Kazuyuki Kuroda

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  32. Envisaging the Physicochemical Processes during the Preparation of Supported Catalysts: Raman Microscopy on the Impregnation of Mo onto Al 2 O 3 Extrudates

    Journal of the American Chemical Society · 2004-10-19

    Jaap A. Bergwerff, Tom Visser, G. Leliveld, Brenda D. Rossenaar, Krijn P. de Jong, Bert Marc Weckhuysen

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  33. Al-rich mesoporous FSM-16 materials: Synthesis, characterization and catalytic properties

    Studies in surface science and catalysis · 2005-01-01

    T. Selvam, V. R. Reddy Marthala, Ralph Herrmann, Wilhelm Schwieger, Norbert Pfänder, Robert Schlögl, Horst Ernst, Dieter Freude

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  34. In situ NMR and XRD studies of the growth mechanism of SBA-1

    Physical Chemistry Chemical Physics · 2005-01-01

    C. C. EggerCurrent address Institut de S, Michael W. Anderson, GORDON J. T. TIDDY, John L. Casci

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  35. Surfactant-templated mesostructured materials from inorganic silica

    Soft Matter · 2005-01-01

    Andreas Berggren, Anders E. C. Palmqvist, Krister Holmberg

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  36. Hydroxy Double Salt Anion Exchange Kinetics: Effects of Precursor Structure and Anion Size

    The Journal of Physical Chemistry B · 2005-02-12

    Everson Kandare, Jeanne M. Hossenlopp

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  37. Characterization of the Initial Stages of SBA-15 Synthesis by in Situ Time-Resolved Small-Angle X-ray Scattering

    The Journal of Physical Chemistry B · 2005-11-12

    Andreï Y. Khodakov, Vladimir Zholobenko, Marianne Impéror‐Clerc, DURAND Dominique Christiane

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  38. Detailed in Situ XRD and Calorimetric Study of the Formation of Silicate/Mixed Surfactant Mesophases under Alkaline Conditions. Influence of Surfactant Chain Length and Synthesis Temperature

    The Journal of Physical Chemistry B · 2006-07-22

    Isabelle Beurroies, Patrik Ågren, Gunter Büchel, Jarl B. Rosenholm, Heinz Wilfried Amenitsch, Renaud Denoyel, Mika Lindén

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  39. Formation Mechanism for Monodispersed Mesoporous Silica Spheres and Its Application to the Synthesis of Core/Shell Particles

    The Journal of Physical Chemistry C · 2006-12-22

    Tadashi Nakamura, Mamoru Mizutani, Hiroshi Nozaki, Noritomo Suzuki, Kazuhisa Yano

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  40. Synthesis, characterization and catalytic properties of mesoporous Al-FSM-16 materials

    Journal of Porous Materials · 2007-01-25

    T. Selvam, Martin Köstner, Godwin T. P. Mabande, Wilhelm Schwieger, Norbert Pfänder, Robert Schlögl

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  41. Catalytic oxidation of cyclohexene over metalloporphyrin supported on mesoporous molecular sieves of FSM-16 type—Steric effects induced by nanospace constraints

    Catalysis Today · 2007-05-08

    Małgorzata Zimowska, Alicja Michalik-Zym, Jan Połtowicz, Mirosława Bazarnik, Krzysztof Bahranowski, Ewa M. Serwicka

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  42. ControlledSynthesisandProcessingofCeramicOxides—AMolecularApproach

    CRC Press eBooks · 2008-11-20

    Mika Lindén, Jarl B. Rosenholm

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  43. In Situ Investigation on the Formation Mechanism of MCM-41 Mesoporous Silica by Microcalorimetry

    Journal of Chemical & Engineering Data · 2008-12-01

    Zhaodong Nan, Meiyun Wang, Bianqing Yan

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  44. Ordered Mesoporous Silica Derived from Layered Silicates

    Advanced Functional Materials · 2009-01-22

    Tatsuo Kimura, Kazuyuki Kuroda

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  45. Synthesis and structural characterization of iron-modified folded sheet mesoporous materials

    Journal of Porous Materials · 2009-09-15

    Khaldoun Bacharı, A. Touileb, Adel Saadi, Djamila Halliche, O. Cherifi

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  46. Observation and Isolation of Layered and Framework Ytterbium Hydroxide Phases Using In Situ Energy-Dispersive X-ray Diffraction

    Chemistry of Materials · 2010-03-04

    Laura J. McIntyre, Timothy J. Prior, Andrew M. Fogg

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  47. Catalytic performance of iron-mesoporous nanomaterials synthesized by a microwave-hydrothermal process

    Reaction Kinetics Mechanisms and Catalysis · 2010-03-30

    Khaldoun Bacharı, R. M. Guerroudj, M. Lamouchi

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  48. Formation Mechanism Studies of Phenylene-Bridged Periodic Mesoporous Organosilicas (PMOs)

    Langmuir · 2010-04-16

    Vivian Rebbin, André Rothkirch, Nobuhiro Ohta, Sérgio S. Funari

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  49. In situ SAXD Studies on Phenylene- and Thiophene-Bridged Periodic Mesoporous Organosilicas (PMOs)

    Chemistry of Materials · 2010-05-24

    Vivian Rebbin, André Rothkirch, Michael Fröba, Sérgio S. Funari

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  50. Structural characterization of Fe-FSM-16 prepared using a microwave–hydrothermal process

    Materials Chemistry and Physics · 2010-09-16

    Khaldoun Bacharı, R. M. Guerroudj, M. Lamouchi

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