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RESEARCH PAPER · Inorganic Chemistry · 2011

Sulfates of the Refractory Metals: Crystal Structure and Thermal Behavior of Nb2O2(SO4)3, MoO2(SO4), WO(SO4)2, and Two Modifications of Re2O5(SO4)2

Ulf Betke, Mathias Siegfried Wickleder

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Sulfates of the Refractory Metals: Crystal Structure and Thermal Behavior of Nb2O2(SO4)3, MoO2(SO4), WO(SO4)2, and Two Modifications of Re2O5(SO4)2OriginalChemInform Abstract: Sulfates of the Refractory Metals: Crystal Structure and Thermal Behavior of Nb2O2(SO4)3, MoO2(SO4), WO(SO4)2, and Two Modifications of Re2O5(SO4)2.0Stabilizing Low‐Valent Refractory Metals in a Strongly Oxidizing Medium: The First Molybdenum(V) Sulfate—MoO(HSO4)(SO4)—from Mo(CO)6 in Oleum10Oleum and Sulfuric Acid as Reaction Media: Structural Features and Thermal Behavior of RE2[W2O3(SO4)6] (RE = Sm–Gd, Ho), RE2Nb2O2(SO4)3[H(SO4)2]2 (RE = Y, Ce–Nd, Sm–Er), Sm2Nb2O2(SO4)5(S2O7), and M2Nb4O5(SO4)8 (M = Bi, Eu)11Methanesulfonates of High‐Valent Metals: Syntheses and Structural Features of MoO2(CH3SO3)2, UO2(CH3SO3)2, ReO3(CH3SO3), VO(CH3SO3)2, and V2O3(CH3SO3)4 and Their Thermal Decomposition under N2 and O2 Atmosphere19The Unique bis-(Disulfato)-aurate Anion [Au(S2O7)2]−: Synthesis and Characterization of Li[Au(S2O7)2] and Na[Au(S2O7)2]26ReO2Cl(S2O7), a Molecular Disulfate23ReO2Cl(S2O7), ein molekulares Disulfat18The Oxidation of ReCl5 with Oleum: Synthesis and Crystal Structure of Re2O4Cl4(SO4)5Oleum and Sulfuric Acid as Reaction Media: The Actinide Examples UO2(S2O7)‐lt (low temperature), UO2(S2O7)‐ht (high temperature), UO2(HSO4)2, An(SO4)2 (An = Th, U), Th4(HSO4)2(SO4)7 and Th(HSO4)2(SO4)32Opening the paddlewheel: unusual coordination of [Mo2] dumbbells in the chain structures of A[Mo2(CF3SO3)5]·2CF3SO3H (A = Na, Rb, Cs)10Synthesis, characterization and thermal stability of a crystalline niobium oxysulfate12The [Au(CH3SO3)4]– Anion in the Crystal Structures of M[Au(CH3SO3)4] (M = Li, Na, Rb)9Sulfur-centred polyoxoniobate-based 3D organic–inorganic hybrid compound and its magnetic behavior34Promotion of ceria for decomposition of ammonia bisulfate over V2O5-MoO3/TiO2 catalyst for selective catalytic reduction101Justus‐Liebig‐Universität Gießen0A Niobium Oxyiodate Sulfate with a Strong Second‐Harmonic‐Generation Response Built by Rational Multi‐Component Design114A Niobium Oxyiodate Sulfate with a Strong Second‐Harmonic‐Generation Response Built by Rational Multi‐Component Design25Promotional effect of CeO2 on low-temperature selective catalytic reduction of NO by NH3 over V 2 O5-WO3/TiO2 catalysts19Microwave-Assisted Solid-State Synthesis of Dichalcogenide Nanostructures for Electrocatalytic Hydrogen Evolution8Crystal structure, optical properties and thermal properties of M 2 [W 2 O 3 (SO 4 ) 6 ] (M = Y, Eu, Tb, Lu, Bi)8RuOx doping synergistically enhances low-temperature H2O(g)/SO2 resistance of VWT catalysts: sacrificial site construction and oxygen activation mechanism3(NH 4 ) 2 [Tc 2 O 2 (S 2 O 7 ) 4 ]: An Unexpected Technetium(V)‐Sulfate From the Reaction of (NH 4 )(TcO 4 ) With SO 31Metal cation effects on the structural, optical and thermal properties of double tungstates AM(WO 4 ) 2 (A = Li, Na, K; M = Y, La, Ce, Pr, Nd, Sm, Bi)0On New Alkaline Sulfatometallates: Cs 6 [(WO 2 ) 2 O(SO 4 ) 4 ], K 8 [(MoO 2 ) 2 (SO 4 ) 6 ], K 7.9 Sr 0.1 [(WO 2 ) 2 (SO 4 ) 6 ] and Na 4 [MoO 2 (SO 4 ) 3 ]0

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  1. ChemInform Abstract: Sulfates of the Refractory Metals: Crystal Structure and Thermal Behavior of Nb2O2(SO4)3, MoO2(SO4), WO(SO4)2, and Two Modifications of Re2O5(SO4)2.

    ChemInform · 2011-03-03

    Ulf Betke, Mathias Siegfried Wickleder

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  2. Stabilizing Low‐Valent Refractory Metals in a Strongly Oxidizing Medium: The First Molybdenum(V) Sulfate—MoO(HSO4)(SO4)—from Mo(CO)6 in Oleum

    Chemistry - A European Journal · 2011-06-15

    Ulf Betke, Kai Neuschulz, Mathias Siegfried Wickleder

    Read original paper ↗ ·

  3. Oleum and Sulfuric Acid as Reaction Media: Structural Features and Thermal Behavior of RE2[W2O3(SO4)6] (RE = Sm–Gd, Ho), RE2Nb2O2(SO4)3[H(SO4)2]2 (RE = Y, Ce–Nd, Sm–Er), Sm2Nb2O2(SO4)5(S2O7), and M2Nb4O5(SO4)8 (M = Bi, Eu)

    European Journal of Inorganic Chemistry · 2011-09-01

    Ulf Betke, Mathias Siegfried Wickleder

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  4. Methanesulfonates of High‐Valent Metals: Syntheses and Structural Features of MoO2(CH3SO3)2, UO2(CH3SO3)2, ReO3(CH3SO3), VO(CH3SO3)2, and V2O3(CH3SO3)4 and Their Thermal Decomposition under N2 and O2 Atmosphere

    Chemistry - A European Journal · 2011-09-28

    Ulf Betke, Kai Neuschulz, Mathias Siegfried Wickleder

    Read original paper ↗ ·

  5. The Unique bis-(Disulfato)-aurate Anion [Au(S2O7)2]−: Synthesis and Characterization of Li[Au(S2O7)2] and Na[Au(S2O7)2]

    Inorganic Chemistry · 2011-09-29

    Christian Logemann, Mathias Siegfried Wickleder

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  6. ReO2Cl(S2O7), a Molecular Disulfate

    Angewandte Chemie International Edition · 2011-10-26

    Ulf Betke, Wilke Dononelli, Thorsten Klüner, Mathias Siegfried Wickleder

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  7. ReO2Cl(S2O7), ein molekulares Disulfat

    Angewandte Chemie · 2011-10-26

    Ulf Betke, Wilke Dononelli, Thorsten Klüner, Mathias Siegfried Wickleder

    Read original paper ↗ ·

  8. The Oxidation of ReCl5 with Oleum: Synthesis and Crystal Structure of Re2O4Cl4(SO4)

    Zeitschrift für anorganische und allgemeine Chemie · 2011-11-16

    Ulf Betke, Mathias Siegfried Wickleder

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  9. Oleum and Sulfuric Acid as Reaction Media: The Actinide Examples UO2(S2O7)‐lt (low temperature), UO2(S2O7)‐ht (high temperature), UO2(HSO4)2, An(SO4)2 (An = Th, U), Th4(HSO4)2(SO4)7 and Th(HSO4)2(SO4)

    European Journal of Inorganic Chemistry · 2011-12-06

    Ulf Betke, Mathias Siegfried Wickleder

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  10. Opening the paddlewheel: unusual coordination of [Mo2] dumbbells in the chain structures of A[Mo2(CF3SO3)5]·2CF3SO3H (A = Na, Rb, Cs)

    Dalton Transactions · 2012-01-01

    Kai Neuschulz, Miriam Penning, Lynn Groß, Thorsten Klüner, Mathias Siegfried Wickleder

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  11. Synthesis, characterization and thermal stability of a crystalline niobium oxysulfate

    Journal of Alloys and Compounds · 2012-01-13

    Qi Wang, Heng Jiang, Hong Gong, Gang Chu, Cuihua Lin, Xiaole Dong

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  12. The [Au(CH3SO3)4]– Anion in the Crystal Structures of M[Au(CH3SO3)4] (M = Li, Na, Rb)

    Zeitschrift für anorganische und allgemeine Chemie · 2012-06-11

    Christian Logemann, Mathias Siegfried Wickleder

    Read original paper ↗ ·

  13. Sulfur-centred polyoxoniobate-based 3D organic–inorganic hybrid compound and its magnetic behavior

    Chemical Communications · 2016-01-01

    Jufang Hu, Tian Han, Yingnan Chi, Zhengguo Lin, Yanqing Xu, Yang Song, Ding Wei, Yan‐Zhen Zheng, Changwen Hu

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  14. Promotion of ceria for decomposition of ammonia bisulfate over V2O5-MoO3/TiO2 catalyst for selective catalytic reduction

    Chemical Engineering Journal · 2016-05-28

    Liyun Song, Chao Jingdi, Yujiao Fang, Hong He, Jian Li, Wenge Qiu, Guizhen Zhang

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  15. Justus‐Liebig‐Universität Gießen

    Unknown journal · 2017-01-11

    Helmut Werner

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  16. A Niobium Oxyiodate Sulfate with a Strong Second‐Harmonic‐Generation Response Built by Rational Multi‐Component Design

    Angewandte Chemie International Edition · 2019-01-21

    Hong‐Xin Tang, Yu‐Xiao Zhang, Chao Zhuo, Ruibiao Fu, Hua Lin, Zuju Ma, Xin‐Tao Wu

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  17. A Niobium Oxyiodate Sulfate with a Strong Second‐Harmonic‐Generation Response Built by Rational Multi‐Component Design

    Angewandte Chemie · 2019-01-21

    Hong‐Xin Tang, Yu‐Xiao Zhang, Chao Zhuo, Ruibiao Fu, Hua Lin, Zuju Ma, Xin‐Tao Wu

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  18. Promotional effect of CeO2 on low-temperature selective catalytic reduction of NO by NH3 over V 2 O5-WO3/TiO2 catalysts

    Environmental Technology & Innovation · 2020-10-16

    Quanming Liang, Jian Li, Tao Yue

    Read original paper ↗ ·

  19. Microwave-Assisted Solid-State Synthesis of Dichalcogenide Nanostructures for Electrocatalytic Hydrogen Evolution

    ACS Applied Nano Materials · 2022-05-24

    Reeti Bajpai, Soumyendu Roy, Sandeep Kumar Verma

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  20. Crystal structure, optical properties and thermal properties of M 2 [W 2 O 3 (SO 4 ) 6 ] (M = Y, Eu, Tb, Lu, Bi)

    Dalton Transactions · 2024-01-01

    Vivien Wessels, Sofia Kügle, Henning A. Höppe

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  21. RuOx doping synergistically enhances low-temperature H2O(g)/SO2 resistance of VWT catalysts: sacrificial site construction and oxygen activation mechanism

    Applied Surface Science · 2025-08-31

    Weiwen Lu, Ao Li, Chengao Ding, Lu Jia, Hongming Long, Zhengwei Yu

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  22. (NH 4 ) 2 [Tc 2 O 2 (S 2 O 7 ) 4 ]: An Unexpected Technetium(V)‐Sulfate From the Reaction of (NH 4 )(TcO 4 ) With SO 3

    Chemistry - A European Journal · 2025-11-30

    Stefan Sutorius, Julian Heinen, David van Gerven, Jörn Bruns, Erik Strub, Mathias Siegfried Wickleder

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  23. Metal cation effects on the structural, optical and thermal properties of double tungstates AM(WO 4 ) 2 (A = Li, Na, K; M = Y, La, Ce, Pr, Nd, Sm, Bi)

    Dalton Transactions · 2026-01-01

    Vivien Wessels, Matthias Hämmer, Florian Becker, Anja Sandner, Narayan Simrit Kaur, Henning A. Höppe

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  24. On New Alkaline Sulfatometallates: Cs 6 [(WO 2 ) 2 O(SO 4 ) 4 ], K 8 [(MoO 2 ) 2 (SO 4 ) 6 ], K 7.9 Sr 0.1 [(WO 2 ) 2 (SO 4 ) 6 ] and Na 4 [MoO 2 (SO 4 ) 3 ]

    Zeitschrift für anorganische und allgemeine Chemie · 2026-01-04

    Vivien Wessels, Matthias Hämmer, Narayan Simrit Kaur, Lkhamsuren Bayarjargal, Henning A. Höppe

    Read original paper ↗ ·
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