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RESEARCH PAPER · Chemistry - A European Journal · 2011

Stabilizing Low‐Valent Refractory Metals in a Strongly Oxidizing Medium: The First Molybdenum(V) Sulfate—MoO(HSO4)(SO4)—from Mo(CO)6 in Oleum

Ulf Betke, Kai Neuschulz, Mathias Siegfried Wickleder

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Stabilizing Low‐Valent Refractory Metals in a Strongly Oxidizing Medium: The First Molybdenum(V) Sulfate—MoO(HSO4)(SO4)—from Mo(CO)6 in OleumOriginalChemInform Abstract: Stabilizing Low‐Valent Refractory Metals in a Strongly Oxidizing Medium: The First Molybdenum(V) Sulfate ‐ MoO(HSO4)(SO4) ‐ From Mo(CO)6 in Oleum.0Methanesulfonates of High‐Valent Metals: Syntheses and Structural Features of MoO2(CH3SO3)2, UO2(CH3SO3)2, ReO3(CH3SO3), VO(CH3SO3)2, and V2O3(CH3SO3)4 and Their Thermal Decomposition under N2 and O2 Atmosphere19The Unique bis-(Disulfato)-aurate Anion [Au(S2O7)2]−: Synthesis and Characterization of Li[Au(S2O7)2] and Na[Au(S2O7)2]26ReO2Cl(S2O7), a Molecular Disulfate23ReO2Cl(S2O7), ein molekulares Disulfat18The Oxidation of ReCl5 with Oleum: Synthesis and Crystal Structure of Re2O4Cl4(SO4)5Oleum and Sulfuric Acid as Reaction Media: The Actinide Examples UO2(S2O7)‐lt (low temperature), UO2(S2O7)‐ht (high temperature), UO2(HSO4)2, An(SO4)2 (An = Th, U), Th4(HSO4)2(SO4)7 and Th(HSO4)2(SO4)32Opening the paddlewheel: unusual coordination of [Mo2] dumbbells in the chain structures of A[Mo2(CF3SO3)5]·2CF3SO3H (A = Na, Rb, Cs)10The [Au(CH3SO3)4]– Anion in the Crystal Structures of M[Au(CH3SO3)4] (M = Li, Na, Rb)9Tb(HSO 4 )(SO 4 ) – a green emitting hydrogensulfate sulfate with second harmonic generation response21

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  1. ChemInform Abstract: Stabilizing Low‐Valent Refractory Metals in a Strongly Oxidizing Medium: The First Molybdenum(V) Sulfate ‐ MoO(HSO4)(SO4) ‐ From Mo(CO)6 in Oleum.

    ChemInform · 2011-09-08

    Ulf Betke, Kai Neuschulz, Mathias Siegfried Wickleder

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  2. Methanesulfonates of High‐Valent Metals: Syntheses and Structural Features of MoO2(CH3SO3)2, UO2(CH3SO3)2, ReO3(CH3SO3), VO(CH3SO3)2, and V2O3(CH3SO3)4 and Their Thermal Decomposition under N2 and O2 Atmosphere

    Chemistry - A European Journal · 2011-09-28

    Ulf Betke, Kai Neuschulz, Mathias Siegfried Wickleder

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  3. The Unique bis-(Disulfato)-aurate Anion [Au(S2O7)2]−: Synthesis and Characterization of Li[Au(S2O7)2] and Na[Au(S2O7)2]

    Inorganic Chemistry · 2011-09-29

    Christian Logemann, Mathias Siegfried Wickleder

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  4. ReO2Cl(S2O7), a Molecular Disulfate

    Angewandte Chemie International Edition · 2011-10-26

    Ulf Betke, Wilke Dononelli, Thorsten Klüner, Mathias Siegfried Wickleder

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  5. ReO2Cl(S2O7), ein molekulares Disulfat

    Angewandte Chemie · 2011-10-26

    Ulf Betke, Wilke Dononelli, Thorsten Klüner, Mathias Siegfried Wickleder

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  6. The Oxidation of ReCl5 with Oleum: Synthesis and Crystal Structure of Re2O4Cl4(SO4)

    Zeitschrift für anorganische und allgemeine Chemie · 2011-11-16

    Ulf Betke, Mathias Siegfried Wickleder

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  7. Oleum and Sulfuric Acid as Reaction Media: The Actinide Examples UO2(S2O7)‐lt (low temperature), UO2(S2O7)‐ht (high temperature), UO2(HSO4)2, An(SO4)2 (An = Th, U), Th4(HSO4)2(SO4)7 and Th(HSO4)2(SO4)

    European Journal of Inorganic Chemistry · 2011-12-06

    Ulf Betke, Mathias Siegfried Wickleder

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  8. Opening the paddlewheel: unusual coordination of [Mo2] dumbbells in the chain structures of A[Mo2(CF3SO3)5]·2CF3SO3H (A = Na, Rb, Cs)

    Dalton Transactions · 2012-01-01

    Kai Neuschulz, Miriam Penning, Lynn Groß, Thorsten Klüner, Mathias Siegfried Wickleder

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  9. The [Au(CH3SO3)4]– Anion in the Crystal Structures of M[Au(CH3SO3)4] (M = Li, Na, Rb)

    Zeitschrift für anorganische und allgemeine Chemie · 2012-06-11

    Christian Logemann, Mathias Siegfried Wickleder

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  10. Tb(HSO 4 )(SO 4 ) – a green emitting hydrogensulfate sulfate with second harmonic generation response

    Dalton Transactions · 2019-01-01

    Philip Netzsch, Harijs Bariss, Lkhamsuren Bayarjargal, Henning A. Höppe

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