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RESEARCH PAPER · The Journal of Physical Chemistry Letters · 2011

In Situ Hydrothermal Synthesis of LiFePO4 Studied by Synchrotron X-ray Diffraction

Jiajun Chen, Jianming Bai, Haiyan Chen, Jason Graetz

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In Situ Hydrothermal Synthesis of LiFePO4 Studied by Synchrotron X-ray DiffractionOriginalWatching nanoparticle kinetics in liquid37Real-Time Probing of the Synthesis of Colloidal Silver Nanocubes with Time-Resolved High-Energy Synchrotron X-ray Diffraction47Synthesis and Electrochemical Properties of Li[Fe0.9Mn0.1]PO4Nanofibers as Cathode Material for Lithium Ion Battery by Electrospinning Method5Applications of in situ synchrotron XRD in hydrometallurgy: Literature review and investigation of chalcopyrite dissolution45Kinetically Controlled Lithium-Staging in Delithiated LiFePO4 Driven by the Fe Center Mediated Interlayer Li–Li Interactions60Free-standing Ag/C coaxial hybrid electrodes as anodes for Li-ion batteries9Recent Progress in Advanced Materials for Lithium Ion Batteries359In Situ Synchrotron X‐Ray Techniques for Real‐Time Probing of Colloidal Nanoparticle Synthesis75Nano particle LiFePO4 prepared by solvothermal process58Solvothermal synthesis of nanoscaled LiFePO4 with thinner thickness along [010] direction1Electrochemical properties of nanostructured Li[Fe0.9Mn0.1]PO4/C as a cathode material for lithium ion batteries prepared by electrospinning method13Rapid Synthesis of LiFePO4 by Coprecipitation12ZnO-doped LiFePO4 cathode material for lithium-ion battery fabricated by hydrothermal method35Morphology regulation of nano LiMn0.9Fe0.1PO4 by solvothermal synthesis for lithium ion batteries35Mössbauer spectroscopy study of defects in hydrothermally synthesized LiFePO4 cathode material5In Situ Studies of Solvothermal Synthesis of Energy Materials159Influence of anion species on the morphology of solvothermal synthesized LiMn0.9Fe0.1PO421A Facile Route To Modify Ferrous Phosphate and Its Use as an Iron-Containing Resource for LiFePO4 via a Polyol Process27Ultimate Limits to Intercalation Reactions for Lithium Batteries1130Hierarchical LiMnPO 4 assembled from nanosheets via a solvothermal method as a high performance cathode material21Hydrothermal synthesis, evolution, and electrochemical performance of LiMn 0.5 Fe 0.5 PO 4 nanostructures61Solvothermal Synthesis of LiMn1–xFexPO4Cathode Materials: A Study of Reaction Mechanisms by Time-Resolved in Situ Synchrotron X-ray Diffraction37Effect of ethylene glycol on morphology, crystallinity, and electrochemical properties of LiFePO4/C in lithium-ion batteries12Calendering effect on the electrochemical performances of the thick Li-ion battery electrodes using a three dimensional Ni alloy foam current collector27Cation exchange mediated elimination of the Fe-antisites in the hydrothermal synthesis of LiFePO471Electrode nanomaterials for lithium-ion batteries95Formation of tavorite-type LiFeSO4F followed by in situ X-ray diffraction5Cadmium phenylphosphonates: preparation, characterisation and in situ investigation33LiFePO4 Crystal Growth during Co-precipitation11Accelerated Removal of Fe-Antisite Defects while Nanosizing Hydrothermal LiFePO4 with Ca2+71Control of the LiFePO4 electrochemical properties using low-cost iron precursor in a melt process24In Situ XRD and TEM Studies of Sol-Gel-Based Synthesis of LiFePO431Confined synthesis of graphene wrapped LiMn0.5Fe0.5PO4 composite via two step solution phase method as high performance cathode for Li-ion batteries59Precursor‐Directed Nucleation and Self‐Assembly Growth: From Hollow Microprisms to Nanoplatelets4Effects of Antisite Defects on Li Diffusion in LiFePO4 Revealed by Li Isotope Exchange80Mild hydrothermal synthesis and crystal morphology control of LiFePO 4 by lithium nitrate14Reaction Mechanisms on Solvothermal Synthesis of Nano LiFePO 4 Crystals and Defect Analysis53Synchrotron X-ray Analytical Techniques for Studying Materials Electrochemistry in Rechargeable Batteries582Exploring the Peculiarities of LiFePO4 Hydrothermal Synthesis Using In Situ Calvet Calorimetry14Challenges in Developing Electrodes, Electrolytes, and Diagnostics Tools to Understand and Advance Sodium‐Ion Batteries287Pitfalls and reproducibility ofin situsynchrotron powder X-ray diffraction studies of solvothermal nanoparticle formation31Effect of Iron on Phosphate Recovery from Sewage Sludge15“Hydrotriphylites” Li 1– x Fe 1+ x (PO 4 ) 1– y (OH) 4 y as Cathode Materials for Li-ion Batteries23Zn ion diffusion in spinel-type cathode materials for rechargeable batteries: the role of point defects19Copper Surfaces with Bimodal Nanoporosity by Microstructural Length Scale Controlled Dealloying of a Hypereutectic Al-Cu Alloy3Ultrafast solid-liquid intercalation enabled by targeted microwave energy delivery29WITHDRAWN: Supercritical solvothermal synthesis and growth mechanism of nano lithium iron phosphate3Near room-temperature formation of Cu3Sn: In-situ synchrotron X-ray diffraction characterization and thermodynamic assessments of its nucleation6Controlled Hydrothermal/Solvothermal Synthesis of High‐Performance LiFePO 4 for Li‐Ion Batteries129Synthesis and Processing by Design of High‐Nickel Cathode Materials23In situ scattering studies of material formation during wet-chemical syntheses1Formation kinetics of sol-gel derived LiFePO4 olivine analyzed by reliable non-isothermal approach27Many-Particle Li Ion Dynamics in LiMPO4 Olivine Phosphates (M = Mn, Fe)22Mineral inspired electrode materials for metal-ion batteries2In situ characterisation for studying nucleation and growth of nanostructured materials and thin films during liquid-based synthesis7Electrical energy storage materials and devices for zero net energy buildings and clean transportation0Phase-Homogeneous LiFePO4 Powders with Crystallites Protected by Ferric-Graphite-Graphene Composite3Progress on solvo/hydrothermal synthesis and optimization of the cathode materials of lithium-ion battery68Control of the LiFePO4 electrochemical properties via a pray-drying-assisted a solid-phase reaction route using Fe3(PO4)2 as iron precursor0Concept Design of the CCU Skif–NSU Experimental Station 1-7 “Basic Methods of Synchrotron Diagnostics for Educational, Research, and Innovative Activities of Students”2Many-Particle Na-Ion Dynamics in NaMPO4 Olivine Phosphates (M = Mn, Fe)1The RAPTR furnace: a rapid heating and cooling sample furnace for in situ X-ray scattering studies of temperature-induced reactions4From waste to material strategy: A closed-loop regeneration process of spent LiFePO4 batteries21A composite reaction mechanism for the hydrothermal synthesis of olivine phosphates0From material synthesis to electrode processing, a holistic approach to enhance LiFePO4 sustainability3Synthesis, phase evolution pathways, and electrochemistry of phosphate-based cathode materials obtained using hydro/solvothermal treatment from simple oxide precursors1Advancing Battery Manufacturing: Synchrotron Characterization for Industry11

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  1. Watching nanoparticle kinetics in liquid

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  2. Real-Time Probing of the Synthesis of Colloidal Silver Nanocubes with Time-Resolved High-Energy Synchrotron X-ray Diffraction

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  3. Synthesis and Electrochemical Properties of Li[Fe0.9Mn0.1]PO4Nanofibers as Cathode Material for Lithium Ion Battery by Electrospinning Method

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  4. Applications of in situ synchrotron XRD in hydrometallurgy: Literature review and investigation of chalcopyrite dissolution

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  5. Kinetically Controlled Lithium-Staging in Delithiated LiFePO4 Driven by the Fe Center Mediated Interlayer Li–Li Interactions

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  6. Free-standing Ag/C coaxial hybrid electrodes as anodes for Li-ion batteries

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  7. Recent Progress in Advanced Materials for Lithium Ion Batteries

    Materials · 2013-01-10

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  8. In Situ Synchrotron X‐Ray Techniques for Real‐Time Probing of Colloidal Nanoparticle Synthesis

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  9. Nano particle LiFePO4 prepared by solvothermal process

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    Li Wang, Wenting Sun, Xianyi Tang, Xiankun Huang, Xiangming He, Jianjun Li, Qingwu Zhang, Jian Gao, Guangyu Tian, Shoushan Fan

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  10. Solvothermal synthesis of nanoscaled LiFePO4 with thinner thickness along [010] direction

    Russian Journal of Electrochemistry · 2013-04-01

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  11. Electrochemical properties of nanostructured Li[Fe0.9Mn0.1]PO4/C as a cathode material for lithium ion batteries prepared by electrospinning method

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  12. Rapid Synthesis of LiFePO4 by Coprecipitation

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  13. ZnO-doped LiFePO4 cathode material for lithium-ion battery fabricated by hydrothermal method

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    Yemin Hu, Jun Yao, Zhe Zhao, Mingyuan Zhu, Ying Li, Hongming Jin, Huijun Zhao, Jiazhao Wang

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  14. Morphology regulation of nano LiMn0.9Fe0.1PO4 by solvothermal synthesis for lithium ion batteries

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  15. Mössbauer spectroscopy study of defects in hydrothermally synthesized LiFePO4 cathode material

    Hyperfine Interactions · 2013-12-23

    Kirsten M. Ø. Jensen, H. P. Gunnlaugsson, Mogens Christensen, Bo B. Iversen

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  16. In Situ Studies of Solvothermal Synthesis of Energy Materials

    ChemSusChem · 2014-03-05

    Kirsten M. Ø. Jensen, Christoffer Tyrsted, Martin Bremholm, Bo B. Iversen

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  17. Influence of anion species on the morphology of solvothermal synthesized LiMn0.9Fe0.1PO4

    Electrochimica Acta · 2014-04-23

    Zhongjia Dai, Li Wang, Feipeng Ye, Chaochao Huang, Jixian Wang, Xiankun Huang, Jianlong Wang, Guangyu Tian, Xiangming He, Minggao Ouyang

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  18. A Facile Route To Modify Ferrous Phosphate and Its Use as an Iron-Containing Resource for LiFePO4 via a Polyol Process

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    Shaomin Li, Xichuan Liu, Rui Mi, Hao Liu, Yinchuan Li, Woon-min Lau, Jun Mei

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  19. Ultimate Limits to Intercalation Reactions for Lithium Batteries

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  20. Hierarchical LiMnPO 4 assembled from nanosheets via a solvothermal method as a high performance cathode material

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  21. Hydrothermal synthesis, evolution, and electrochemical performance of LiMn 0.5 Fe 0.5 PO 4 nanostructures

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  22. Solvothermal Synthesis of LiMn1–xFexPO4Cathode Materials: A Study of Reaction Mechanisms by Time-Resolved in Situ Synchrotron X-ray Diffraction

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  23. Effect of ethylene glycol on morphology, crystallinity, and electrochemical properties of LiFePO4/C in lithium-ion batteries

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  24. Calendering effect on the electrochemical performances of the thick Li-ion battery electrodes using a three dimensional Ni alloy foam current collector

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  25. Cation exchange mediated elimination of the Fe-antisites in the hydrothermal synthesis of LiFePO4

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  26. Electrode nanomaterials for lithium-ion batteries

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  27. Formation of tavorite-type LiFeSO4F followed by in situ X-ray diffraction

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  28. Cadmium phenylphosphonates: preparation, characterisation and in situ investigation

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  29. LiFePO4 Crystal Growth during Co-precipitation

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  30. Accelerated Removal of Fe-Antisite Defects while Nanosizing Hydrothermal LiFePO4 with Ca2+

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  32. In Situ XRD and TEM Studies of Sol-Gel-Based Synthesis of LiFePO4

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  33. Confined synthesis of graphene wrapped LiMn0.5Fe0.5PO4 composite via two step solution phase method as high performance cathode for Li-ion batteries

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  34. Precursor‐Directed Nucleation and Self‐Assembly Growth: From Hollow Microprisms to Nanoplatelets

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  35. Effects of Antisite Defects on Li Diffusion in LiFePO4 Revealed by Li Isotope Exchange

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  36. Mild hydrothermal synthesis and crystal morphology control of LiFePO 4 by lithium nitrate

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  37. Reaction Mechanisms on Solvothermal Synthesis of Nano LiFePO 4 Crystals and Defect Analysis

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  39. Exploring the Peculiarities of LiFePO4 Hydrothermal Synthesis Using In Situ Calvet Calorimetry

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  43. “Hydrotriphylites” Li 1– x Fe 1+ x (PO 4 ) 1– y (OH) 4 y as Cathode Materials for Li-ion Batteries

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