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RESEARCH PAPER · Journal of Chemical Crystallography · 2006

A new dabco templated metal sulfate, (C6H14N2)[Mn (H2O)6](SO4)2. Chemical preparation, hydrogen-bonded structure and thermal decomposition

Walid Rekik, Houcine Naı̈li, Tahar Mhiri, Thierry Bataille B

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A new dabco templated metal sulfate, (C6H14N2)[Mn (H2O)6](SO4)2. Chemical preparation, hydrogen-bonded structure and thermal decompositionOriginalSynthesis, crystal structures, phase transition characterization and thermal decomposition of a new dabcodiium hexaaquairon(II) bis(sulfate): (C6H14N2)[Fe(H2O)6](SO4)2602,2′-Biimidazolium hexaaquamanganese(II) bis(sulfate)2Synthesis, structural characterisation and thermal decomposition of a new organic–inorganic hybrid material (C5H14N2)[Cu(SO4)2(H2O)4]·H2O16Ethylenediammonium tetraaquadisulfatomagnesium(II)10Crystal structure, phase transition and thermal decomposition of a copper (II) sulfate dihydrate containing a chiral organic ammonium cation23A Slow Leak Synthetic Route to Organically Templated Gallium Sulfates8Synthesis, characterization and magnetic properties of four new organically templated metal sulfates [C5H14N2][MII(H2O)6](SO4)2, (MII = Mn, Fe, Co, Ni)35Crystal Structure, Phase Transition and Thermal Behaviour of Dabcodiium hexaaquacopper(II) bis(selenate/sulfate), (C6H14N2)[Cu(H2O)6](S0.66Se0.34O4)28Ethylenediammonium tetraaquadisulfatocadmate7Synthesis, Crystal Structure and Characterization of a New Dabcodiium Hexaaquacobalt(II) Bis(Selenate), (C6H14N2)[Co(H2O)6](SeO4)215Synthesis, crystal structures and thermal behaviour of organic–inorganic hybrids incorporating a chiral diamine19Crystal structures of two enantiomorphous 2-ethylpiperazinediium hexaaquacopper sulfates [(R or S)-C5H14N2][Cu(H2O)6](SO4)26A new dabco-templated metal sulfate: 1,4-diazoniabicyclo[2.2.2]octane hexaaquacadmium bis(sulfate)1Three organically templated magnesium sulfates: Chemical preparation, hydrogen-bonded structures and thermal behavior16The structural transformation of monoclinic [(R)-C5H14N2][Cu(SO4)2(H2O)4]·2H2O into orthorhombic [(R)-C5H14N2]2[Cu(H2O)6](SO4)3: crystal structures and thermal behavior3Crystal structures and characterization of two divalent metal selenates templated by dabco, (C6H14N2)[MII(H2O)6](SeO4)2 (MII: NiII, ZnII)11A new nickel selenate templated by piperazine: chemical preparation, crystal structure, thermal decomposition, and magnetic properties13Divalent Copper Selenate Complex: Two Types of Octahedral Coordination in the Unit Cell and Disordered 1,4‐Diazabicyclo[2.2.2]octane53-D Hydrogen bonded networks of three organically templated cadmium sulfates. Dehydration reactions and crystallization behavior5Synthesis, structural characterization, IR- and Raman spectroscopy, magnetic properties of new organically templated metal sulfates with 4-aminopyridinium20NCI calculations for understanding a physical phase transition in (C 6 H 14 N 2 )[Mn(H 2 O) 6 ](SeO 4 ) 26Phase transition from disordered high-temperature to twinned low-temperature structure of tris(ethylenediamine)zinc(II) selenate3Spectroscopic, Structural and Thermal Properties of Three New Metal Nitrates Templated by DABCO: (C6H14N2)[MII(H2O)6](NO3)4 with MII: Mn, Ni and Zn7New Cobalt and Nickel Sulfates Templated with N,N'-Dimethyletethylenediammonium Cation: Synthesis, Crystal Structures, and Topological Features1Double sulfates with 1-methylpiperazinediium and divalent cations: Synthesis, structures, spectroscopic characterization, thermal stability, and topological features of (C5H14N2)[M(H2O)6](SO4)2∙H2O (M = Mg, Mn, Fe, Co, Ni, Zn, and Cd) and (C5H14N2)(SO4)∙H2O2Diethylenetriamine-driven assembly of a dimeric cadmium bromide hybrid and an organic bromide salt: structural, vibrational, optical, in silico study and biological insights1High-efficiency electro-Fenton mineralization of triclosan using a novel octahedral iron( iii ) complex: structure, mechanism, and performance4Integrated structural, vibrational, thermal, and optical characterization of a zinc-based organic–inorganic hybrid with DFT and molecular docking insights into its biological properties1Linking structure, reactivity, and function in a multifunctional zinc bromide hybrid material: application to bisphenol A sensing and antimicrobial activity0Structural, optical, and electrochemical properties of a new 1D copper( ii ) halometalate for highly sensitive dopamine detection2Non-centrosymmetric hybrid zinc halide crystal with dual NLO and Cu2+ sensing functionality2Structural, optical, and electrochemical properties of a copper (II) chloride hybrid for reliable detection of ascorbic acid in biological samples2Dual palladium sites and pseudo-gap optics in a 1D hybrid perovskite for sensing applications0

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  1. Synthesis, crystal structures, phase transition characterization and thermal decomposition of a new dabcodiium hexaaquairon(II) bis(sulfate): (C6H14N2)[Fe(H2O)6](SO4)2

    Journal of Solid State Chemistry · 2007-10-24

    S. Yahyaoui, Walid Rekik, Houcine Naı̈li, Tahar Mhiri, Thierry Bataille B

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  2. 2,2′-Biimidazolium hexaaquamanganese(II) bis(sulfate)

    Acta Crystallographica Section E Structure Reports Online · 2008-07-08

    Mukhtar A. Kurawa, Christopher J. Adams, A. Guy. Orpen

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  3. Synthesis, structural characterisation and thermal decomposition of a new organic–inorganic hybrid material (C5H14N2)[Cu(SO4)2(H2O)4]·H2O

    Polyhedron · 2009-04-01

    Fadhel Hajlaoui, S. Yahyaoui, Houcine Naı̈li, Tahar Mhiri, Thierry Bataille B

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  4. Ethylenediammonium tetraaquadisulfatomagnesium(II)

    Acta Crystallographica Section E Structure Reports Online · 2009-10-22

    Walid Rekik, Houcine Naı̈li, Tahar Mhiri, Thierry Bataille B

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  5. Crystal structure, phase transition and thermal decomposition of a copper (II) sulfate dihydrate containing a chiral organic ammonium cation

    Inorganica Chimica Acta · 2009-11-24

    Fadhel Hajlaoui, S. Yahyaoui, Houcine Naı̈li, Tahar Mhiri, Thierry Bataille B

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  6. A Slow Leak Synthetic Route to Organically Templated Gallium Sulfates

    Crystal Growth & Design · 2010-09-08

    Elizabeth A. Kaufman, Mat­thias Zeller, Alexander J. Norquist

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  7. Synthesis, characterization and magnetic properties of four new organically templated metal sulfates [C5H14N2][MII(H2O)6](SO4)2, (MII = Mn, Fe, Co, Ni)

    Dalton Transactions · 2011-01-01

    Fadhel Hajlaoui, Houcine Naı̈li, S. Yahyaoui, Mark M. Turnbull, Tahar Mhiri, Thierry Bataille B

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  8. Crystal Structure, Phase Transition and Thermal Behaviour of Dabcodiium hexaaquacopper(II) bis(selenate/sulfate), (C6H14N2)[Cu(H2O)6](S0.66Se0.34O4)2

    Journal of Chemical Crystallography · 2011-06-22

    Nouha Loulou Nkhili, Walid Rekik, Houcine Naı̈li, Tahar Mhiri, Thierry Bataille B

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  9. Ethylenediammonium tetraaquadisulfatocadmate

    Acta Crystallographica Section E Structure Reports Online · 2011-08-02

    Walid Rekik, Houcine Naı̈li, Tahar Mhiri, Thierry Bataille B

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  10. Synthesis, Crystal Structure and Characterization of a New Dabcodiium Hexaaquacobalt(II) Bis(Selenate), (C6H14N2)[Co(H2O)6](SeO4)2

    Journal of Chemical Crystallography · 2011-11-30

    Omar Kammoun, Nouha Loulou, Walid Rekik, Houcine Naı̈li, Tahar Mhiri, Thierry Bataille B

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  11. Synthesis, crystal structures and thermal behaviour of organic–inorganic hybrids incorporating a chiral diamine

    Journal of Organometallic Chemistry · 2011-12-01

    Fadhel Hajlaoui, Houcine Naı̈li, S. Yahyaoui, Alexander J. Norquist, Tahar Mhiri, Thierry Bataille B

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  12. Crystal structures of two enantiomorphous 2-ethylpiperazinediium hexaaquacopper sulfates [(R or S)-C5H14N2][Cu(H2O)6](SO4)2

    Journal of Structural Chemistry · 2012-03-01

    Fadhel Hajlaoui, Houcine Naı̈li, S. Yahyaoui, Tahar Mhiri, Thierry Bataille B

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  13. A new dabco-templated metal sulfate: 1,4-diazoniabicyclo[2.2.2]octane hexaaquacadmium bis(sulfate)

    Acta Crystallographica Section E Structure Reports Online · 2012-05-11

    Bi‐Qin Wang, Hai-Biao Yan, Cijun Fang, Zhi Zhang

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  14. Three organically templated magnesium sulfates: Chemical preparation, hydrogen-bonded structures and thermal behavior

    Solid State Sciences · 2012-09-11

    Walid Rekik, Houcine Naı̈li, Tahar Mhiri, Thierry Bataille B

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  15. The structural transformation of monoclinic [(R)-C5H14N2][Cu(SO4)2(H2O)4]·2H2O into orthorhombic [(R)-C5H14N2]2[Cu(H2O)6](SO4)3: crystal structures and thermal behavior

    Phase Transitions · 2013-05-23

    Salem Saïd, Noureddine Mhadhbi, Fadhel Hajlaoui, S. Yahyaoui, Alexander J. Norquist, Tahar Mhiri, Thierry Bataille B, Houcine Naı̈li

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  16. Crystal structures and characterization of two divalent metal selenates templated by dabco, (C6H14N2)[MII(H2O)6](SeO4)2 (MII: NiII, ZnII)

    Arabian Journal of Chemistry · 2013-09-18

    Nouha Loulou Nkhili, Walid Rekik, Houcine Naı̈li, Tahar Mhiri, Thierry Bataille B

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  17. A new nickel selenate templated by piperazine: chemical preparation, crystal structure, thermal decomposition, and magnetic properties

    Monatshefte für Chemie - Chemical Monthly · 2014-01-23

    Nouha Loulou Nkhili, Walid Rekik, Houcine Naı̈li

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  18. Divalent Copper Selenate Complex: Two Types of Octahedral Coordination in the Unit Cell and Disordered 1,4‐Diazabicyclo[2.2.2]octane

    Zeitschrift für anorganische und allgemeine Chemie · 2014-09-30

    Walid Rekik, Nouha Loulou Nkhili, Houcine Naı̈li, Slimane Dahaoui B

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  19. 3-D Hydrogen bonded networks of three organically templated cadmium sulfates. Dehydration reactions and crystallization behavior

    Journal of Coordination Chemistry · 2014-11-21

    Walid Rekik, Houcine Naı̈li, Thierry Bataille B

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  20. Synthesis, structural characterization, IR- and Raman spectroscopy, magnetic properties of new organically templated metal sulfates with 4-aminopyridinium

    Journal of Molecular Structure · 2016-05-11

    Tamara J. Bednarchuk, Vasyl Kinzhybalo, Oleksandr Bednarchuk, A. Pietraszko

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  21. NCI calculations for understanding a physical phase transition in (C 6 H 14 N 2 )[Mn(H 2 O) 6 ](SeO 4 ) 2

    Solid State Sciences · 2017-10-23

    Houcine Naı̈li, Michel François, Alexander J. Norquist, Walid Rekik

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  22. Phase transition from disordered high-temperature to twinned low-temperature structure of tris(ethylenediamine)zinc(II) selenate

    Monatshefte für Chemie - Chemical Monthly · 2019-09-17

    Marwa Abid Derbel, Michel François, Houcine Naı̈li, Walid Rekik

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  23. Spectroscopic, Structural and Thermal Properties of Three New Metal Nitrates Templated by DABCO: (C6H14N2)[MII(H2O)6](NO3)4 with MII: Mn, Ni and Zn

    Journal of Inorganic and Organometallic Polymers and Materials · 2020-03-14

    Dhouha Ben Hassan, Houcine Naı̈li, Walid Rekik

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  24. New Cobalt and Nickel Sulfates Templated with N,N'-Dimethyletethylenediammonium Cation: Synthesis, Crystal Structures, and Topological Features

    Crystallography Reports · 2025-06-01

    Dmitri O. Charkin, V. E. Kireev, Н. В. Сомов, Dmitri N. Dmitriev, A. M. Banaru, Sergey M. Aksenov

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  25. Double sulfates with 1-methylpiperazinediium and divalent cations: Synthesis, structures, spectroscopic characterization, thermal stability, and topological features of (C5H14N2)[M(H2O)6](SO4)2∙H2O (M = Mg, Mn, Fe, Co, Ni, Zn, and Cd) and (C5H14N2)(SO4)∙H2O

    Polyhedron · 2025-09-05

    Dmitri O. Charkin, Alevtina N. Gosteva, Vadim A. Kireev, A. M. Banaru, Dmitri N. Dmitriev, Dina V. Deyneko, Nikita Sergeyevich Tsvetov, Ivan Gundarovich Tananaev, Sergey M. Aksenov

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  26. Diethylenetriamine-driven assembly of a dimeric cadmium bromide hybrid and an organic bromide salt: structural, vibrational, optical, in silico study and biological insights

    RSC Advances · 2026-01-01

    Iteb Ben Mahmoud, Mashael A. Alghamdi, Houda Lazreg Aref, Noureddine Mhadhbi, Hossam H. Nasrallah, Ahlem Guesmi, Naoufel Ben Hamadi, Sandra Walha, Ferdinando Costantino, Houcine Naı̈li

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  27. High-efficiency electro-Fenton mineralization of triclosan using a novel octahedral iron( iii ) complex: structure, mechanism, and performance

    RSC Advances · 2026-01-01

    Nejmeddine Rabaaoui, Ahlem Guesmi, Wiem Jabeur, Noureddine Mhadhbi, Naoufel Ben Hamadi, Lotfi Khezami, Mourad Cherif, Houcine Naı̈li

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  28. Integrated structural, vibrational, thermal, and optical characterization of a zinc-based organic–inorganic hybrid with DFT and molecular docking insights into its biological properties

    RSC Advances · 2026-01-01

    Hiba Khlifi, Mashael A. Alghamdi, Intissar Tababi, Hayet Edziri, Marwa Melliti, Ahlem Guesmi, Hossam H. Nasrallah, Noureddine Mhadhbi, Naoufel Ben Hamadi, Houcine Naı̈li

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  29. Linking structure, reactivity, and function in a multifunctional zinc bromide hybrid material: application to bisphenol A sensing and antimicrobial activity

    RSC Advances · 2026-01-01

    Intissar Hamdi, K. S. Al-Namshah, Hayet Edziri, Jassem Wannassi, Noureddine Mhadhbi, Marwa Melliti, Ali Ben Ahmed, Ahlem Guesmi, Naoufel Ben Hamadi, Houcine Barhoumi, Houcine Naı̈li

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  30. Structural, optical, and electrochemical properties of a new 1D copper( ii ) halometalate for highly sensitive dopamine detection

    Dalton Transactions · 2026-01-01

    Hiba Khlifi, Jassem Wannassi, Noureddine Mhadhbi, Hajir Wahbi, Erwann Jeanneau B, Naoufel Ben Hamadi, Ahlem Guesmi, Lotfi Khezami, Houcine Barhoumi, Houcine Naı̈li

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  31. Non-centrosymmetric hybrid zinc halide crystal with dual NLO and Cu2+ sensing functionality

    Microchemical Journal · 2026-02-10

    Intissar Hamdi, Jassem Wannassi, Noureddine Mhadhbi, Ali Ben Ahmed, Erwann Jeanneau B, Naoufel Ben Hamadi, Ahlem Guesmi, Lotfi Khezami, Houcine Barhoumi, Houcine Naı̈li

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  32. Structural, optical, and electrochemical properties of a copper (II) chloride hybrid for reliable detection of ascorbic acid in biological samples

    Journal of Molecular Structure · 2026-03-27

    Najeh Abbassi, Hajir Wahbi, Jassem Wannassi, Noureddine Mhadhbi, Walid Rekik, Naoufel Ben Hamadi, Ahlem Guesmi, Lotfi Khezami, Houcine Barhoumi, Houcine Naı̈li

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  33. Dual palladium sites and pseudo-gap optics in a 1D hybrid perovskite for sensing applications

    Inorganic Chemistry Communications · 2026-09-06

    Imen Khannoussi, Jassem Wannassi, Noureddine Mhadhbi, Abdellah Tahiri, Ahlem Guesmi, Wesam Abd El‐Fattah, Naoufel Ben Hamadi, Hajir Wahbi, Houcine Barhoumi, Houcine Naı̈li

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