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RESEARCH PAPER · Chemistry of Materials · 2016

Toward Reaction-by-Design: Achieving Kinetic Control of Solid State Chemistry with Metathesis

Andrew J. Martinolich, James Richmond Neilson

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Toward Reaction-by-Design: Achieving Kinetic Control of Solid State Chemistry with MetathesisOriginalHigh-pressure discovery of β-NiBi17Materials space of solid-state electrolytes: unraveling chemical composition–structure–ionic conductivity relationships in garnet-type metal oxides using cheminformatics virtual screening approaches53Structure‐Selective Cation Exchange in the Synthesis of Zincblende MnS and CoS Nanocrystals77Structure‐Selective Cation Exchange in the Synthesis of Zincblende MnS and CoS Nanocrystals13One-Step, Solventless, and Scalable Mechanosynthesis of WO3·2H2O Ultrathin Narrow Nanosheets with Superior UV–Vis-Light-Driven Photocatalytic Activity41More than 2017 Reasons We Appreciate Our Authors, Reviewers, and Readers0Soft chemistry of ion-exchangeable layered metal oxides183Utilizing Diselenide Precursors toward Rationally Controlled Synthesis of Metastable CuInSe 2 Nanocrystals89V2Te2O: A Two-Dimensional van der Waals Correlated Metal37Structure-Selective Synthesis of Wurtzite and Zincblende ZnS, CdS, and CuInS2 Using Nanoparticle Cation Exchange Reactions81Pushing boundaries: High pressure, supercritical optical floating zone materials discovery24Hydride Synthesis and Thermoelectric Properties of Type-I Clathrate K8E8Ge38 (E = Al, Ga, In)17The development of strategies for nanoparticle synthesis: Considerations for deepening understanding of inherently complex systems20Epitaxial stabilization versus interdiffusion: synthetic routes to metastable cubic HfO 2 and HfV 2 O 7 from the core–shell arrangement of precursors9Selective Formation of Yttrium Manganese Oxides through Kinetically Competent Assisted Metathesis Reactions57A Hydride Route to Ternary Alkali Metal Borides: A Case Study of Lithium Nickel Borides30Heteroanionic Materials by Design: Progress Toward Targeted Properties237Self-Combustion Synthesis of Novel Metastable Ternary Molybdenum Nitrides28Multi-Step Topochemical Pathway to Metastable Mo 2 AlB 2 and Related Two-Dimensional Nanosheet Heterostructures161Semi-supervised machine-learning classification of materials synthesis procedures150Kinetically Controlled Low-Temperature Solid-State Metathesis of Manganese Nitride Mn3N227Yttrium Manganese Oxide Phase Stability and Selectivity Using Lithium Carbonate Assisted Metathesis Reactions17Catalytic behavior of hexaphenyldisiloxane in the synthesis of pyrite FeS 22Selective metathesis synthesis of MgCr 2 S 4 by control of thermodynamic driving forces44Selective Phase Control of Dopant-Free Potassium Sodium Niobate Perovskites in Solution34A Partial Anion Disorder in SrVO2H Induced by Biaxial Tensile Strain13A thermal-gradient approach to variable-temperature measurements resolved in space22The interplay between thermodynamics and kinetics in the solid-state synthesis of layered oxides264Similarity of Precursors in Solid-State Synthesis as Text-Mined from Scientific Literature85Polymorphic Metastability in Colloidal Semiconductor Nanocrystals46Defect-Accommodating Intermediates Yield Selective Low-Temperature Synthesis of YMnO 3 Polymorphs30Kinetic Pathways Templated by Low-Temperature Intermediates during Solid-State Synthesis of Layered Oxides68Chemistry of Quantum Spin Liquids185Mechanistic insight of KBiQ 2 (Q = S, Se) using panoramic synthesis towards synthesis-by-design27Honeycomb layered oxides: structure, energy storage, transport, topology and relevant insights94Mechanochemical methods for the transfer of electrons and exchange of ions: inorganic reactivity from nanoparticles to organometallics65Selective kinetic growth and role of local coordination in forming Al 2 TiO 5 -based coatings at lower temperatures8Halide Replacement with Complete Preservation of Crystal Lattice in Mixed‐Anion Lanthanide Oxyhalides26Halide Replacement with Complete Preservation of Crystal Lattice in Mixed‐Anion Lanthanide Oxyhalides1Lowering Ternary Oxide Synthesis Temperatures by Solid-State Cometathesis Reactions20A graph-based network for predicting chemical reaction pathways in solid-state materials synthesis119Rational Solid-State Synthesis Routes for Inorganic Materials115Ternary ACd4P3 (A = Na, K) Nanostructures via a Hydride Solution-Phase Route8In Situ Mechanistic Studies of Two Divergent Synthesis Routes Forming the Heteroanionic BiOCuSe27Panoramic (in beam) studies of materials synthesis1Ternary colloidal semiconductors for energy applications0Topochemical stabilization and single-crystal transformations of a metastable 2D γʹ-V2O5 intercalation cathode19Unconventional synthesis of novel borides: interplay between crystal structures, magnetic and catalytic properties0Investigation of Metastable Low Dimensional Halometallates5Experimental Synthesis of Theoretically Predicted Multivalent Ternary Nitride Materials73Metathesis routes to materials7Metastable hexagonal close-packed palladium hydride in liquid cell TEM91nmfMapping : a cloud-based web application for non-negative matrix factorization of powder diffraction and pair distribution function datasets16Thermodynamically Driven Synthetic Optimization for Cation‐Disordered Rock Salt Cathodes61Rapid and Energetic Solid-State Metathesis Reactions for Iron, Cobalt, and Nickel Boride Formation and Their Investigation as Bifunctional Water Splitting Electrocatalysts29Circumventing Thermodynamic Constraints in Nucleation-Controlled Crystallization of Al2TiO5-Based Chemical Vapor Deposition Coatings4Path Less Traveled: A Contemporary Twist on Synthesis and Traditional Structure Solution of Metastable LiNi12B88Electrocatalysis on oxide surfaces: Fundamental challenges and opportunities30Relative Kinetics of Solid-State Reactions: The Role of Architecture in Controlling Reactivity29Molecular Decomposition Routes of Diaryl Diselenide Precursors in Relation to the Phase Determination of Copper Selenides21Thermochemical reaction strategies for the rapid formation of inorganic solid-state materials3Role of Oxygen in Vacancy-Induced Phase Formation and Crystallization of Al2TiO5-Based Chemical Vapor-Deposited Coatings9Overlooked impact of precursor mixing: Implications in the electrochemical performance of battery electrode materials21Emergence of Dynamically‐Disordered Phases During Fast Oxygen Deintercalation Reaction of Layered Perovskite12Application of high energy X-ray diffraction and Rietveld refinement in layered lithium transition metal oxide cathode materials16Modernist materials synthesis: Finding thermodynamic shortcuts with hyperdimensional chemistry19In situ neutron diffraction to investigate the solid-state synthesis of Ni-rich cathode materials7Design Principles for Noncentrosymmetric Materials23Transformation of K2Sb8Q13 and KSb5Q8 Bulk Crystals to Sb2Q3 (Q = S, Se) Nanofibers by Acid–Base Solution Chemistry7Selective Synthesis of Perovskite Oxyhydrides Using a High-Pressure Flux Method5Predictive Synthesis of Copper Selenides Using a Multidimensional Phase Map Constructed with a Data-Driven Classifier32Stability and Metastability of Li3YCl6 and Li3HoCl613Assessing Thermodynamic Selectivity of Solid-State Reactions for the Predictive Synthesis of Inorganic Materials41Anionic Redox Topochemistry for Materials Design: Chalcogenides and Beyond9Soft Chemistry of Hard Materials: Low-Temperature Pathways to Bulk and Nanostructured Layered Metal Borides17An autonomous laboratory for the accelerated synthesis of inorganic materials1000Resolving Fast Relative Kinetics in Inorganic Solid-State Synthesis15Oxygen content：the key role enabling phase transition during calcination of sodium layered oxides cathode0Strategies to alleviate distortive phase transformations in Li-ion intercalation reactions: an example with vanadium pentoxide16Elucidating the Reaction Pathway in the Ammonolysis of MoO3 via In Situ Powder X-ray Diffraction and Transmission Electron Microscopy8Memory Effect on the Synthesis of Perovskite-Type Li-Ion Conductor LixLa2/3–x/3TiO3 (LLTO)15Synthesis of Inorganic Solids Using the Deep Eutectic Solvent (DES) Route0Structure and phase transitions in niobium and tantalum derived nanoscale transition metal perovskites, Ba(Ti,MV)O3, M=Nb,Ta5Data-driven physics-informed descriptors of cation ordering in multicomponent perovskite oxides17Kinetic and Thermodynamic Pathways Via Ion Exchange Metathesis of Cobalt Thiophosphate0Computationally Guided Synthesis of Battery Materials11A critical reflection on attempts to machine-learn materials synthesis insights from text-mined literature recipes16Concentration-Dependent Layer-Stacking and the Influence on Phase-Conversion in Colloidally Synthesized WSe2 Nanocrystals2Synthesis, Electronic Structure, and Redox Chemistry of Li 2 MnP 2 S 6 , a Candidate High-Voltage Cathode Material1Emerging Superionic Sulfide and Halide Glass–Ceramic Solid Electrolytes: Recent Progress and Future Perspectives26Coherent‐Precipitation‐Stabilized Phase Formation in Over‐Stoichiometric Rocksalt‐Type Li Superionic Conductors9Exploring the Solution-Based Metathesis Reaction Pathway Toward Cu3Si Formation0High- T c Ag x BC and Cu x BC superconductors accessible via topochemical reactions0Synthesis challenges, thermodynamic stability, and growth kinetics of La–Si–P ternary compounds1Solid-State Synthesis Enables Enhanced Crystallinity and Tunable Optical Properties in Lanthanum Oxytelluride2When Two Becomes Three: Predicting Stable Ternary Boron‐Based Compounds by Populating Unique Lattice Sites in Binary Prototype Structures0Rational Approaches toward the Design and Synthesis of Carbon Nanothreads9Synthesis and Characterization of Metastable Cobalt Honeycomb KCoAsO41Thermally quenched metastable phase in the Ising model with competing interactions0Unveiling phase evolution of complex oxides toward precise solid-state synthesis22Reaction pathway variability in electrochemical conversion reactions for ion batteries1Two-dimensional layered metal oxides (2D LMOs) for next-generation electronic devices8Discovering Complex Metal Chalcogenide Nanostructures through Nanoreactor-Mediated Synthesis3Anharmonic effects on the dynamical stability of Ce–Co–Cu intermetallic ternary compounds0Metastable Materials with Linear Chains: Photoinduced Chemical Reactions in K 2 X 2 (X = S, Se, Te)2Protonation-state engineering enables low-temperature and phase-selective synthesis of lanthanide tellurites and high-entropy derivatives0Phase-Pure Synthesis and Thermal Transport Properties of Metallic Telluride Cu5Ge2Te71A Synthetic Perspective of Strategies for Accessing Metastable Polymorphs: Lessons Learned from Hafnium(IV) Oxide0Composites of covalently linked lignin and cellulose from one feedstock0Thermodynamically-Selective Metathesis and Salt-Mediated Syntheses of Monoclinic BiVO40Next-generation materials and devices by combustion processes0Toward Reliable Materials Discovery: Lessons from Halide Double Perovskites0

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  12. Hydride Synthesis and Thermoelectric Properties of Type-I Clathrate K8E8Ge38 (E = Al, Ga, In)

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