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RESEARCH PAPER · Accounts of Chemical Research · 2018

Progress toward Solid State Synthesis by Design

Juan R. Chamorro, Tyrel M. McQueen

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Progress toward Solid State Synthesis by DesignOriginalPushing boundaries: High pressure, supercritical optical floating zone materials discovery24Nonpolar-to-Polar Trimerization Transitions in the S = 1 Kagomé Magnet Na 2 Ti 3 Cl 825Navigating the design space of inorganic materials synthesis using statistical methods and machine learning43Ceramics based on the Sm2O3–Y2O3 and Sm2O3–HfO2 systems at high temperatures: Thermodynamics and modeling20Controlling the Self-Assembly of New Metastable Tin Vanadium Selenides Using Composition and Nanoarchitecture of Precursors8Recycling of spent lithium nickel cobalt manganese oxides via a low-temperature ammonium sulfation roasting approach106Chemistry of Quantum Spin Liquids185Mechanistic insight of KBiQ 2 (Q = S, Se) using panoramic synthesis towards synthesis-by-design27A vapor thermal approach to selective recycling of spent lithium-ion batteries41Colloidal synthesis of metal chalcogenide nanomaterials from metal–organic precursors and capping ligand effect on electrocatalytic performance: progress, challenges and future perspectives36Mechanochemical methods for the transfer of electrons and exchange of ions: inorganic reactivity from nanoparticles to organometallics65Zincothermic reduction of silica to silicon: make the impossible possible30Predicting stable crystalline compounds using chemical similarity113Recent Developments on Molten Salt Synthesis of Inorganic Nanomaterials: A Review207Samarium zirconate: Thermodynamics and vaporization at high temperatures4Self-Driven Salt-Thermal Reduction Approach for the Synthesis of Cu2O and AgCl–Cu2O Hybrids with Superior Photocatalytic Activity10Observing and Modeling the Sequential Pairwise Reactions that Drive Solid‐State Ceramic Synthesis89Rational Solid-State Synthesis Routes for Inorganic Materials115Kinetically Stabilized Cation Arrangement in Li 3 YCl 6 Superionic Conductor during Solid‐State Reaction57Construction of Two‐Component Chemically Reactive Supramolecular Assemblies‐Acyl Migration Reactions in Cocrystals of Napthalene‐2,3‐Diol and Its Diesters0Capturing Metastable Oxide Semiconductors for Applications in Solar Energy Conversion44Radiation-Induced Solid-State Transformations of Uranyl Peroxides16Challenges in synthesis of heterostructures15Identification of a metastable uranium metal–organic framework isomer through non-equilibrium synthesis9Unconventional synthesis of novel borides: interplay between crystal structures, magnetic and catalytic properties0Investigation of Metastable Low Dimensional Halometallates5Review of computational approaches to predict the thermodynamic stability of inorganic solids196Review of modification strategies in emerging inorganic solid-state electrolytes for lithium, sodium, and potassium batteries288Renaissance of Topotactic Ion‐Exchange for Functional Solids with Close Packed Structures18Identifying New Classes of High Temperature Superconductors With Convolutional Neural Networks10Dataset of solution-based inorganic materials synthesis procedures extracted from the scientific literature83Path Less Traveled: A Contemporary Twist on Synthesis and Traditional Structure Solution of Metastable LiNi12B88Thin-Film Paradigm to Probe Interfacial Diffusion during Solid-State Metathesis Reactions4Investigation of the Pb–Fe–Se Ternary System and the Synthesis of a Ternary Pb1–xFexSe Phase3The chemistry of quantum materials2Machine-Learning Rationalization and Prediction of Solid-State Synthesis Conditions79High‐temperature mass spectrometric study and modeling of ceramics based on the Al 2 O 3 ‐SiO 2 ‐ZrO 2 system7Metal oxides based materials for display devices3Interpretable Machine Learning Enabled Inorganic Reaction Classification and Synthesis Condition Prediction41Metastability and Photoelectrochemical Properties of Cu 2 SnO 3 and Cu 2– x Li x TiO 3 : Two Cu(I)-Based Oxides with Delafossite Structures12Solid-State Synthesis of Aluminophosphate Zeotypes by Calcination of Amorphous Precursors21Refreshing the liquid-gas reaction interface to provoke the zincothermic reduction of SiCl4 to prepare lithium-storage nano silicon8Autonomous decision making for solid-state synthesis of inorganic materials1Precursor recommendation for inorganic synthesis by machine learning materials similarity from scientific literature65Transformation of K2Sb8Q13 and KSb5Q8 Bulk Crystals to Sb2Q3 (Q = S, Se) Nanofibers by Acid–Base Solution Chemistry7Predicting the synthesizability of crystalline inorganic materials from the data of known material compositions38Cation exchange route to a Eu(II)-containing tantalum oxide1Stability and Metastability of Li3YCl6 and Li3HoCl613A comprehensive review on perovskite and its functional composites in smart textiles: Progress, challenges, opportunities, and future directions69Autonomous and dynamic precursor selection for solid-state materials synthesis47Soft Chemistry of Hard Materials: Low-Temperature Pathways to Bulk and Nanostructured Layered Metal Borides17Exploring innovative approaches for enhanced performance of piezo catalysts19AlabOS: a Python-based reconfigurable workflow management framework for autonomous laboratories33High-efficiency tunable self-trapped exciton emission in one-dimensional β-Cs 3 Cu 2 Br 5 via Ag alloying for optoelectronic applications2Stable Ca-Pt Compounds Under Pressure0Unlocking the potential of open-tunnel oxides: DFT-guided design and machine learning-enhanced discovery for next-generation industry-scale battery technologies7Novelty Detection in the Design of Synthesis of Energy Storage Materials: a Case Study of Garnet-Structured Solid Electrolytes1Soft-Chemical Synthesis, Structure Evolution, and Insulator-to-Metal Transition in Pyrochlore-like λ-RhO25Optimal thermodynamic conditions to minimize kinetic by-products in aqueous materials synthesis26Automated analysis of surface facets: the example of cesium telluride6Novelty detection in the design of synthesis of garnet-structured solid electrolytes6Simple to Quadruple Perovskite Transformation by Coordination Switching upon Solid-State Ion Exchange of NaNbO33Graphene controlled solid-state growth of oxygen vacancies riched V2O5 catalyst to highly activate Fenton-like reaction3Particle‐Based Photoelectrodes for PEC Water Splitting: Concepts and Perspectives109Advances and prospects in the development of GdVO4-based photocatalysts for water pollutants removal activity: A review13Designing Topotactic Ion-Exchange Reactions in Solid-State Oxides Through First-Principles Calculations4Amalgams as Hydrogen-Free Reducing Agents for Topotactic Oxide Deintercalation3Kinetic and Thermodynamic Pathways Via Ion Exchange Metathesis of Cobalt Thiophosphate0Quantifying the regime of thermodynamic control for solid-state reactions during ternary metal oxide synthesis27Structural Evolution of Millisecond Laser-Induced Metastable Crystalline GeTe0Chemical Recycling of Step-Growth Polymers Guided by Le Chatelier’s Principle27Review on the Polymeric and Chelate Gel Precursor for Li-Ion Battery Cathode Material Synthesis22Solid-state synthesis of aluminophosphate-based zeotypes from conventional amorphous precursors: Strategy and catalytic performance4Experimental Testing of the Theoretically Predicted Magnetic Properties for Kagomé Compounds in the Li–Fe–Ge System3The Changing Landscape of Materials Discovery0Progress in multi-electron sodium vanadium phosphate cathode for emerging sodium-ion batteries50Green Synthesis of N,N′-(1,2-phenylene)bis(phthalimide-5-carboxilic acid) and the prediction of its properties: Standard enthalpies of formation and sublimation0Photoactivated solid-state self-assembly: a mechanochemistry-free route to high-purity aromatic amine crystals0How to accelerate the inorganic materials synthesis: from computational guidelines to data-driven method?9First-Principles and PSO-Driven Exploration of Ca-Pt Intermetallics: Stable Phases and Pressure-Driven Transitions0Green synthesis of N,N′-(1,2-phenylene)bis(phthalimide-5-carboxilic acid) and the prediction of its properties: Standard enthalpies of formation and sublimation3Efficient Recycling of Spent LiCoO 2 Cathodes Via Confined Pore‐Assisted Simplified Direct Carbothermic Reduction Without External Reducing Agents8Structural design and multiple magnetic orderings of the intergrowth compound Eu 2 CuMn 2 P 31Primitive Cubic Cation-Disordered Niobium Tungsten Oxides2Interplay Between Lone Pair Stereochemical Activity and Structural Anisotropy Drives Ultralow Thermal Conductivity in Layered AGeS 3 (A = Pb, Sn) Metal Sulfides10Nucleation-Limited Phase Formation in the Nb–Se Binary System0Unveiling phase evolution of complex oxides toward precise solid-state synthesis22High-performance mg-ion battery materials: Recent progress and future perspectives10Synthetic Accessibility and Sodium Ion Conductivity of the Na8–xAxP2O9 (NAP) High-Temperature Sodium Superionic Conductor Framework2Progress and Challenges in Li M OCl 4 and Na M OCl 4 ( M = Nb, Ta) Oxyhalide Solid Electrolytes for Solid‐State Batteries14Preferential Site Ordering Alters the Magnetic Behavior of Sm3Ru4Sn13–xGex (x = 0–2)1Iron-Directed Thermolysis of Pyridine- N -Oxide in Layered Metal Cyanides0Influence of microwave annealing on the structural, optical, and microwave dielectric properties of NBT thin films0Perovskite materials for multifaceted energy applications: From fundamental properties to industrialization challenges4Entropy-regulated solid-state synthesis of Na-based Mn-rich layered oxides2Gas-mediated defect engineering in earth-abundant Mn-rich layered oxides for non-aqueous sodium-based batteries12Non‐Equilibrium Manufacturing for High‐Energy‐Input Solid‐State Battery Materials6Smart Semiconductors: An Overview of AZnOS (A= Ca, Sr, Ba) Based Phosphors, Multi‐Stimuli Responsive Luminescence, and Potential Application Prospects12Chemical weathering of molecular single crystals to monoliths of quantum dots3A review on nano-structured electrodes for high-performance supercapacitors: panoramic insights across dimensional spectra35Reaction Pathway Informed Strategy for Fast Solid-State Synthesis of Garnet-Type Solid Electrolyte3Text-mined dataset of solid-state syntheses with impurity phases using Large Language Model6High-throughput ceramics processing method using cellulose nanofiber dispersions for rapid materials exploration0Small Gases, Big Effect: Regulating Microstructural Defects in Earth-Abundant Cathodes for Advanced Batteries0Thermodynamic assessment of machine learning models for solid-state synthesis prediction0Metastable Materials with Linear Chains: Photoinduced Chemical Reactions in K 2 X 2 (X = S, Se, Te)2Two-Step Growth of Layered Perovskite Y 2 Ti 2 O 5 S 2 Yields Faceted Crystals with Controlled Size and Morphology1Protonation-state engineering enables low-temperature and phase-selective synthesis of lanthanide tellurites and high-entropy derivatives0Ladder‐Like Structural Architecture of Layered Magnetic A 2.4 Cr 8 Te 14 ( A = Rb, Cs) Compounds by Self‐Flux Synthesis0Diffusion-Mediated Synthesis of Durable High-Entropy Sulfide Nanocrystals: Le Chatelier-Driven and Electron Configuration Effects2A Greener Solid-State Route to Thermochromic VO 2 (M1) Powders: Low-Vacuum Synthesis with Minimal Waste and Tungsten Doping1From synthesis to characterization: Advancing disordered rocksalts for cobalt-free lithium-ion batteries1A powder metallurgy review on synthesis and densification processing of REBCO superconductors0Syntheses, Structures and Optoelectronic Properties of Copper(I) Tungstate/Molybdate Solid Solutions0Photochemical Reactions in A 2 X 2 (A = Na, Rb and X = S, Se, Te): A Path toward Nonclassical Bonds in Metastable Compounds0Mechanochemistry for sustainable organometallic synthesis: A review across the d-block1Predicting Inorganic Material Synthesis Pathways Based on Language Models0Chloride‐Regulated Depolymerization of Aluminosilicate Networks for Fast Ion Transport Compliant Interfaces in Sustainable All‐Solid‐State Sodium Batteries0Chloride‐Regulated Depolymerization of Aluminosilicate Networks for Fast Ion Transport Compliant Interfaces in Sustainable All‐Solid‐State Sodium Batteries0Salt Flux Synthetic Catholicon: A Universal Route to Refractory and High-Entropy Alloys and Intermetallics0From Molecular Crystals to Electronic Devices: Investigating Structure–Property Relationships of Iron(III) and Cobalt(II) Coordination Complexes0Kinetic decoupling enables homogeneous phase evolution in single-crystal Ni-rich layered oxide synthesis0

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  1. Pushing boundaries: High pressure, supercritical optical floating zone materials discovery

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  2. Nonpolar-to-Polar Trimerization Transitions in the S = 1 Kagomé Magnet Na 2 Ti 3 Cl 8

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  5. Controlling the Self-Assembly of New Metastable Tin Vanadium Selenides Using Composition and Nanoarchitecture of Precursors

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  6. Recycling of spent lithium nickel cobalt manganese oxides via a low-temperature ammonium sulfation roasting approach

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  8. Mechanistic insight of KBiQ 2 (Q = S, Se) using panoramic synthesis towards synthesis-by-design

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  11. Mechanochemical methods for the transfer of electrons and exchange of ions: inorganic reactivity from nanoparticles to organometallics

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  18. Rational Solid-State Synthesis Routes for Inorganic Materials

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  41. Solid-State Synthesis of Aluminophosphate Zeotypes by Calcination of Amorphous Precursors

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  42. Refreshing the liquid-gas reaction interface to provoke the zincothermic reduction of SiCl4 to prepare lithium-storage nano silicon

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  43. Autonomous decision making for solid-state synthesis of inorganic materials

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  44. Precursor recommendation for inorganic synthesis by machine learning materials similarity from scientific literature

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  45. Transformation of K2Sb8Q13 and KSb5Q8 Bulk Crystals to Sb2Q3 (Q = S, Se) Nanofibers by Acid–Base Solution Chemistry

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  46. Predicting the synthesizability of crystalline inorganic materials from the data of known material compositions

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  47. Cation exchange route to a Eu(II)-containing tantalum oxide

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  48. Stability and Metastability of Li3YCl6 and Li3HoCl6

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  49. A comprehensive review on perovskite and its functional composites in smart textiles: Progress, challenges, opportunities, and future directions

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  50. Autonomous and dynamic precursor selection for solid-state materials synthesis

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