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RESEARCH PAPER · CrystEngComm · 2012

Formation and characterisation of Mn-MIL-100

Helge Reinsch, Norbert Stock

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Formation and characterisation of Mn-MIL-100OriginalCrystallisation of solvothermally synthesised ZIF-8 investigated at the bulk, single crystal and surface level60Aluminum-1,4-cyclohexanedicarboxylates: High-Throughput and Temperature-Dependent in Situ EDXRD Studies72High valence 3p and transition metal based MOFs605Insight into the mechanism of modulated syntheses: in situ synchrotron diffraction studies on the formation of Zr-fumarate MOF158In Situ Energy-Dispersive X-ray Diffraction for the Synthesis Optimization and Scale-up of the Porous Zirconium Terephthalate UiO-66219In Situ Studies of Solvothermal Synthesis of Energy Materials159Facile synthesis and characterization of trimesic acid-Cu based metal organic frameworks63Indium Imidazolate Frameworks with Differently Distorted ReO3-Type Structures: Syntheses, Structures, Phase Transitions, and Crystallization Studies13Group 13 Metal Carboxylates: Using Molecular Clusters As Hybrid Building Units in a MIL-53 Type Framework15Acid-functionalized UiO-66(Zr) MOFs and their evolution after intra-framework cross-linking: structural features and sorption properties231Benign Preparation of Metal–Organic Frameworks of Trimesic Acid and Cu, Co or Ni for Potential Sensor Applications70Impact of the Nature of the Organic Spacer on the Crystallization Kinetics of UiO‐66(Zr)‐Type MOFs49Synthesis, Crystal Structure and Properties of Three Metal Complexes Based on a Flexible Schiff Base Ligand8Protection of open-metal V(III) sites and their associated CO2/CH4/N2/O2/H2O adsorption properties in mesoporous V-MOFs40Reversible Lithium Storage in Manganese 1,3,5-Benzenetricarboxylate Metal–Organic Framework with High Capacity and Rate Performance343An in situ study of resin-assisted solvothermal metal-organic framework synthesis8Atomistic Modeling of Water Thermodynamics and Kinetics within MIL-100(Fe)23Improved synthesis of trigone trimer cluster metal organic framework MIL-100Al by a later entry of methyl groups19Electrochemical energy storage in Mn 2 O 3 porous nanobars derived from morphology-conserved transformation of benzenetricarboxylate-bridged metal–organic framework94A thermally activated manganese 1,4-benzenedicarboxylate metal organic framework with high anodic capability for Li-ion batteries155Ambient pressure synthesis of MIL-100(Fe) MOF from homogeneous solution using a redox pathway68Nanostructured Co( ii )-based MOFs as promising anodes for advanced lithium storage85Novel transition bimetal–organic frameworks: recyclable catalyst for the oxidative coupling of primary amines to imines at mild conditions29In Situ Observation of Successive Crystallizations and Metastable Intermediates in the Formation of Metal–Organic Frameworks60In Situ Observation of Successive Crystallizations and Metastable Intermediates in the Formation of Metal–Organic Frameworks16Metal-organic framework engineering: directed assembly from molecules to spherical agglomerates12Templated formation of porous Mn 2 O 3 octahedra from Mn-MIL-100 for lithium-ion battery anode materials62High Anodic Performance of Co 1,3,5-Benzenetricarboxylate Coordination Polymers for Li-Ion Battery210In SituStudies of the Crystallization of Metal-Organic Frameworks10Synthesis of Bimetallic MOFs MIL-100(Fe-Mn) as an Efficient Catalyst for Selective Catalytic Reduction of NO x with NH395Chemistry of Metal-organic Frameworks Monitored by Advanced X-ray Diffraction and Scattering Techniques21Nucleation and Crystal Growth of a {V14Sb8O42} Cluster from a {V15Sb6O42} Polyoxovanadate: In Situ XRD Studies28Synthesis and Characterization of [M2(OH)2(C4O4)2(H2O)4]·2H2O (M = Al or Ga)5Electrodeposited films to MOF-derived electrochemical energy storage electrodes: a concept of simplified additive-free electrode processing for self-standing, ready-to-use materials39Structural variety in ytterbium dicarboxylate frameworks and in situ study diffraction of their solvothermal crystallisation14Synthesis of MOFs: a personal view on rationalisation, application and exploration37Synthesis and electrochemical properties of Fe3O4@MOF core-shell microspheres as an anode for lithium ion battery application95Synthesis of highly efficient Mn 2 O 3 catalysts for CO oxidation derived from Mn-MIL-100206Revealing the Initial Reaction Behavior in the Continuous Synthesis of Metal–Organic Frameworks Using Real-Time Synchrotron X-ray Analysis14Co-Ligand Dependent Formation and Phase Transformation of Four Porphyrin-Based Cerium Metal–Organic Frameworks38Mn-MIL-100 heterogeneous catalyst for the selective oxidative cleavage of alkenes to aldehydes47In situ monitoring metal-ligand exchange processes by optical spectroscopy and X-ray diffraction analysis: a review22A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions33Raman Observation of the “Volcano Curve” in the Formation of Carbonized Metal–Organic Frameworks15Formation of a new type of uranium( iv ) poly-oxo cluster {U 38 } based on a controlled release of water via esterification reaction44Metal organic frameworks as a catalyst for oxygen reduction: an unexpected outcome of a highly active Mn-MOF-based catalyst incorporated in activated carbon56MIL-100Cr with open Cr sites for a record N 2 O capture53Bi-metal organic framework derived nickel manganese oxide spinel for lithium-ion battery anode68In Situ, Time-Resolved, and Mechanistic Studies of Metal–Organic Framework Nucleation and Growth610Facile Synthesis of Highly Efficient Amorphous Mn‐MIL‐100 Catalysts: Formation Mechanism and Structure Changes during Application in CO Oxidation122Catalytic performance of Co 1,3,5-benzenetricarboxylate in the conversion of CO2 to cyclic carbonates14Monitoring the Hydrothermal Growth of Cobalt Spinel Water Oxidation Catalysts: From Preparative History to Catalytic Activity20Restricted self-diffusion of adsorbed water in MIL-100(Al)7Structure, characterization, and catalytic properties of open-metal sites in metal organic frameworks142Variability and Periodicity of Properties of Metal-Organic Frameworks: D.I. Mendeleev’s Periodic System in Action0XX Mendeleev Congress on General and Applied Chemistry0Interfacing Manganese Oxide and Cobalt in Porous Graphitic Carbon Polyhedrons Boosts Oxygen Electrocatalysis for Zn–Air Batteries526Remarkable promotion effect of lauric acid on Mn-MIL-100 for non-thermal plasma-catalytic decomposition of toluene54Analysis by synchrotron X-ray scattering of the kinetics of formation of an Fe-based metal-organic framework with high CO2 adsorption5Elucidating the Interaction of CO2 in the Giant Metal–Organic Framework MIL-100 through Large-Scale Periodic Ab Initio Modeling24Highly efficient Mn2O3 catalysts derived from Mn-MOFs for toluene oxidation: The influence of MOFs precursors179Structure of Metal Organic Frameworks and the Periodicity of Their Properties2MOF-derived manganese oxide/carbon nanocomposites with raised capacitance for stable asymmetric supercapacitor60Spectroscopy, microscopy, diffraction and scattering of archetypal MOFs: formation, metal sites in catalysis and thin films116Síntese de polímeros e redes de coordenação do tipo MOF utilizando ácido trimésico, Diimidas Naftálicas e metais de transição >i /i<0Enabling Access to Reduced Open-Metal Sites in Metal-Organic Framework Materials through Choice of Anion Identity: The Case of MIL-100(Cr)23CuO/MnOx composites obtained from Mn-MIL-100 precursors as efficient catalysts for the catalytic combustion of chlorobenzene30Pd/APN-Mn(BTC) as novel, highly efficient, and recyclable catalyst for Suzuki–Miyaura cross coupling reaction8Highly Porous MIL-100(Fe) for the Hydrogen Evolution Reaction (HER) in Acidic and Basic Media141Design strategies for MOF-derived porous functional materials: Preserving surfaces and nurturing pores172In situ X-ray Diffraction Investigation of the Crystallisation of Perfluorinated Ce(IV)-based Metal-Organic Frameworks with UiO-66 and MIL-140 architectures2Co( ii )-based metal–organic framework induces apoptosis through activating the HIF-1α/BNIP3 signaling pathway in microglial cells14Revisiting the MIL-101 metal–organic framework: design, synthesis, modifications, advances, and recent applications326Enhanced performance of carbon-coated manganese catalysts derived from metal-organic framework for rechargeable zinc-air batteries40In Situ X‐ray Diffraction Investigation of the Crystallisation of Perfluorinated Ce IV ‐Based Metal–Organic Frameworks with UiO‐66 and MIL‐140 Architectures**23Selective Styrene Oxidation to Benzaldehyde over Recently Developed Heterogeneous Catalysts69In situ scattering studies of material formation during wet-chemical syntheses1Defects controlled by acid-modulators and water molecules enabled UiO-67 for exceptional toluene uptakes: An experimental and theoretical study151Impact of hydrofluoric acid treatment on the composition, electrical conductivity, and structure of carbonized metal–organic frameworks1Rational Design and General Synthesis of Multimetallic Metal–Organic Framework Nano‐Octahedra for Enhanced Li–S Battery486Solvothermal Crystallization Kinetics and Control of Crystal Size Distribution of MOF-808 in a Continuous Flow Reactor32Carbon black supported on a Mn-MIL-100 framework as high-efficiency electrocatalysts for nitrophenol reduction18Facile Synthesis and Characterization of the Mn-MOF Electrode Material for Flexible Supercapacitors9Different Degradation Mechanisms of Low-Concentration Ozone for Mil-100(Fe) and Mil-100(Mn) Over Wide Humidity Fluctuation28Synthesis and characterisation of novel phosphonate-based linkers and metal-organic frameworks based on tetravalent metals0The missing MIL-101(Mn): geometrically guided synthesis and topologically correlated valence states13Two-step pyrolysis of Mn MIL-100 MOF into MnO nanoclusters/carbon and the effect of N-doping17In Situ Construction of MIL-100@NiMn-LDH Hierarchical Architectures for Highly Selective Photoreduction of CO2 to CH455Tuning CO2 Binding in Metal–Organic Framework Materials by Varying Metal Identity and Oxidation State5Towards(MOFs) Integration for the Preservation of Cultural Heritage0Synthesis, Structure, and Thermal Stability of a Mesoporous Titanium(III) Amine-Containing MOF23Hematite nanoparticle decorated MIL-100 for the highly selective and sensitive electrochemical detection of trace-level paraquat in milk and honey93MOF-Derived MnO/C Nanocomposites for High-Performance Supercapacitors25Mn-MOFs-derived Mn2O3 as an effective peroxymonosulfate activator for the degradation of organics in water14Catalytic Activation of Hydrogen Peroxide Using Highly Porous Hydrothermally Modified Manganese Catalysts for Removal of Azithromycin Antibiotic from Aqueous Solution4Kinetic and X-ray Absorption Spectroscopic Analysis of Catalytic Redox Cycles over Highly Uniform Polymetal Oxo Clusters6Freestanding MOF-Derived Honeycomb-Shape Porous MnOC@CC as an Electrocatalyst for Reversible LiOH Chemistry in Li-O2 Batteries16A Symmetry Concept for the Self-Assembly Synthesis of Mn-MIL-100 Using a Capping Agent and Its Adsorption Performance with Methylene Blue1MOF/bacterial cellulose derived octahedral MnO/carbon nanofiber network: A hybrid for peroxymonosulfate activation toward degradation of tetracycline16Solvent-controlled synthesis of Ni-PTA MOFs as high performance anode material for Li-ion batteries4Transformation of ZIF-67 Nanocubes to ZIF-L Nanoframes73Manganese-oxide-supported gold catalyst derived from metal–organic frameworks for trace PCl 3 oxidation in an organic system3Transient intermediate in the formation of an amorphous metal–organic framework13Deciphering Metal–Organic Framework Synthesis from Hydroxy Double Salts: In-Situ Insights via Synchrotron X-ray Diffraction and Absorption Spectroscopy10In-situ fabrication of MOF-derived MnO-C modified graphite felt for electro-activation of peroxymonosulfate toward degradation of tetracycline: Performance, mechanism and degradation pathway35Wide temperature adaptive oxidase-like based on mesoporous manganese based metal-organic framework for detecting total antioxidant capacity31Mixed N,O‐donor Directed Blue Emissive Nano‐dispersed Mesoporous Mn(II)‐MOF: Dual Sensing Probe for Recyclable and Ultrasensitive ppb‐Level Recognition of TNP and Cr(VI)‐Oxoanions19Mn-MIL-100 derived MnO2@carbon for the photo-induced thermal catalytic HCHO oxidation14Photothermal Catalytic Recycling of Polyester Over Magnetic Ni−MnO x Nanocatalyst16Enhancement of cycling capacity and stability of Co3O4/Ca4O4 as a cathode material in aqueous calcium-ion electrolytes via the integration of reduced graphene oxide (rGO)3Electrochemical and ion-kinetics performances of BMOF-derived Co3O4/CaO cathodes for calcium-ion batteries2Impact of transition metals (M=Mn, Fe, Co, Ni, Cu, Zn) on the formation of local and crystal structure of MBTC phases3Facile preparation of MnO catalysts derived from MOFs for efficient toluene Oxidation: Synergistic enhancement of active site density and reactivity14Advancements in Understanding the Physicochemical Properties of Reticular Materials: An In Situ and Operando Spectroscopic Perspective25Toward Reversible Crystalline-to-Amorphous Guest-Induced Transitions in Manganese(III) Carboxylate Metal–Organic Frameworks1Multifunctional Liposomes with Enhanced Stability for Imaging-Guided Cancer Chemodynamic and Photothermal Therapy2Enhanced Electrocatalytic Degradation of Phenol by Mn-MIL-100-Derived Carbon Materials0Two-step pyrolytic engineering of carbon-doped Mn3O4 with rich defects for efficient photothermal acetone oxidation4Synthesis of a MnMO@C-type MOF derivative (M = Co, Cu, Ni) and its application for hydrogen production in photocatalytic water decomposition0Ozone-coupled photocatalytic H2O2 synthesis via Mn/Ce bimetallic metal organic framework: synergistic catalysis and sacrificial agent-free efficiency2Bayesian Exploration of Metal‐Organic Framework‐Derived Nanocomposites for High‐Performance Supercapacitors1Study on the conformational transformation and biocompatibility of mixed valence MOFs as micro arc oxidation treated binder jetting printed titanium alloy implant coatings3F‐Mediated Precise Control Over Amorphous/Crystalline Fe/Ni‐Based Phosphides Heterostructure for Efficient Oxygen Evolution Reaction1Synthesis and Characterization of a Cerium(IV) Coordination Polymer Containing Isonicotinic Acid Zwitterions0Microwave-assisted synthesis of MIL-100(Al and Fe) for fluoride remediation: A dual experimental–computational approach1A CN/MnO modified graphite felt anode for electrochemical activation of peroxymonosulfate: performance and mechanistic insights into metronidazole degradation0Electroporation-based death of bacteria on assembled piezoelectric nanoenzyme-tips for implant disinfection5Synthesis of MILs metal–organic frameworks and applications for adsorption of H2O and CO21MOF–polymer mixed matrix membranes for advanced gas separation: Progress, challenges, and future perspectives0

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  1. Crystallisation of solvothermally synthesised ZIF-8 investigated at the bulk, single crystal and surface level

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  2. Aluminum-1,4-cyclohexanedicarboxylates: High-Throughput and Temperature-Dependent in Situ EDXRD Studies

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  3. High valence 3p and transition metal based MOFs

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  4. Insight into the mechanism of modulated syntheses: in situ synchrotron diffraction studies on the formation of Zr-fumarate MOF

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  5. In Situ Energy-Dispersive X-ray Diffraction for the Synthesis Optimization and Scale-up of the Porous Zirconium Terephthalate UiO-66

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  6. In Situ Studies of Solvothermal Synthesis of Energy Materials

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  7. Facile synthesis and characterization of trimesic acid-Cu based metal organic frameworks

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  8. Indium Imidazolate Frameworks with Differently Distorted ReO3-Type Structures: Syntheses, Structures, Phase Transitions, and Crystallization Studies

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  9. Group 13 Metal Carboxylates: Using Molecular Clusters As Hybrid Building Units in a MIL-53 Type Framework

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  10. Acid-functionalized UiO-66(Zr) MOFs and their evolution after intra-framework cross-linking: structural features and sorption properties

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  11. Benign Preparation of Metal–Organic Frameworks of Trimesic Acid and Cu, Co or Ni for Potential Sensor Applications

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  12. Impact of the Nature of the Organic Spacer on the Crystallization Kinetics of UiO‐66(Zr)‐Type MOFs

    Chemistry - A European Journal · 2015-03-18

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  13. Synthesis, Crystal Structure and Properties of Three Metal Complexes Based on a Flexible Schiff Base Ligand

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  14. Protection of open-metal V(III) sites and their associated CO2/CH4/N2/O2/H2O adsorption properties in mesoporous V-MOFs

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  15. Reversible Lithium Storage in Manganese 1,3,5-Benzenetricarboxylate Metal–Organic Framework with High Capacity and Rate Performance

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  16. An in situ study of resin-assisted solvothermal metal-organic framework synthesis

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  17. Atomistic Modeling of Water Thermodynamics and Kinetics within MIL-100(Fe)

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  18. Improved synthesis of trigone trimer cluster metal organic framework MIL-100Al by a later entry of methyl groups

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  19. Electrochemical energy storage in Mn 2 O 3 porous nanobars derived from morphology-conserved transformation of benzenetricarboxylate-bridged metal–organic framework

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  20. A thermally activated manganese 1,4-benzenedicarboxylate metal organic framework with high anodic capability for Li-ion batteries

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  21. Ambient pressure synthesis of MIL-100(Fe) MOF from homogeneous solution using a redox pathway

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  22. Nanostructured Co( ii )-based MOFs as promising anodes for advanced lithium storage

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  23. Novel transition bimetal–organic frameworks: recyclable catalyst for the oxidative coupling of primary amines to imines at mild conditions

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  24. In Situ Observation of Successive Crystallizations and Metastable Intermediates in the Formation of Metal–Organic Frameworks

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  25. In Situ Observation of Successive Crystallizations and Metastable Intermediates in the Formation of Metal–Organic Frameworks

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  26. Metal-organic framework engineering: directed assembly from molecules to spherical agglomerates

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  27. Templated formation of porous Mn 2 O 3 octahedra from Mn-MIL-100 for lithium-ion battery anode materials

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  28. High Anodic Performance of Co 1,3,5-Benzenetricarboxylate Coordination Polymers for Li-Ion Battery

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  29. In SituStudies of the Crystallization of Metal-Organic Frameworks

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  30. Synthesis of Bimetallic MOFs MIL-100(Fe-Mn) as an Efficient Catalyst for Selective Catalytic Reduction of NO x with NH3

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  31. Chemistry of Metal-organic Frameworks Monitored by Advanced X-ray Diffraction and Scattering Techniques

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  32. Nucleation and Crystal Growth of a {V14Sb8O42} Cluster from a {V15Sb6O42} Polyoxovanadate: In Situ XRD Studies

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  33. Synthesis and Characterization of [M2(OH)2(C4O4)2(H2O)4]·2H2O (M = Al or Ga)

    Zeitschrift für anorganische und allgemeine Chemie · 2016-11-29

    Selda Halis, Helge Reinsch, Norbert Stock

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  34. Electrodeposited films to MOF-derived electrochemical energy storage electrodes: a concept of simplified additive-free electrode processing for self-standing, ready-to-use materials

    Journal of Materials Chemistry A · 2017-01-01

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  35. Structural variety in ytterbium dicarboxylate frameworks and in situ study diffraction of their solvothermal crystallisation

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    Matthew I. Breeze, Thomas W. Chamberlain, Guy J. Clarkson, Raíssa Pires De Camargo, Yue Wu, Juliana Fonseca de Lima, Franck Millange, Osvaldo Antônio Serra, Dermot M. O'Hare, Richard I. Walton

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  36. Synthesis of MOFs: a personal view on rationalisation, application and exploration

    Dalton Transactions · 2017-01-01

    Helge Reinsch, Norbert Stock

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  37. Synthesis and electrochemical properties of Fe3O4@MOF core-shell microspheres as an anode for lithium ion battery application

    Applied Surface Science · 2017-02-04

    Xuemin Sun, Ge Gao, Dongwei Yan, Chuanqi Feng

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  38. Synthesis of highly efficient Mn 2 O 3 catalysts for CO oxidation derived from Mn-MIL-100

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    Xiaodong Zhang, Hong‐Xin Li, Fulin Hou, Yang Yang, Dong Jun Han, Ning Liu, Yuxin Wang, Lifeng Cui

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  39. Revealing the Initial Reaction Behavior in the Continuous Synthesis of Metal–Organic Frameworks Using Real-Time Synchrotron X-ray Analysis

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    Angelos Polyzoidis, Martin Etter, Michael J. Herrmann, Stefan Loebbecke, Robert E. Dinnebier

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  40. Co-Ligand Dependent Formation and Phase Transformation of Four Porphyrin-Based Cerium Metal–Organic Frameworks

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  41. Mn-MIL-100 heterogeneous catalyst for the selective oxidative cleavage of alkenes to aldehydes

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    Ying Ha, Manman Mu, Qingling Liu, Na Ji, Chunfeng Song, Degang Ma

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  42. In situ monitoring metal-ligand exchange processes by optical spectroscopy and X-ray diffraction analysis: a review

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    Huayna Terraschke, Merrit Rothe, Patric Lindenberg

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  43. A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions

    Review of Scientific Instruments · 2017-10-01

    Niclas Heidenreich, U. Rütt, Milan Köppen, A. Ken Inge, S. Beier, Ann‐Christin Dippel, Ralf Suren, Norbert Stock

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  44. Raman Observation of the “Volcano Curve” in the Formation of Carbonized Metal–Organic Frameworks

    The Journal of Physical Chemistry C · 2017-10-02

    Tsung Pei, Zhao‐Quan Zhang, Bing-Han Li, Madhan Vinu, Chia‐Her Lin, Szetsen Lee

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  45. Formation of a new type of uranium( iv ) poly-oxo cluster {U 38 } based on a controlled release of water via esterification reaction

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    Nicolas P. Martin, Christophe Volkringer, Natacha Henry, Xavier Trivelli, Grégory Stoclet, Atsushi Ikeda‐Ohno, Thierry Loiseau

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  46. Metal organic frameworks as a catalyst for oxygen reduction: an unexpected outcome of a highly active Mn-MOF-based catalyst incorporated in activated carbon

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    Shmuel Gonen, Oran Lori, Gili Cohen-Taguri, Lior Elbaz

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  47. MIL-100Cr with open Cr sites for a record N 2 O capture

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    Jiangfeng Yang, Bingjie Du, Jiaqi Liu, Rajamani Krishna, Feifei Zhang, Wei Zhou, Yong Wang, Jinping Li, Banglin Chen

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  48. Bi-metal organic framework derived nickel manganese oxide spinel for lithium-ion battery anode

    Materials Science and Engineering B · 2018-01-04

    Sandipan Maiti, Atin Pramanik, Tanumoy Dhawa, Monjoy Sreemany, Sourindra Mahanty

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  49. In Situ, Time-Resolved, and Mechanistic Studies of Metal–Organic Framework Nucleation and Growth

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    Mary J. Van Vleet, Tingting Weng, Xinyi Li, J. R. Schmidt

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  50. Facile Synthesis of Highly Efficient Amorphous Mn‐MIL‐100 Catalysts: Formation Mechanism and Structure Changes during Application in CO Oxidation

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