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RESEARCH PAPER · Angewandte Chemie International Edition · 2023

Multi‐Stimuli Responsive Luminescence and Domino Phase Transition of Hybrid Copper Halides with Nonlinear Optical Switching Behavior

Jiajing Wu, Yue Guo, Jing‐Li Qi, Wen‐Dong Yao, Su‐Xin Yu, Wenlong Liu, Sheng‐Ping Guo

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Multi‐Stimuli Responsive Luminescence and Domino Phase Transition of Hybrid Copper Halides with Nonlinear Optical Switching BehaviorOriginal(C 5 H 6.16 N 2 Cl 0.84 )(IO 2 Cl 2 ): a birefringent crystal featuring unprecedented (IO 2 Cl 2 ) − anions and π-conjugated organic cations56From H 12 C 4 N 2 CdI 4 to H 11 C 4 N 2 CdI 3 : a highly polarizable CdNI 3 tetrahedron induced a sharp enhancement of second harmonic generation response and birefringence50Quasi-linear CuX 2 (X = Cl, Br) motif-built hybrid copper halides realizing encouraging nonlinear optical activities28Unveiling the Superior Optical Properties of Novel Melamine‐Based Nonlinear Optical Material with Strong Second‐Harmonic Generation and Giant Optical Anisotropy74α- and β-(C4H5N2O)(IO3)·HIO3: Two SHG Materials Based on Organic–Inorganic Hybrid Iodates14Dual Monomeric Inorganic Units Constructed Bright Emissive Zero-Dimensional Antimony Chlorides with Solvent-Induced Reversible Structural Transition27Reversible tri-state structural transitions of hybrid copper( i ) bromides toward tunable multiple emissions45Ln 2 F 2 (OH 2 )(MoO 3 ) 2 (SeO 3 ) 2 : Promising Multifunctional Nonlinear Optical Materials Created by Partial Fluorination Strategy under Corrosion Resistant Supercritical Reactions25Cluster-Centered Excited-State-Induced Bright Low-Energy Emissive Hybrid Copper Iodide Constructing Stable White LEDs33Antimony Doping Enabled Photoluminescence Quantum Yield Enhancement in 0D Inorganic Bismuth Halide Crystals22Tellurium(IV) Halide Achieving Effective Nonlinear-Optical Activity: The Role of Chiral Ligands and Lattice Distortion17A UV non-hydrogen pure selenite nonlinear optical material for achieving balanced properties through framework-optimized structural transformation41Construction and characterization of an inorganic–organic hybrid copper( i ) iodide coordination polymer with semiconducting luminescence8Dual-color photoluminescence modulation of zero-dimensional hybrid copper halide microcrystals11Halide-driven polarity tuning and optimized SHG-bandgap balance in (C 4 H 11 N 2 )ZnX 3 (X = Cl, Br, I)34Solvent-induced structural regulation and luminescence switching of hybrid copper( i ) halides for encryption and anti-counterfeiting applications22Tunable luminescence based on structural regulation in organic antimony halides for X-ray scintillation16[C(NH2)3]6Mo7O24: A Guanidinium Molybdate as a UV Nonlinear Optical Crystal with Large Birefringence17Multisite Fine‐Tuning in Hybrid Cadmium Halides Enables Wide Range Emissions for Anti‐Counterfeiting6Multisite Fine‐Tuning in Hybrid Cadmium Halides Enables Wide Range Emissions for Anti‐Counterfeiting92Supramolecular Metal Halide Complexes for High-Temperature Nonlinear Optical Switches53Thermally Activated Delayed Fluorescent Binuclear Copper(I) Alkynyl Complexes with Cuprophilic Interactions8Dual-Emissive γ-[Cu4I8]4– Enables Luminescent Thermochromism in an Organic–Inorganic Hybrid Copper(I) Halide21Highly crystallization-induced emissive luminophores with mechanoluminescent features for two-photon harvesting fluorescence imaging and latent fingerprint identification5Optical Phenomena in Molecule-Based Magnetic Materials154Manipulating Chiroptical Activities in 0D Chiral Hybrid Manganese Bromides by Solvent Molecular Engineering26(C4H6N3O)(HSO4): A Cytosinium Bisulfate with Large Birefringence and Moderate Second Harmonic Generation Effect Produced via Combining a Promising Planar Nonlinear Optical-Active Motif with a Tetrahedral Group13Thermally Induced Reversible Fluorochromism by Self-Trapped Excitonic Emission in a Two-Dimensional Hybrid Copper(I)-Halide Single Crystal31Photoluminescent Cu(I) Assemblies with High‐Temperature Solid‐State Transitions as a New Class of Thermic History Tracers9Remarkable Second Harmonic Generation Response in (C 5 H 6 NO) + (CH 3 SO 3 ) − : Unraveling the Role of Hydrogen Bond in Thermal Driven Nonlinear Optical Switch50Remarkable Second Harmonic Generation Response in (C5H6NO)+(CH3SO3)−: Unraveling the Role of Hydrogen Bond in Thermal Driven Nonlinear Optical Switch10Highly Selective Protic-Solvent-Mediated Organic–Inorganic Hybrid Cuprous Bromides Achieving Structural Transformation20Near Ultraviolet‐Excitable Cyan‐Emissive Hybrid Copper(I) Halides Nonlinear Optical Crystals with Near‐Unity Photoluminescence Quantum Yield and High‐Efficiency X‐ray Scintillation82Near Ultraviolet‐Excitable Cyan‐Emissive Hybrid Copper(I) Halides Nonlinear Optical Crystals with Near‐Unity Photoluminescence Quantum Yield and High‐Efficiency X‐ray Scintillation13Unlocking the Potential of Organic‐Inorganic Hybrid Manganese Halides for Advanced Optoelectronic Applications169Organic‐Inorganic Cuprous Halides With Reversible Photoluminescence for Multiple Optical Applications38l -Homoproline-Directed Synthesis of Organic–Inorganic Metal Iodides for Second Harmonic Generation14Chirality and Solvent Coassist the Structural Evolution of Hybrid Manganese Chlorides with Second-Harmonic-Generation Response7CPL-active hybrid copper(I) halides enabled by cation inclusion with chiral crown-ether11Realizing Near‐Unity Photoluminescence Quantum Yield in Metal Halide RbCdCl3:Mn2+ Crystals via Phase Transformation Engineering16Reversible Structural Phase Transitions in Zero‐Dimensional Cu(I)‐Based Metal Halides for Dynamically Tunable Emissions76Reversible Structural Phase Transitions in Zero‐Dimensional Cu(I)‐Based Metal Halides for Dynamically Tunable Emissions5Enhancing Optical Properties of Zn‐Mn Solid Solution Hybrid Halides for Wide Color Gamut Backlight Displays11Polar Thiazole Derivative-Induced Second Harmonic Response in Hybrid Bismuth Chlorate with Reversible Photochromism9Guest‐Dependent Stimuli‐Responsive Photoluminescence in 0D Antimony Chlorides for Anticounterfeiting and Encryption Applications27A Highly Optical Anisotropic Hybrid Metal Halide for Modulation and Generation of Polarized Light44Two α‐SiO 2 ‐Related Deep‐Ultraviolet Phase‐Matchable Optical Nonlinear Beryllium Silicate Crystals Na 2 BeSiO 4 and Li 2 BeSiO 4 with Enhanced SHG Effect10Luminescence Thermochromism of a Noncluster Copper Iodide Complex4Rational Design of Single‐Component White‐Light Emissive Molecular Copper Clusters8Unusual Thermo‐Enhanced Second Harmonic Generation in Organic Configurationally‐Locked Polyene Crystals8“This or that” – light emission from hybrid organic–inorganic vs. coordination Cu( i ) halides77Organic Ligand Exchange: The Chiral Structure–Property Regulation of Cuprous Halides4Photochromic Film Based on a Mixed-Heteroatom-Templated ErIII-Incorporated Polyoxometalate Used for Inkless Prints and Anti-Counterfeiting19Water-triggered stimuli-responsive luminescent crown-ether-coordinated cuprous bromides for multi-functional applications15(C 14 H 14 N 2 )MCl 4 (M = Zn, Cd): two hybrid metal halides exhibiting strong second harmonic generation responses, large birefringence, and broadband photoluminescence12A high phase transition temperature organic–inorganic Sn( iv )-based metal halide designed by applying amino positional isomerism to the cation11An NIR-luminescent nitrate-bridged hybrid bimetal dielectric with a switchable dielectric constant2From poor-active to high performance via heteroleptic tetrahedra engineering: rational design of non-π-conjugated hybrids for phase-matchable ultraviolet nonlinear optics12Halogen and solvent effects induced structural transformation and isostructural luminescence regulation in copper-based hybrid halides8Manipulating weak interactions between host/guest and analytes in Cu(I)-cluster-based MOF for fluorescent gas sensing towards chlorinated volatile organic compounds19Multifunctional light-emitting materials based on hybrid copper iodide compounds2Multiple stimuli dual-optical mode responsive hybrid copper( i ) halides for advanced anti-counterfeiting and information encryption22Non-centrosymmetric structures designed rationally via a “dimensionality addition” strategy toward the promising nonlinear optical family [A–X][In–Se] (A = K/Ba and Rb/Ba; X = Cl and Br)13Prismatic crystal field stabilized divalent rare-earth chalcogenide REIIBII6CIII6QVI16 with bifunctionality30Zero-dimensional organic–inorganic hybrid antimony bromide with efficient broadband orange emission and nonlinear optical response17Cationic Modification in Hybrid Iodates: A Pathway to Superior Performance12Manganese halides with timely and delayed reversible thermal fluorescence quenching for dual-secure information encryption and anti-counterfeiting38Ultra-stable, multimodal, and reversible luminescence switching in 0D Mn(II)-based hybrid halide nanofiber film for photonic applications11In Situ Synthesis of Highly Emissive Manganese Halides with Modified Bisphosphonium Cations toward Information Encryption12Cost-effective fabrication of copper(I) halide arrays with mitigated optical crosstalk for high-definition X-ray radiography15An inorganic−organic hybrid KBBF-type zinc borate imidazole complex: A promising nonlinear-optical crystal4Toward the Strongest Nonlinear Optical Response and Largest Birefringence in Solvent‐Free Organic–Inorganic Metal Halides by Hydrogen Bond Engineering39Blue-Light-Excitable Yellow Emissive One-Dimensional Hybrid Copper(I) Iodide for White-Light-Emitting Diode and Methanol Sensing Application15Phase Engineering for Achieving Full‐Color Tunable Emission from Blue to Red and Multi‐Level Information Security in Isomeric Hybrid Copper Halides6Phase Engineering for Achieving Full‐Color Tunable Emission from Blue to Red and Multi‐Level Information Security in Isomeric Hybrid Copper Halides46[C(NH2)3]Y(HCOO)4: Constructing 3D Framework for Guanidine-Based UV Nonlinear Optical Crystals with Good Performance8Rearrangement of Sb···Br Secondary Bonds Resulting in Reversible Transformation between Dimeric and Chain-Like Antimony Bromide Hybrid Materials: Tunability of Electron Self-Trapped Luminescence and Proton Conductivity2Reversible Thermodynamic Phase‐Transition in Zero‐Dimensional Manganese Halides Enables Dual‐Secure Optical Information Anti‐Counterfeiting and Encryption21Halogens-co-mixing strategy for the elucidation of halogen effect in copper-based hybrid luminescent materials6Exploring stimuli‐responsive luminescence in metal halide perovskites for emerging applications17Enriching the emission from Mn2+-based organic-inorganic hybrid metal halides through Bi3+-doping for versatile applications6Structural Transformation and Luminescence Switching of Hybrid Antimony Halides for Single-Component White Light and Encryption18Polar Lithium l -Aspartate Monohydrate: A Semiorganic Ultraviolet Transparent Nonlinear Optical Crystal1A Bendable Photoluminescent Molecular Crystal with Phase Transition Accompanied by SHG Switching6Structural Evolution of Hybrid Bismuth-Based Halides toward Enhanced Second-Harmonic Generation Response and Birefringence through Multisite Chemical Substitution7Zero-Dimensional Antimony Oxychloride Scintillators with High Photoluminescent Efficiency7Thermally‐Induced Reversible Phase Transition and Luminescence Switching in 0D Hybrid Copper Halide Isomers for Anti‐Counterfeiting and Thermo‐Responsive Scintillators34KF·[SO 2 (NH 2 ) 2 ]: the First Deep‐Ultraviolet Transparent Sulfonamide Fluoride Nonlinear Optical Crystal with Novel Cairo Pentagonal Structure13KF·[SO 2 (NH 2 ) 2 ]: the First Deep‐Ultraviolet Transparent Sulfonamide Fluoride Nonlinear Optical Crystal with Novel Cairo Pentagonal Structure5Mechanochemical Construction of 0D Cu(I)-Based Luminescent Superclusters through Dynamic Ligand Fusion: Toward Eco-Friendly Stimuli-Switchable Optical Materials10Deprotonation-Regulated Conformational Switching in Malonates Enables High-Performance Ultraviolet Polar Crystals3pH‐Regulated Ring‐Opening/Closing Transformation in Polyoxometalates Enables High‐Performance Nonlinear Optical Crystals1pH‐Regulated Ring‐Opening/Closing Transformation in Polyoxometalates Enables High‐Performance Nonlinear Optical Crystals13Tetrahydroxyhexanedioic Acid-Ornamented Phosphite-and-Bismuth-Bridging Eu III -Encapsulated Phospho(III)tungstate and Its Photochromic and Photoluminescence Switching Properties8Charge Transfer Regulation toward Organic Copper Iodides with Tunable and Multiswitchable Full-Color Luminescence10A Predictive Framework for Discovering Organic Metal Halide Hybrids beyond Perovskites1Photoluminescence Enhancement in Zero-Dimensional Hybrid Copper Halide Single Crystals4H 3 PO 2 ‐Induced Dimensionality‐Dependent Photoluminescence in Hybrid Cuprous Halides with Reversible Transformation30D organic–inorganic hybrid chloroantimonate with thermochromic luminescence for optical temperature detection and anticounterfeiting0Excitation-wavelength-dependent emission of a luminescent host–guest Zn( ii ) metal–organic framework for high-performance white LEDs0From centrosymmetric (C 4 H 8 N 5 )(SbF 4 ) to polar (C 4 H 7 N 4 O)(SbF 4 ): a new UV nonlinear optical material achieved by functional group modulation8Solvent engineering for achieving six copper-based halides from a single organic cation: full-colour luminescence and multimode-stimulus response2Supramolecular template modulation in chiral lead bromide hybrids toward enhanced second-harmonic generation0Hybrid Cd 2+ -Based Halide Birefringent Crystals Achieving Tunable Dual-Color Emission for Multifunctional LED and Anticounterfeiting Applications2Pressure‐Gated Inverse Steric Enforcement in Coordinated Rotors as Programmable Optical Switching for Hierarchical Information Encryption2Zn 4 S(C 2 H 2 N 3 ) 3 (NCS) 3 : Coordination-Driven Structural Distortion Engineering Triggers Exceptional NLO Effect in Mixed-Bonding Zinc Isothiocyanate6Dynamic luminescence modulation in copper-cluster-based MOFs for advanced anti-counterfeiting applications2Unlocking Strong SHG Response and Large Birefringence in Hybrid Antimony Halides via a Three-in-One Strategy7Engineering Lattice Asymmetry via a Cs + ‐Triggered Domino Effect for Ultra‐Broadband Visible Emission from a Single Sb 3 + Luminophore0Nonlinear Optical Responses in One-Dimensional Zinc Thiocyanates Functionalized with Natural Amino Acids8Controllable Synthesis and Pressure-Induced Luminescence Response of Copper Bromide Hybrids for Latent Fingerprint Recognition, Writable Ink, and White Light-Emitting Diode1Hydrogen Bonding-Induced Synergistic Effect on Second-Harmonic Generation and High Photoluminescence of Morpholinium Cuprous Bromide Dihydrate Single Crystals1An Ultra-Wide Bandgap Sulfonate with Two-Step Second-Harmonic Generation Switching2Highly Anisotropic Quasi‐Direct Organic Metal Halide Hybrids: A Platform for Polarization‐Sensitive Optoelectronics1Supramolecular‐Assembled Chiral Cu(I) Halide Scintillators With Near‐Unity Cyan Photoluminescence for High‐Resolution X‐Ray Imaging4Luminescence Switching Red‐to‐Green in Zero‐Dimensional Manganese Halides via Dehydration‐Driven Structural Phase Transition for Anti‐Counterfeiting2Manganese(II) Mixed Halide: Enhanced Thermal/UV Stability and Humidity History Memory0Novel Organic–Inorganic Hybrid Cu(I)‐Based Metal Halides: Anti‐Thermal Quenching, Interconvertible Structure and Encryption Application0Reversible Transformation between 0D Cluster and 1D Chain with Luminescence and Dielectric Dual Switching in Two New Decanuclear Copper(I) Iodide Halides0Multi‐Component Lanthanide Halides for Multidimensional Optical Dynamic Anti‐Counterfeiting and Encryption Based on Stimulus‐Responsive Luminescence Regulation0Blue Light Emission and Stable Zero-Dimensional Hybrid Zinc Halide Modulated by Donor-π-Acceptor-Based Organic Cation0Fluorinated substituent engineering in naphthyl chalcone crystals for enhanced second-order nonlinear optical responses and measurable terahertz emission0Halogen-Driven Modulation of Structural Symmetry and Optical Properties in Hybrid Copper(I) Halides: Tunable Luminescence, Birefringence, and Composition-Dependent Second-Harmonic Generation0Ratiometric Luminescent Thermo‐Hygrometry, Metal‐Dependent Second Harmonic Generation, and Humidity‐Variable Magnetic Relaxation in a Manganese(II)‐Doped Zinc(II) Molecular Halide0Crystal‐Field Engineering of Excited‐State Dynamics in Sb 3+ ‐Doped Metal Halides for Versatile Optoelectronic Applications0

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  1. (C 5 H 6.16 N 2 Cl 0.84 )(IO 2 Cl 2 ): a birefringent crystal featuring unprecedented (IO 2 Cl 2 ) − anions and π-conjugated organic cations

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  2. From H 12 C 4 N 2 CdI 4 to H 11 C 4 N 2 CdI 3 : a highly polarizable CdNI 3 tetrahedron induced a sharp enhancement of second harmonic generation response and birefringence

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  3. Quasi-linear CuX 2 (X = Cl, Br) motif-built hybrid copper halides realizing encouraging nonlinear optical activities

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  4. Unveiling the Superior Optical Properties of Novel Melamine‐Based Nonlinear Optical Material with Strong Second‐Harmonic Generation and Giant Optical Anisotropy

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  5. α- and β-(C4H5N2O)(IO3)·HIO3: Two SHG Materials Based on Organic–Inorganic Hybrid Iodates

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  6. Dual Monomeric Inorganic Units Constructed Bright Emissive Zero-Dimensional Antimony Chlorides with Solvent-Induced Reversible Structural Transition

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  7. Reversible tri-state structural transitions of hybrid copper( i ) bromides toward tunable multiple emissions

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  8. Ln 2 F 2 (OH 2 )(MoO 3 ) 2 (SeO 3 ) 2 : Promising Multifunctional Nonlinear Optical Materials Created by Partial Fluorination Strategy under Corrosion Resistant Supercritical Reactions

    Advanced Science · 2023-10-23

    Yun‐Xiang Ma, Pengfei Li, Chun‐Li Hu, Jiang‐Gao Mao, Fang Kong

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  9. Cluster-Centered Excited-State-Induced Bright Low-Energy Emissive Hybrid Copper Iodide Constructing Stable White LEDs

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  10. Antimony Doping Enabled Photoluminescence Quantum Yield Enhancement in 0D Inorganic Bismuth Halide Crystals

    Inorganic Chemistry · 2023-11-21

    Zhen Jia, Pifu Gong, Mingxing Chen, Zhigang Wang, Xinhui Li, Yan Song, Shengnan Zhang, Ning Zhang, Mingjun Xia

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  11. Tellurium(IV) Halide Achieving Effective Nonlinear-Optical Activity: The Role of Chiral Ligands and Lattice Distortion

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  12. A UV non-hydrogen pure selenite nonlinear optical material for achieving balanced properties through framework-optimized structural transformation

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  13. Construction and characterization of an inorganic–organic hybrid copper( i ) iodide coordination polymer with semiconducting luminescence

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  14. Dual-color photoluminescence modulation of zero-dimensional hybrid copper halide microcrystals

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  15. Halide-driven polarity tuning and optimized SHG-bandgap balance in (C 4 H 11 N 2 )ZnX 3 (X = Cl, Br, I)

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  16. Solvent-induced structural regulation and luminescence switching of hybrid copper( i ) halides for encryption and anti-counterfeiting applications

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  17. Tunable luminescence based on structural regulation in organic antimony halides for X-ray scintillation

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  23. Dual-Emissive γ-[Cu4I8]4– Enables Luminescent Thermochromism in an Organic–Inorganic Hybrid Copper(I) Halide

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  27. (C4H6N3O)(HSO4): A Cytosinium Bisulfate with Large Birefringence and Moderate Second Harmonic Generation Effect Produced via Combining a Promising Planar Nonlinear Optical-Active Motif with a Tetrahedral Group

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  28. Thermally Induced Reversible Fluorochromism by Self-Trapped Excitonic Emission in a Two-Dimensional Hybrid Copper(I)-Halide Single Crystal

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  29. Photoluminescent Cu(I) Assemblies with High‐Temperature Solid‐State Transitions as a New Class of Thermic History Tracers

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  30. Remarkable Second Harmonic Generation Response in (C 5 H 6 NO) + (CH 3 SO 3 ) − : Unraveling the Role of Hydrogen Bond in Thermal Driven Nonlinear Optical Switch

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  31. Remarkable Second Harmonic Generation Response in (C5H6NO)+(CH3SO3)−: Unraveling the Role of Hydrogen Bond in Thermal Driven Nonlinear Optical Switch

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  32. Highly Selective Protic-Solvent-Mediated Organic–Inorganic Hybrid Cuprous Bromides Achieving Structural Transformation

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  33. Near Ultraviolet‐Excitable Cyan‐Emissive Hybrid Copper(I) Halides Nonlinear Optical Crystals with Near‐Unity Photoluminescence Quantum Yield and High‐Efficiency X‐ray Scintillation

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  34. Near Ultraviolet‐Excitable Cyan‐Emissive Hybrid Copper(I) Halides Nonlinear Optical Crystals with Near‐Unity Photoluminescence Quantum Yield and High‐Efficiency X‐ray Scintillation

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    Jing‐Li Qi, Yue Guo, Jiajing Wu, Qiao‐Feng Huang, Junjie Xu, Shufang Yan, Wenlong Liu, Sheng‐Ping Guo

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  35. Unlocking the Potential of Organic‐Inorganic Hybrid Manganese Halides for Advanced Optoelectronic Applications

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    Wei Zhang, Wei Zheng, Lingyun Li, Ping Huang, Jin Xu, Wen Ji Zhang, Zhiqing Shao, Xueyuan Chen

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  36. Organic‐Inorganic Cuprous Halides With Reversible Photoluminescence for Multiple Optical Applications

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  37. l -Homoproline-Directed Synthesis of Organic–Inorganic Metal Iodides for Second Harmonic Generation

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  38. Chirality and Solvent Coassist the Structural Evolution of Hybrid Manganese Chlorides with Second-Harmonic-Generation Response

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  39. CPL-active hybrid copper(I) halides enabled by cation inclusion with chiral crown-ether

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