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RESEARCH PAPER · Inorganic Chemistry · 2013

Crystal Growth of New Hexahydroxometallates Using a Hydroflux

W. Michael Chance, Daniel E. Bugaris, Athena S. Sefat, Hans‐Conrad zur Loye

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Crystal Growth of New Hexahydroxometallates Using a HydrofluxOriginalSynthesis and Crystal Structure of Dibarium Tungstate Hydrate, Ba2WO5·H2O7ChemInform Abstract: Crystal Growth of New Hexahydroxometallates Using a Hydroflux.0Synthesis, structure, and optical properties of a series of quaternary oxides, K2Ba(MO4)2 (M = Cr, Mo, W)21Synthesis, crystal structure, and magnetic properties of the oxometallates KBaMnO4 and KBaAsO412Hydrothermal Crystal Growth and Structure Determination of Double Hydroxides LiSb(OH)6, BaSn(OH)6, and SrSn(OH)628Synthesis and Crystal Structure of Sodium Arsenate Oxyhydroxide: Na4(AsO4)OH12Flux-mediated crystal growth of metal oxides: synthetic tunability of particle morphologies, sizes, and surface features for photocatalysis research154A 5 RE 4 X[TO 4 ] 4 crystal growth and photoluminescence. Hydroflux synthesis of sodium rare earth silicate hydroxides20Hydroflux synthesis and crystal structure of new lanthanide tungstate oxyhydroxides10New Insulating Antiferromagnetic Quaternary Iridates MLa10Ir4O24 (M = Sr, Ba)4Influence of rare earth cation size on the crystal structure in rare earth silicates, Na2RESiO4(OH) (RE = Sc, Yb) and NaRESiO4 (RE = La, Yb)22Understanding the Formation of Salt-Inclusion Phases: An Enhanced Flux Growth Method for the Targeted Synthesis of Salt-Inclusion Cesium Halide Uranyl Silicates61Synthesis of a Ferrolite: A Zeolitic All‐Iron Framework10Synthesis of a Ferrolite: A Zeolitic All‐Iron Framework1Where Do New Materials Come From? Neither the Stork nor the Birds and the Bees! In Search of the Next “First Material”1BaFe4O7 and K0.22Ba0.89Fe4O7: Canted Antiferromagnetic Diferrites with Exceptionally High Magnetic Ordering Temperatures18Hydrothermal Growth of Centimeter-Scale CuO Plates: Planar Chromium(III) Oligomer as a Facet-Directing Agent0Hydrothermal Synthesis, Study, and Classification of Microporous Uranium Silicates and Germanates18Ba3Na(OH)3(CO3)2: A Non-centrosymmetric Hydroxycarbonate Crystallized Using the Hydroflux Method2Alkaline-Earth Rhodium Hydroxides: Synthesis, Structures, and Thermal Decomposition to Complex Oxides14Oxo‐Hydroxoferrate K 2− x Fe 4 O 7− x (OH) x : Hydroflux Synthesis, Chemical and Thermal Instability, Crystal and Magnetic Structures26Incorporation of Si into Iron Oxide-based Microporous Zeolitic Framework for Improving Thermal Stability and Changing Guest Species1Antiferromagnetic Alkali Metal Oxohydroxoferrates(III) with Correlated Hydrogen Bonding Systems19Applications of Alkali Metal Hydroxide Hydrofluxes to the Synthesis of Single‐Crystal Ternary Actinide Oxides5Densification of a Solid-State NASICON Sodium-Ion Electrolyte Below 400 °C by Cold Sintering With a Fused Hydroxide Solvent60The Hydrogarnets Sr3[RE(OH)6]2 (RE = Sc, Y, Ho – Lu): Syntheses, Crystal Structures, and their Thermal Decomposition to Ternary Rare‐Earth Metal Oxides15CaNa[Cr(OH)6] – A Layered Hydroxochromate(III) with Ordered Brucite Structure and its Thermal Decomposition12Hydroflux-assisted densification: applying flux crystal growth techniques to cold sintering17Hydroflux synthesis and crystal structure of Tl3IO13Tunable Potassium Ion Conductivity and Magnetism in Substituted Layered Ferrates14Ba 3 [Rh(OH) 6 ] 2 ⋅ H 2 O – a Precursor to Barium Oxorhodates with One‐dimensional Hydrogen Bonding Systems9Recent Developments on Molten Salt Synthesis of Inorganic Nanomaterials: A Review207Dynamics of the Chemically Driven Densification of Barium Titanate Using Molten Hydroxides22Potassium Ion Conductivity in the Cubic Labyrinth of a Piezoelectric, Antiferromagnetic Oxoferrate(III) Tellurate(VI)11Chalcogenides by Reduction of their Dioxides in Ultra‐Alkaline Media27Chalkogenide durch Reduktion ihrer Dioxide in ultra‐alkalischen Medien6Reactions of Neptunium(V) in Alkali-Metal Hydroxides9Formation of Tetraselenodiarsenate(II) Anions in Ultra‐alkaline Medium4Orthoperiodato Rhodium(III) Complex as a Possible Key to Catalytic Oxidation of Organic Dyes6A top-down strategy for amorphization of hydroxyl compounds for electrocatalytic oxygen evolution154An unusual member of the solid solution series between cristobalite and potassium ferrate(III) obtained from hydroflux2Crystal structure of potassium orthoselenate(IV), K2SeO34Ba(BO 2 OH) – A Monoprotonated Monoborate from Hydroflux Showing Intense Second Harmonic Generation6Coherent approach to two-dimensional heterolayered oxychalcogenides using molten hydroxides21Rare‐Earth Hydroxometalates Ba[RE(OH)5] with RE=Tb, Dy, Ho5Discovery of chalcogenides structures and compositions using mixed fluxes53Sr(Ag 1− x Li x ) 2 Se 2 and [Sr 3 Se 2 ][(Ag 1− x Li x ) 2 Se 2 ] Tunable Direct Band Gap Semiconductors5Sr(Ag1−xLix)2Se2 and [Sr3Se2][(Ag1−xLix)2Se2] Tunable Direct Band Gap Semiconductors0K3[MO4][MO3N] (M=Tc, Re) – Nitridotrioxidorhenate and ‐technetate from Highly Alkaline Media3Oxohydroxo‐Tellurates(VI) K2[TeO2(OH)4] and K2[Fe2TeO6(OH)2] ⋅ 2H2O from Alkaline Hydroflux4Amorphous CoSnO3 for conductometric triethylamine gas sensing36Development of molten salt–based processes through thermodynamic evaluation assisted by machine learning9Hydroflux Synthesis and Structural Phase Transition of Rare‐Earth Borate Hydroxides Na2[RE(BO3)(OH)2] (RE=Y, Gd−Er)7Hydroflux crystal growth of alkali tellurate oxide-hydroxides0Mixed-Flux Techniques for Rational Synthesis and Structural Control in Silver Chalcogenides3Hydroflux Synthesis and Crystal Structures of Na5[RE(OH)6][MO4] (RE = Y, Sc, Er–Lu; M = Cr, Mo, W) and Na8[Sc(OH)6]2[CrO4]1Two Polymorphs of the Magnetic Catena ‐Orthoperiodato‐Cuprate(II) K 3 [CuIO 6 ]·4H 2 O from Ultra‐Alkaline Media1Denaturation of Water in Alkaline Melts2Eutectic-Mediated Template-Free Synthesis of Mesoporous Single-Crystalline CdS for CO 2 Photoreduction0Hydroflux Access to Hydroxide‐Free Yttrium Oxovanadate and Arsenite Layers: K 6 [Y(VO 4 ) 3 ]·2H 2 O, K 6 [Y(VO 4 ) 3 ], and Na 3 [Y(AsO 3 ) 2 ]0

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  1. Synthesis and Crystal Structure of Dibarium Tungstate Hydrate, Ba2WO5·H2O

    Journal of Chemical Crystallography · 2013-10-19

    W. Michael Chance, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  2. ChemInform Abstract: Crystal Growth of New Hexahydroxometallates Using a Hydroflux.

    ChemInform · 2013-12-12

    W. Michael Chance, Daniel E. Bugaris, Athena S. Sefat, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  3. Synthesis, structure, and optical properties of a series of quaternary oxides, K2Ba(MO4)2 (M = Cr, Mo, W)

    Solid State Sciences · 2013-12-22

    W. Michael Chance, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  4. Synthesis, crystal structure, and magnetic properties of the oxometallates KBaMnO4 and KBaAsO4

    Solid State Sciences · 2014-09-02

    Karl D. zur Loye, W. Michael Chance, Jeongho Yeon, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  5. Hydrothermal Crystal Growth and Structure Determination of Double Hydroxides LiSb(OH)6, BaSn(OH)6, and SrSn(OH)6

    Inorganic Chemistry · 2014-09-10

    Hiroshi Mizoguchi, Nattamai S. P. Bhuvanesh, Young‐Il Kim, Satoshi Ohara, Patrick M. Woodward

    Read original paper ↗ ·

  6. Synthesis and Crystal Structure of Sodium Arsenate Oxyhydroxide: Na4(AsO4)OH

    Journal of Chemical Crystallography · 2014-11-21

    Karl D. zur Loye, Allison M. Latshaw, Mark D. Smith, W. Michael Chance, Hans‐Conrad zur Loye

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  7. Flux-mediated crystal growth of metal oxides: synthetic tunability of particle morphologies, sizes, and surface features for photocatalysis research

    CrystEngComm · 2014-11-24

    Jonathan A. Boltersdorf, Nacole King, Paul A. Maggard

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  8. A 5 RE 4 X[TO 4 ] 4 crystal growth and photoluminescence. Hydroflux synthesis of sodium rare earth silicate hydroxides

    CrystEngComm · 2015-01-01

    Allison M. Latshaw, W. Michael Chance, Nathan M. Trenor, Gregory W. Morrison, Mark D. Smith, Jeongho Yeon, Derek E. Williams, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  9. Hydroflux synthesis and crystal structure of new lanthanide tungstate oxyhydroxides

    Solid State Sciences · 2015-03-04

    Allison M. Latshaw, Mark D. Smith, W. Michael Chance, Hans‐Conrad zur Loye

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  10. New Insulating Antiferromagnetic Quaternary Iridates MLa10Ir4O24 (M = Sr, Ba)

    Scientific Reports · 2015-07-01

    Qingbiao Zhao, Fei Han, Constantinos C. Stoumpos, Tianheng H. Han, Hao Li, John F. Mitchell

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  11. Influence of rare earth cation size on the crystal structure in rare earth silicates, Na2RESiO4(OH) (RE = Sc, Yb) and NaRESiO4 (RE = La, Yb)

    Solid State Sciences · 2015-11-25

    Allison M. Latshaw, Branford O. Wilkins, W. Michael Chance, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  12. Understanding the Formation of Salt-Inclusion Phases: An Enhanced Flux Growth Method for the Targeted Synthesis of Salt-Inclusion Cesium Halide Uranyl Silicates

    Journal of the American Chemical Society · 2016-05-24

    Gregory W. Morrison, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  13. Synthesis of a Ferrolite: A Zeolitic All‐Iron Framework

    Angewandte Chemie International Edition · 2016-09-21

    Allison M. Latshaw, W. Michael Chance, Gregory W. Morrison, Karl D. zur Loye, Branford O. Wilkins, Mark D. Smith, Pamela S. Whitfield, Melanie Kirkham, Sebastian A. Stoian, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  14. Synthesis of a Ferrolite: A Zeolitic All‐Iron Framework

    Angewandte Chemie · 2016-09-21

    Allison M. Latshaw, W. Michael Chance, Gregory W. Morrison, Karl D. zur Loye, Branford O. Wilkins, Mark D. Smith, Pamela S. Whitfield, Melanie Kirkham, Sebastian A. Stoian, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  15. Where Do New Materials Come From? Neither the Stork nor the Birds and the Bees! In Search of the Next “First Material”

    Scholar Commons (University of South Carolina) · 2017-01-01

    Gregory W. Morrison, Dileka Abeysinghe, Justin B. Felder, Shani Egodawatte, Timothy Ferreira, Hans‐Conrad zur Loye

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  16. BaFe4O7 and K0.22Ba0.89Fe4O7: Canted Antiferromagnetic Diferrites with Exceptionally High Magnetic Ordering Temperatures

    Chemistry of Materials · 2017-03-25

    Timothy Ferreira, Gregory W. Morrison, W. Michael Chance, Stuart Calder, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  17. Hydrothermal Growth of Centimeter-Scale CuO Plates: Planar Chromium(III) Oligomer as a Facet-Directing Agent

    Inorganic Chemistry · 2018-03-07

    Yuan Zhang, Long Yuan, Xia Zhong, Keke Huang, Shouhua Feng

    Read original paper ↗ ·

  18. Hydrothermal Synthesis, Study, and Classification of Microporous Uranium Silicates and Germanates

    Inorganic Chemistry · 2018-04-02

    Haijian Li, Philip Kegler, Dirk Bosbach, Evgeny V. Alekseev

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  19. Ba3Na(OH)3(CO3)2: A Non-centrosymmetric Hydroxycarbonate Crystallized Using the Hydroflux Method

    Journal of Chemical Crystallography · 2018-06-26

    Karl D. zur Loye, Allison M. Latshaw, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  20. Alkaline-Earth Rhodium Hydroxides: Synthesis, Structures, and Thermal Decomposition to Complex Oxides

    Inorganic Chemistry · 2018-08-14

    Daniel Sean Cook, Guy J. Clarkson, Daniel M. Dawson, Sharon Elizabeth Ashbrook, Janet M. Fisher, David Thompsett, David M. Pickup, Alan V Chadwick, Richard I. Walton

    Read original paper ↗ ·

  21. Oxo‐Hydroxoferrate K 2− x Fe 4 O 7− x (OH) x : Hydroflux Synthesis, Chemical and Thermal Instability, Crystal and Magnetic Structures

    ChemistryOpen · 2019-01-01

    Ralf Albrecht, Jens Hunger, Theresa Block, Rainer Pöttgen, Anatoliy Senyshyn, Thomas Doert, Michael Ruck

    Read original paper ↗ ·

  22. Incorporation of Si into Iron Oxide-based Microporous Zeolitic Framework for Improving Thermal Stability and Changing Guest Species

    Chemistry Letters · 2019-08-01

    Yuki Shinno, Kenta Iyoki, Tatsuya Okubo

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  23. Antiferromagnetic Alkali Metal Oxohydroxoferrates(III) with Correlated Hydrogen Bonding Systems

    ChemistryOpen · 2019-12-01

    Ralf Albrecht, Jens Hunger, Markus Hölzel, Theresa Block, Rainer Pöttgen, Thomas Doert, Michael Ruck

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  24. Applications of Alkali Metal Hydroxide Hydrofluxes to the Synthesis of Single‐Crystal Ternary Actinide Oxides

    Chemistry - A European Journal · 2019-12-05

    Evan Lyle Thomas, Samantha Stegman, S. Skanthakumar, Richard E. Wilson

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  25. Densification of a Solid-State NASICON Sodium-Ion Electrolyte Below 400 °C by Cold Sintering With a Fused Hydroxide Solvent

    ACS Applied Energy Materials · 2020-04-08

    Zane M. Grady, Kosuke Tsuji, Arnaud Ndayishimiye, Joo Hwan-Seo, Clive A. Randall

    Read original paper ↗ ·

  26. The Hydrogarnets Sr3[RE(OH)6]2 (RE = Sc, Y, Ho – Lu): Syntheses, Crystal Structures, and their Thermal Decomposition to Ternary Rare‐Earth Metal Oxides

    Zeitschrift für anorganische und allgemeine Chemie · 2020-04-15

    Ralf Albrecht, Thomas Doert, Michael Ruck

    Read original paper ↗ ·

  27. CaNa[Cr(OH)6] – A Layered Hydroxochromate(III) with Ordered Brucite Structure and its Thermal Decomposition

    Zeitschrift für anorganische und allgemeine Chemie · 2020-04-16

    Ralf Albrecht, Jens Hunger, Thomas Doert, Michael Ruck

    Read original paper ↗ ·

  28. Hydroflux-assisted densification: applying flux crystal growth techniques to cold sintering

    Journal of Materials Science · 2020-06-17

    Sarah Lowum, Richard D. Floyd, Jon‐Paul Maria

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  29. Hydroflux synthesis and crystal structure of Tl3IO

    Acta Crystallographica Section E Crystallographic Communications · 2020-09-11

    Ralf Albrecht, Heinrich Menning, Thomas Doert, Michael Ruck

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  30. Tunable Potassium Ion Conductivity and Magnetism in Substituted Layered Ferrates

    European Journal of Inorganic Chemistry · 2020-12-10

    Ralf Albrecht, Jens Hunger, Markus Hoelzel, Emmanuelle Suard, Walter Schnelle, Thomas Doert, Michael Ruck

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  31. Ba 3 [Rh(OH) 6 ] 2 ⋅ H 2 O – a Precursor to Barium Oxorhodates with One‐dimensional Hydrogen Bonding Systems

    Zeitschrift für anorganische und allgemeine Chemie · 2021-01-28

    Ralf Albrecht, Vincent Bretschneider, Thomas Doert, Michael Ruck

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  32. Recent Developments on Molten Salt Synthesis of Inorganic Nanomaterials: A Review

    The Journal of Physical Chemistry C · 2021-02-23

    Santosh K. Gupta, Yuanbing Mao

    Read original paper ↗ ·

  33. Dynamics of the Chemically Driven Densification of Barium Titanate Using Molten Hydroxides

    Nano Letters · 2021-04-14

    Arnaud Ndayishimiye, Mert Y. Sengul, Dooman Akbarian, Zhongming Fan, Kosuke Tsuji, Sun Hwi Bang, Adri C. T. van Duin, Clive A. Randall

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  34. Potassium Ion Conductivity in the Cubic Labyrinth of a Piezoelectric, Antiferromagnetic Oxoferrate(III) Tellurate(VI)

    Chemistry - A European Journal · 2021-07-28

    Ralf Albrecht, Markus Hoelzel, Henrik Beccard, Michael Rüsing, Lukas M. Eng, Thomas Doert, Michael Ruck

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  35. Chalcogenides by Reduction of their Dioxides in Ultra‐Alkaline Media

    Angewandte Chemie International Edition · 2021-08-10

    Ralf Albrecht, Michael Ruck

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  36. Chalkogenide durch Reduktion ihrer Dioxide in ultra‐alkalischen Medien

    Angewandte Chemie · 2021-08-10

    Ralf Albrecht, Michael Ruck

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  37. Reactions of Neptunium(V) in Alkali-Metal Hydroxides

    Inorganic Chemistry · 2021-11-12

    Richard E. Wilson, Samantha Stegman, Michael L. Tarlton

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  38. Formation of Tetraselenodiarsenate(II) Anions in Ultra‐alkaline Medium

    Zeitschrift für anorganische und allgemeine Chemie · 2021-11-22

    Ralf Albrecht, Franziska Jach, Michael Ruck

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  39. Orthoperiodato Rhodium(III) Complex as a Possible Key to Catalytic Oxidation of Organic Dyes

    Zeitschrift für anorganische und allgemeine Chemie · 2022-02-22

    Huanyu He, Ralf Albrecht, Michael Ruck

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  40. A top-down strategy for amorphization of hydroxyl compounds for electrocatalytic oxygen evolution

    Nature Communications · 2022-03-04

    Shangheng Liu, Shize Geng, Ling Li, Ying Zhang, Guomian Ren, Bolong Huang, Zhiwei Hu, Jyh‐Fu Lee, Yu-Hong Lai, Ying‐Hao Chu, Yong Xu, Qi Shao, Xiaoqing Huang

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  41. An unusual member of the solid solution series between cristobalite and potassium ferrate(III) obtained from hydroflux

    Zeitschrift für Naturforschung B · 2022-03-19

    Ralf Albrecht, Michael Ruck

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  42. Crystal structure of potassium orthoselenate(IV), K2SeO3

    Acta Crystallographica Section E Crystallographic Communications · 2022-05-17

    Ralf Albrecht, Thomas Doert, Michael Ruck

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  43. Ba(BO 2 OH) – A Monoprotonated Monoborate from Hydroflux Showing Intense Second Harmonic Generation

    Zeitschrift für anorganische und allgemeine Chemie · 2022-07-20

    Yuxi Li, Peter A. Hegarty, Michael Rüsing, Lukas M. Eng, Michael Ruck

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  44. Coherent approach to two-dimensional heterolayered oxychalcogenides using molten hydroxides

    Nature Synthesis · 2022-08-15

    Xiuquan Zhou, Christos D. Malliakas, Andrey Andreevich Yakovenko, Brandon Wilfong, Suyin G. Wang, Yu‐Sheng Chen, Lei Yu, Jianguo Wen, Mahalingam Balasubramanian, Hsien‐Hau Wang, Duck Young Chung, Mercouri G. Kanatzidis

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  45. Rare‐Earth Hydroxometalates Ba[RE(OH)5] with RE=Tb, Dy, Ho

    Zeitschrift für anorganische und allgemeine Chemie · 2022-10-24

    Yuxi Li, Ralf Albrecht, Michael Ruck

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  46. Discovery of chalcogenides structures and compositions using mixed fluxes

    Nature · 2022-11-09

    Xiuquan Zhou, Venkata Surya Chaitanya Kolluru, Wenqian Xu, Luqing Wang, Tieyan Chang, Yu‐Sheng Chen, Lei Yu, Jianguo Wen, Maria K. Y. Chan, Duck Young Chung, Mercouri G. Kanatzidis

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  47. Sr(Ag 1− x Li x ) 2 Se 2 and [Sr 3 Se 2 ][(Ag 1− x Li x ) 2 Se 2 ] Tunable Direct Band Gap Semiconductors

    Angewandte Chemie International Edition · 2023-01-27

    Xiuquan Zhou, Brandon Wilfong, Xinglong Chen, Craig C. Laing, Indra Raj Pandey, Ying‐Pin Chen, Yu‐Sheng Chen, Duck Young Chung, Mercouri G. Kanatzidis

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  48. Sr(Ag1−xLix)2Se2 and [Sr3Se2][(Ag1−xLix)2Se2] Tunable Direct Band Gap Semiconductors

    Angewandte Chemie · 2023-01-27

    Xiuquan Zhou, Brandon Wilfong, Xinglong Chen, Craig C. Laing, Indra Raj Pandey, Ying‐Pin Chen, Yu‐Sheng Chen, Duck Young Chung, Mercouri G. Kanatzidis

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  49. K3[MO4][MO3N] (M=Tc, Re) – Nitridotrioxidorhenate and ‐technetate from Highly Alkaline Media

    European Journal of Inorganic Chemistry · 2023-06-21

    Désirée Badea, Selina Olthof, Jörg‐M. Neudörfl, Robert Glaum, Rainer Pöttgen, Maximilian Kai Reimann, Klaus Meerholz, Max Reimer, Christian Logemann, Erik Strub, Jörn Bruns

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  50. Oxohydroxo‐Tellurates(VI) K2[TeO2(OH)4] and K2[Fe2TeO6(OH)2] ⋅ 2H2O from Alkaline Hydroflux

    Zeitschrift für anorganische und allgemeine Chemie · 2023-09-26

    Huanyu He, Yuxi Li, Ralf Albrecht, Michael Ruck

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