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RESEARCH PAPER · Journal of Solid State Chemistry · 2007

Hydrothermal chemistry of Th(IV) with aromatic dicarboxylates: New framework compounds and in situ ligand syntheses

Kate L. Ziegelgruber, Karah E. Knope, M. Frisch, Christopher L. Cahill

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Hydrothermal chemistry of Th(IV) with aromatic dicarboxylates: New framework compounds and in situ ligand synthesesOriginalThe first uranyl–lanthanide heterometallic complexes: metal–organic frameworks with DOTA and oxalato ligands45Syntheses, crystal structures and photoluminescence of two new pyrazinecarboxylate-based cadmium(II) coordination polymers27Thorium(IV) Coordination Polymers in the Pyridine and Pyrazinedicarboxylic Acid Systems56In Situ Synthesis of Tetradentate Dye for Construction of Three-Dimensional Homochiral Phosphor64New Examples of Metal Coordination Architectures of 3,3′,4,4′‐Biphenyltetracarboxylic Acid – Syntheses, Crystal Structures, and Physical Properties31Structural variability in uranyl–lanthanide heterometallic complexes with DOTA and oxalato ligands49Hydrothermal in situ ligand reaction: copper(II)-mediated stepwise oxidation of 2,3,5- and 2,4,6-trimethylpyridine to pyridinecarboxylates22Uranyl Ion Complexation by Cucurbiturils in the Presence of Perrhenic, Phosphoric, or Polycarboxylic Acids. Novel Mixed-Ligand Uranyl−Organic Frameworks79Hydrothermal Synthesis and Crystal Structures of Cd(II)-Based 1D Coordination Polymer and Mn(II) Coordination Complex with Mixed N- and O-donor Ligands: [Cd2(4-4′-bpy)2(pa)4] n ·0.25(H2O) and [Mn(4-4′-bpy)2(pa)(H2O)3]ClO4·2(H2O)4Uranyl–organic assemblies with the macrocyclic ligand 1,4,8,11-tetraazacyclotetradecane-1,4,8,11-tetraacetate (TETA)34X-Ray Diffraction and μ-Raman Investigation of the Monoclinic-Orthorhombic Phase Transition in Th1−xUx(C2O4)2·2H2O Solid Solutions73Crystal structure of diaqua-bis(hydrogen 2-propyl-1H-imidazole-4,5-dicarboxylato)calcium(II), Ca(H2O)2(C8H9N2O4)24Crystal structure of triaqua-(pyrazine-2,3-dicarboxylato)cerium(III), Ce(H2O)3(C6H2N2O4)2Crystal chemistry of thorium nitrates and chromates23Crystal structure of hexaaqua-bis(pyridine-2,6-dicarboxylato)-oxalatodiytterbium( III) pentahydrate, Yb2(H2O)6(C7H3NO4)2(C2O4) · 5H2O2Hydrothermal Synthesis of Uranyl Squarates and Squarate-Oxalates: Hydrolysis Trends and in Situ Oxalate Formation82catena-Poly[thorium(IV)-tetrakis(μ2-3-carboxyadamantane-1-carboxylato)]: a quadruple helical strand driven by a synergy of coordination and hydrogen bonding9Uranyl triazolate formation via an in situ Huisgen 1,3-dipolar cycloaddition reaction23Refinement of the crystal structure of triaqua(2,3-pyrazinedi-carboxylato) cadmium(II), Cd(H2O)3(C6H2N2O4), a correction to the article “Crystal structure of triaqua(2,3-pyrazinedicarboxylato)-cerium(III), Ce(H2O)3(C6H2N2O4)”, Z. Kristallogr. NCS 225 (2010) 71-730In situ oxalate formation during hydrothermal synthesis of uranyl hybrid materials50Oxalate Bridged Copper Pyrazole Complex Templated Anderson-Evans Cluster Based Solids23Solid State Structure of Thorium(IV) Complexes with Common Aminopolycarboxylate Ligands42Controlling Disulfide Bond Formation and Crystal Growth from 2-Mercaptobenzoic Acid39Uranyl Ion Complexation by Aliphatic Dicarboxylic Acids in the Presence of Cucurbiturils as Additional Ligands or Structure-Directing Agents124Uranyl–Alkali Metal Ion Heterometallic Complexes with Cucurbit[6]uril and a Sulfonated Catechol67New Metal–Organic Framework Solids Built from Barium and Isoelectronic Chelidamic and Chelidonic Acids12Coordination Polymers and Frameworks in Uranyl Ion Complexes with Sulfonates and Cucurbit[6]uril32Polymeric Structure of Oxalato-Bridged Complexes of Tetravalent Actinides Th, U, Np and Pu44Synthesis, Structure, and Characterization of an Organic Compound Based on 3-Nitrobenzoic Acid Moiety3Investigation of in Situ Oxalate Formation from 2,3-Pyrazinedicarboxylate under Hydrothermal Conditions Using Nuclear Magnetic Resonance Spectroscopy59In situ synthesis of an inorganic–organic hybrid based on a molybdenum-oxo chain: [Cu2(pz)(Mo3O10)] n6pH Dependent structural diversity of lead compounds based on new flexible ligand [3-(2-pyridyl)-1-pyrazolyl] acetic acid18Single Crystal Synthesis Methods Dedicated to Structural Investigations of Very Low Solubility Mixed-Actinide Oxalate Coordination Polymers192.13 Product Class 13: Organometallic Complexes of the Actinides2Uranyl–copper(ii) heterometallic oxalate complexes: coordination polymers and frameworks47Crystal Growth and First Crystallographic Characterization of Mixed Uranium(IV)–Plutonium(III) Oxalates512,2′‐Bipyridine and 1,10‐Phenanthroline as Coligands or Structure‐Directing Agents in Uranyl–Organic Assemblies with Polycarboxylic Acids56Actinide oxalates, solid state structures and applications160Isolation of thorium benzoate polytypes with discrete ThO8 square antiprismatic units involved in chain-like assemblies16Spectroscopic Studies and Crystal Structures of Double Thorium(IV) Oxalates with Sodium Ions15Molecular and Polymeric Uranyl and Thorium Complexes with Sulfonate‐Containing Ligands33Increasing Complexity in the Uranyl Ion–Kemp’s Triacid System: From One- and Two-Dimensional Polymers to Uranyl–Copper(II) Dodeca- and Hexadecanuclear Species47Construction of 0D to 3D Copper(II) MOFs based on heterocyclic carboxylic acid: Synthesis, structures, cyclic voltammograms, and luminescent properties8Impurity characterization and thermal decomposition mechanism of ammonium diuranate during in-situ synthesis of U3O8 using simultaneous TG–DTA–FTIR and PXRD measurements15A Tridentate In Situ Generated Ligand Leading the Self-Assembly of a Transition Metal Coordination Polymer: Solvothermal Synthesis and Structural Characterization of 1D Cadmium Pyridine-2-Carboxylate2Mixed sandwich thorium complexes incorporating bis(tri-isopropylsilyl)cyclooctatetraenyl and pentamethylcyclopentadienyl ligands: synthesis, structure and reactivity37Synthesis, spectroscopic characterization and crystal structures of thorium(IV) mononuclear lactato and hexanuclear formato complexes19Metal Oxygen Connectivities in Cu(II) Complexes of Meso-2,3-dibromosuccinic Acid (H2DBrS): [Cu3(H2O)2(μ 3–OH)2(μ 2–OAc)2(DBrS)]⋅4H2O 1 and [Cu3(H2O)4(DBrS)2](DBrSM)⋅4H2O 21Thorium Terephthalates Coordination Polymers Synthesized in Solvothermal DMF/H2O System143Low temperature decomposition of U(IV) and Th(IV) oxalates to nanograined oxide powders81Crystal growth methods dedicated to low solubility actinide oxalates18Structural Variations in the Uranyl/4,4′-Biphenyldicarboxylate System. Rare Examples of 2D → 3D Polycatenated Uranyl–Organic Networks78Surprising coordination for low-valent actinides resembling uranyl( vi ) in thorium( iv ) organic hybrid layered and framework structures based on a graphene-like (6,3) sheet topology34Synthesis and Crystal Structure Characterization of Thorium Trimesate Coordination Polymers34A tetranuclear copper (II) complex with pyrazole-3,5-dicarboxylate ligands: synthesis, characterization and electrochemical properties23RE-p-halobenzoic acid–terpyridine complexes, Part II: structural diversity, supramolecular assembly, and luminescence properties in a series of p-bromobenzoic acid rare-earth hybrid materials22RE-p-halobenzoic acid–terpyridine complexes, part III: structural and supramolecular trends in a series of p-iodobenzoic acid rare-earth hybrid materials29Synthesis of Coordination Polymers of Tetravalent Actinides (Uranium and Neptunium) with a Phthalate or Mellitate Ligand in an Aqueous Medium34Uranyl Complexes as Scaffolding or Spacers for Cucurbit[6]uril Molecules in Homo‐ and Heterometallic Species, Including a Uranyl–Lanthanide Complex13Network Dimensionality of Selected Uranyl(VI) Coordination Polymers and Octopus-like Uranium(IV) Clusters16Stress compensation in an extended series of lanthanide 2-sulfonatoterephthalates [Ln(TPSO3)(H2O)2]n (Ln = Ce − Lu, except Pm)11Conversion of lanthanide glutarate chlorides with interstitial THF into lanthanide glutarates with unprecedented topologies5Synthèse et étude cristallochimique de carboxylates d'actinides tétravalents (Th, U, Np) : polymères de coordination et entités moléculaires à haute nucléarité0Molecular and polymeric uranyl and thorium hybrid materials featuring methyl substituted pyrazole dicarboxylates and heterocyclic 1,3-diketones11One ligand capable of in situ reaction in a mixed-ligand system with two new different frameworks1Time-controlled synthesis of the 3D coordination polymer U(1,2,3-Hbtc) 2 followed by the formation of molecular poly-oxo cluster {U 14 } containing hemimellitate uranium( iv )14Thermal and spectroscopic study of zinc, manganese, copper, cobalt and nickel 2,3-pyrazinedicarboxylate9Metal‐Carboxyl Helical Chain Secondary Units Supported Ion‐Exchangeable Anionic Uranyl–Organic Framework15Copper and Ruthenium Pyridyltriazole Complexes and Their Reactivity Toward Carbon Dioxide and Water0From Isolated Molecular Complexes to Extended Networks: Synthesis and Characterization of Thorium Furanmono‐ and Dicarboxylates2Insights into the thermal decomposition of plutonium(IV) oxalate – a DFT study of the intermediate structures16An updated status and trends in actinide metal-organic frameworks (An-MOFs): From synthesis to application145Enhanced Xe/Kr separation via the pore size confinement effect of a microporous thorium-based metal–organic framework9Leveraging Nitrogen Linkages in the Formation of a Porous Thorium–Organic Nanotube Suitable for Iodine Capture24Structural and Bonding Analysis in Monomeric Actinide(IV) Oxalate from Th(IV) to Pu(IV): Comparison with the An(IV) Nitrate Series19Insight into the Structural Ambiguity of Actinide(IV) Oxalate Sheet Structures: A Case for Alternate Coordination Geometries**6Mining for Metal–Organic Systems: Chemistry Frontiers of Th-, U-, and Zr-Materials18Rational design of a rare N-coordinated thorium organic framework for efficient CO2 capture and catalytic conversion2

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  1. The first uranyl–lanthanide heterometallic complexes: metal–organic frameworks with DOTA and oxalato ligands

    CrystEngComm · 2008-01-01

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  2. Syntheses, crystal structures and photoluminescence of two new pyrazinecarboxylate-based cadmium(II) coordination polymers

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    Lan-Fen Chen, Zhaoji Li, Ye‐Yan Qin, Jian‐Kai Cheng, Yuan‐Gen Yao

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  3. Thorium(IV) Coordination Polymers in the Pyridine and Pyrazinedicarboxylic Acid Systems

    Crystal Growth & Design · 2008-06-21

    M. Frisch, Christopher L. Cahill

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  4. In Situ Synthesis of Tetradentate Dye for Construction of Three-Dimensional Homochiral Phosphor

    Chemistry of Materials · 2008-08-15

    Jian Zhang, Tao Wu, Pingyun Feng, Xianhui Bu

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  5. New Examples of Metal Coordination Architectures of 3,3′,4,4′‐Biphenyltetracarboxylic Acid – Syntheses, Crystal Structures, and Physical Properties

    Zeitschrift für anorganische und allgemeine Chemie · 2008-12-30

    Guang‐Xiang Liu, Kun Zhu, Hong Chen, Rong‐Yi Huang, Xiaoming Ren

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  6. Structural variability in uranyl–lanthanide heterometallic complexes with DOTA and oxalato ligands

    CrystEngComm · 2009-01-01

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  7. Hydrothermal in situ ligand reaction: copper(II)-mediated stepwise oxidation of 2,3,5- and 2,4,6-trimethylpyridine to pyridinecarboxylates

    CrystEngComm · 2009-09-15

    Cui‐Jin Li, Zhuojia Lin, Yun Bo Lei, Yuling Xie, Ji‐Dong Leng, Yong‐Cong Ou, Ming‐Liang Tong

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  8. Uranyl Ion Complexation by Cucurbiturils in the Presence of Perrhenic, Phosphoric, or Polycarboxylic Acids. Novel Mixed-Ligand Uranyl−Organic Frameworks

    Crystal Growth & Design · 2009-11-19

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  9. Hydrothermal Synthesis and Crystal Structures of Cd(II)-Based 1D Coordination Polymer and Mn(II) Coordination Complex with Mixed N- and O-donor Ligands: [Cd2(4-4′-bpy)2(pa)4] n ·0.25(H2O) and [Mn(4-4′-bpy)2(pa)(H2O)3]ClO4·2(H2O)

    Journal of Inorganic and Organometallic Polymers and Materials · 2009-12-01

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  10. Uranyl–organic assemblies with the macrocyclic ligand 1,4,8,11-tetraazacyclotetradecane-1,4,8,11-tetraacetate (TETA)

    CrystEngComm · 2010-01-01

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  11. X-Ray Diffraction and μ-Raman Investigation of the Monoclinic-Orthorhombic Phase Transition in Th1−xUx(C2O4)2·2H2O Solid Solutions

    Inorganic Chemistry · 2010-01-22

    Nicolas Clavier, N. Hingant, Murielle Rivenet, S. Obbade, Nicolas Dacheux, Nicole Barré, F. Abraham

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  12. Crystal structure of diaqua-bis(hydrogen 2-propyl-1H-imidazole-4,5-dicarboxylato)calcium(II), Ca(H2O)2(C8H9N2O4)2

    Zeitschrift für Kristallographie - New Crystal Structures · 2010-03-01

    Xun Feng, Shaobin Miao, Rongfang Li, Xin-Ge Shi, Liya Wang

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  13. Crystal structure of triaqua-(pyrazine-2,3-dicarboxylato)cerium(III), Ce(H2O)3(C6H2N2O4)

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    Xun Feng, Jian-She Zhao, Xin-Ge Shi, Fang Ruan, Li‐Ya Wang

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  14. Crystal chemistry of thorium nitrates and chromates

    Journal of Solid State Chemistry · 2010-05-06

    Ginger E. Sigmon, Peter Carman Burns

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  15. Crystal structure of hexaaqua-bis(pyridine-2,6-dicarboxylato)-oxalatodiytterbium( III) pentahydrate, Yb2(H2O)6(C7H3NO4)2(C2O4) · 5H2O

    Zeitschrift für Kristallographie - New Crystal Structures · 2010-06-01

    Xun Feng, Xin-Ge Shi, Qian Yao Sun, Wen-Wei Zhu

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  16. Hydrothermal Synthesis of Uranyl Squarates and Squarate-Oxalates: Hydrolysis Trends and in Situ Oxalate Formation

    Inorganic Chemistry · 2010-06-16

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  17. catena-Poly[thorium(IV)-tetrakis(μ2-3-carboxyadamantane-1-carboxylato)]: a quadruple helical strand driven by a synergy of coordination and hydrogen bonding

    Acta Crystallographica Section C Crystal Structure Communications · 2010-09-03

    Olga M. Nazarenko, Julia A. Rusanova, Harald Krautscheid, K.V. Domasevitch

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  18. Uranyl triazolate formation via an in situ Huisgen 1,3-dipolar cycloaddition reaction

    CrystEngComm · 2010-09-06

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  19. Refinement of the crystal structure of triaqua(2,3-pyrazinedi-carboxylato) cadmium(II), Cd(H2O)3(C6H2N2O4), a correction to the article “Crystal structure of triaqua(2,3-pyrazinedicarboxylato)-cerium(III), Ce(H2O)3(C6H2N2O4)”, Z. Kristallogr. NCS 225 (2010) 71-73

    Zeitschrift für Kristallographie - New Crystal Structures · 2010-12-01

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  20. In situ oxalate formation during hydrothermal synthesis of uranyl hybrid materials

    CrystEngComm · 2011-01-01

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  21. Oxalate Bridged Copper Pyrazole Complex Templated Anderson-Evans Cluster Based Solids

    Australian Journal of Chemistry · 2011-01-13

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  22. Solid State Structure of Thorium(IV) Complexes with Common Aminopolycarboxylate Ligands

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  23. Controlling Disulfide Bond Formation and Crystal Growth from 2-Mercaptobenzoic Acid

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  24. Uranyl Ion Complexation by Aliphatic Dicarboxylic Acids in the Presence of Cucurbiturils as Additional Ligands or Structure-Directing Agents

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  25. Uranyl–Alkali Metal Ion Heterometallic Complexes with Cucurbit[6]uril and a Sulfonated Catechol

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  26. New Metal–Organic Framework Solids Built from Barium and Isoelectronic Chelidamic and Chelidonic Acids

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  27. Coordination Polymers and Frameworks in Uranyl Ion Complexes with Sulfonates and Cucurbit[6]uril

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  28. Polymeric Structure of Oxalato-Bridged Complexes of Tetravalent Actinides Th, U, Np and Pu

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  29. Synthesis, Structure, and Characterization of an Organic Compound Based on 3-Nitrobenzoic Acid Moiety

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  30. Investigation of in Situ Oxalate Formation from 2,3-Pyrazinedicarboxylate under Hydrothermal Conditions Using Nuclear Magnetic Resonance Spectroscopy

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  31. In situ synthesis of an inorganic–organic hybrid based on a molybdenum-oxo chain: [Cu2(pz)(Mo3O10)] n

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  32. pH Dependent structural diversity of lead compounds based on new flexible ligand [3-(2-pyridyl)-1-pyrazolyl] acetic acid

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    Qiao‐Yun Li, Ming‐Hua He, Zhen-Dong Shen, Gao‐Wen Yang, Zhi-Yong Yuan

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  33. Single Crystal Synthesis Methods Dedicated to Structural Investigations of Very Low Solubility Mixed-Actinide Oxalate Coordination Polymers

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  34. 2.13 Product Class 13: Organometallic Complexes of the Actinides

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  35. Uranyl–copper(ii) heterometallic oxalate complexes: coordination polymers and frameworks

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  36. Crystal Growth and First Crystallographic Characterization of Mixed Uranium(IV)–Plutonium(III) Oxalates

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  37. 2,2′‐Bipyridine and 1,10‐Phenanthroline as Coligands or Structure‐Directing Agents in Uranyl–Organic Assemblies with Polycarboxylic Acids

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  38. Actinide oxalates, solid state structures and applications

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    F. Abraham, Bénédicte Arab-Chapelet, Murielle Rivenet, Christelle Tamain, S. Grandjean

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  39. Isolation of thorium benzoate polytypes with discrete ThO8 square antiprismatic units involved in chain-like assemblies

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  40. Spectroscopic Studies and Crystal Structures of Double Thorium(IV) Oxalates with Sodium Ions

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  41. Molecular and Polymeric Uranyl and Thorium Complexes with Sulfonate‐Containing Ligands

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  42. Increasing Complexity in the Uranyl Ion–Kemp’s Triacid System: From One- and Two-Dimensional Polymers to Uranyl–Copper(II) Dodeca- and Hexadecanuclear Species

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  43. Construction of 0D to 3D Copper(II) MOFs based on heterocyclic carboxylic acid: Synthesis, structures, cyclic voltammograms, and luminescent properties

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  44. Impurity characterization and thermal decomposition mechanism of ammonium diuranate during in-situ synthesis of U3O8 using simultaneous TG–DTA–FTIR and PXRD measurements

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  45. A Tridentate In Situ Generated Ligand Leading the Self-Assembly of a Transition Metal Coordination Polymer: Solvothermal Synthesis and Structural Characterization of 1D Cadmium Pyridine-2-Carboxylate

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  46. Mixed sandwich thorium complexes incorporating bis(tri-isopropylsilyl)cyclooctatetraenyl and pentamethylcyclopentadienyl ligands: synthesis, structure and reactivity

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  47. Synthesis, spectroscopic characterization and crystal structures of thorium(IV) mononuclear lactato and hexanuclear formato complexes

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  48. Metal Oxygen Connectivities in Cu(II) Complexes of Meso-2,3-dibromosuccinic Acid (H2DBrS): [Cu3(H2O)2(μ 3–OH)2(μ 2–OAc)2(DBrS)]⋅4H2O 1 and [Cu3(H2O)4(DBrS)2](DBrSM)⋅4H2O 2

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  49. Thorium Terephthalates Coordination Polymers Synthesized in Solvothermal DMF/H2O System

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  50. Low temperature decomposition of U(IV) and Th(IV) oxalates to nanograined oxide powders

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