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RESEARCH PAPER · Journal of the American Ceramic Society · 2010

In Situ Time‐Resolved X‐Ray Diffraction of Tobermorite Formation Process Under Autoclave Condition

Jun Kikuma, Masamichi Tsunashima, Tetsuji Ishikawa, Shinya Matsuno, Akihiro Ogawa, Kunio Matsui, Masugu Sato

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In Situ Time‐Resolved X‐Ray Diffraction of Tobermorite Formation Process Under Autoclave ConditionOriginalDevelopment of an in situ X-ray Diffraction System for Hydrothermal Reaction0Influence of addition of AI compound and gypsum on tobermorite formation in autoclaved aerated concrete studied by in situ X-ray diffraction4Use of fine particle quartz sand for AAC production: model study by in situ X-ray diffraction and NMR1In situ time-resolved X-ray diffraction of tobermorite formation in autoclaved aerated concrete: Influence of silica source reactivity and Al addition173In situtime-resolved X-ray diffraction of tobermorite synthesis process under hydrothermal condition5Recent advances in the field of cement hydration and microstructure analysis210In situ time-resolved X-ray diffraction of tobermorite formation process under hydrothermal condition: Influence of reactive al compound7Effects of quartz particle size and water-to-solid ratio on hydrothermal synthesis of tobermorite studied by in-situ time-resolved X-ray diffraction51Preparation of Needle-Shaped Crystals on the Surface of Slag Compact to Control Its Light Absorption Properties3The Oxford-Diamond In Situ Cell for studying chemical reactions using time-resolved X-ray diffraction45IN SITU XRD AND 29Si SOLID-STATE NMR ANALYSIS ON TOBERMORITE FORMATION：EFFECT OF THE C-S-H STRUCTURE IN CaO-SiO2-H2O SYSTEM1IN SITU XRD AND SOLID-STATE NMR ANALYSIS ON TOBERMORITE FORMATION：EFFECT OF γ-Al2O3 AND GYPSUM ADDITION5Material and Elastic Properties of Al ‐Tobermorite in Ancient Roman Seawater Concrete138Atom‐Efficient Route for Converting Incineration Ashes into Heavy Metal Sorbents23ANALYSIS OF CALCIUM-SILICATE-HYDRATES ON THE TOBERMORITE FORMATION PROCESS BY ULTRA SMALL-ANGLE X-RAY SCATTERING4Slump flow of autoclaved aerated concrete slurries3ANALYSIS OF CALCIUM-SILICATE-HYDRATES ON THE TOBERMORITE FORMATION PROCESS BY ULTRA SMALL-ANGLE X-RAY SCATTERING：EFFECTS OF γ-Al2O3 AND GYPSUM ADDITION2Pre-reaction temperature effect on C–S–H colloidal properties and xonotlite formation via steam assisted crystallization21Preparation and characterization of whisker-reinforced ceramics from coal fly ash52Seed-Assisted Hydrothermal Treatment with Composite Silicon–Aluminum Additive for Solidification of Heavy Metals in Municipal Solid Waste Incineration Fly Ash39Influence of addition of calcium sulfate dihydrate on drying of autoclaved aerated concrete8Alkali-reinforced hydrothermal synthesis of lathy tobermorite fibers using mixture of coal fly ash and lime68THE HYDROTHERMAL SYNTHESIS OF 1.13 nm TOBERMORITE FROM GRANITE SAWING POWDER WASTE9In situ monitoring of hydrothermal reactions by X-ray diffraction with Bragg–Brentano geometry2Microstructure and properties of fly ash/cement-based pastes activated with MgO and CaO under hydrothermal conditions60Influence of foreign ions on calcium silicate hydrate under hydrothermal conditions: A review51Determining the disordered nanostructure of calcium silicate hydrate (C‐S‐H) from broad X‐ray diffractograms16Insight into the local C-S-H structure and its evolution mechanism controlled by curing regime and Ca/Si ratio143Synthesis of High Crystallinity 1.13 nm Tobermorite and Xonotlite from Natural Rocks, Their Properties and Application for Heat-Resistant Products20Solubility and characterization of synthesized 11 Å Al-tobermorite92Hydrophobicity/Oleophilicity of Autoclaved Aerated Concrete (AAC) Grains Coated with Oleic and Stearic Acids for Application as Oil/Water Separating Filtration and Adsorbent Materials in Vietnam5Understanding the effect of sulfate ions on the hydrothermal curing of autoclaved aerated concrete28Carbonation of photocatalytic aluminosilicate cement composites: Evolution of self-cleaning and radiative cooling properties14Effect of waste glass powder on quartz sand autoclaved material: strength, hydration products and microstructure6The Usability of Metallurgical Production Waste as a Siliceous Component in Autoclaved Aerated Concrete Technology1Kinetic Investigation of Tobermorite Synthesis for the Recovery of Carcinogenic Respirable Crystalline Silica (RCS)2Mechanisms of acid modified magnesium slag as a calcium source in regulating slurry behavior, pore structure, and tobermorite formation in fly ash-based autoclaved aerated concrete0

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  1. Development of an in situ X-ray Diffraction System for Hydrothermal Reaction

    BUNSEKI KAGAKU · 2011-01-01

    Jun Kikuma, Shinya Matsuno

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  2. Influence of addition of AI compound and gypsum on tobermorite formation in autoclaved aerated concrete studied by in situ X-ray diffraction

    Cement Wapno Beton · 2011-01-01

    Koshi Matsui, A. Ogawa, Jun Kikuma, Masamichi Tsunashima, Takehiko Ishikawa, S. Matsuno

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  3. Use of fine particle quartz sand for AAC production: model study by in situ X-ray diffraction and NMR

    Cement Wapno Beton · 2011-01-01

    Jun Kikuma, Masamichi Tsunashima, Takehiko Ishikawa, S. Matsuno, A. Ogawa, Koshi Matsui

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  4. In situ time-resolved X-ray diffraction of tobermorite formation in autoclaved aerated concrete: Influence of silica source reactivity and Al addition

    Cement and Concrete Research · 2011-02-26

    Kunio Matsui, Jun Kikuma, Masamichi Tsunashima, Tetsuji Ishikawa, Shinya Matsuno, Akihiro Ogawa, Masugu Sato

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  5. In situtime-resolved X-ray diffraction of tobermorite synthesis process under hydrothermal condition

    IOP Conference Series Materials Science and Engineering · 2011-03-01

    Jun Kikuma, Masamichi Tsunashima, Takehiko Ishikawa, S. Matsuno, Ami Ogawa, K Matsui, M. Sato

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  6. Recent advances in the field of cement hydration and microstructure analysis

    Cement and Concrete Research · 2011-05-07

    Jochen Stark

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  7. In situ time-resolved X-ray diffraction of tobermorite formation process under hydrothermal condition: Influence of reactive al compound

    Powder Diffraction · 2011-06-01

    K. Matsui, Ami Ogawa, Jun Kikuma, Masamichi Tsunashima, Takehiko Ishikawa, S. Matsuno

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  8. Effects of quartz particle size and water-to-solid ratio on hydrothermal synthesis of tobermorite studied by in-situ time-resolved X-ray diffraction

    Journal of Solid State Chemistry · 2011-06-25

    Jun Kikuma, Masamichi Tsunashima, T. Ishikawa, S. Matsuno, A. Ogawa, K. Matsui, M. Sato

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  9. Preparation of Needle-Shaped Crystals on the Surface of Slag Compact to Control Its Light Absorption Properties

    Journal of the Japan Institute of Metals and Materials · 2012-01-01

    Toshifumi Yamamoto, Yohei Katayama, Masanori Suzuki, Shigeru Katsuyama, Toshihiro Tanaka

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  10. The Oxford-Diamond In Situ Cell for studying chemical reactions using time-resolved X-ray diffraction

    Review of Scientific Instruments · 2012-08-01

    Saul J. Moorhouse, Nenad Vranješ, Andrew C. Jupe, Michael Drakopoulos, Dermot M. O'Hare

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  11. IN SITU XRD AND 29Si SOLID-STATE NMR ANALYSIS ON TOBERMORITE FORMATION：EFFECT OF THE C-S-H STRUCTURE IN CaO-SiO2-H2O SYSTEM

    Cement Science and Concrete Technology · 2013-01-01

    Akihiro OGAWA, Kunio Matsui, Shinya Matsuno, Mie NAYUKI

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  12. IN SITU XRD AND SOLID-STATE NMR ANALYSIS ON TOBERMORITE FORMATION：EFFECT OF γ-Al2O3 AND GYPSUM ADDITION

    Cement Science and Concrete Technology · 2013-01-01

    Kunio Matsui, Akihiro OGAWA, Shinya Matsuno, Mie NAYUKI

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  13. Material and Elastic Properties of Al ‐Tobermorite in Ancient Roman Seawater Concrete

    Journal of the American Ceramic Society · 2013-05-28

    Marie D. Jackson, Juhyuk Moon, Emanuele Gotti, Rae Taylor, Sejung Rosie Chae, Martin Kunz, Abdul-Hamid M. Emwas, Çağla Meral Akgül, Peter Guttmann, Pierre Levitz, H. R. Wenk, Paulo J.M. Monteiro

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  14. Atom‐Efficient Route for Converting Incineration Ashes into Heavy Metal Sorbents

    ChemSusChem · 2013-12-12

    Yi Wai Chiang, Rafael M. Santos, Kenneth Vanduyfhuys, Boudewijn D. Meesschaert, Johan A. Martens

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  15. ANALYSIS OF CALCIUM-SILICATE-HYDRATES ON THE TOBERMORITE FORMATION PROCESS BY ULTRA SMALL-ANGLE X-RAY SCATTERING

    Cement Science and Concrete Technology · 2014-01-01

    Kunio Matsui, Naoki Sakamoto, Jiro WATANABE, Shinya Matsuno

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  16. Slump flow of autoclaved aerated concrete slurries

    TU/e Research Portal · 2014-01-01

    Chris Chris Straub, G George Quercia, M.V.A. Florea, H.J.H. Brouwers

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  17. ANALYSIS OF CALCIUM-SILICATE-HYDRATES ON THE TOBERMORITE FORMATION PROCESS BY ULTRA SMALL-ANGLE X-RAY SCATTERING：EFFECTS OF γ-Al2O3 AND GYPSUM ADDITION

    Cement Science and Concrete Technology · 2015-01-01

    Kunio Matsui, Naoki Sakamoto, Jiro WATANABE, Shinya Matsuno

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  18. Pre-reaction temperature effect on C–S–H colloidal properties and xonotlite formation via steam assisted crystallization

    Materials and Structures · 2015-01-31

    Hsing‐I Hsiang, Wei‐Sheng Chen, Wei-Chao Huang

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  19. Preparation and characterization of whisker-reinforced ceramics from coal fly ash

    Ceramics International · 2016-10-10

    Yang Luo, Shuhua Ma, Zhenqing Zhao, Zehua Wang, Shili Zheng, Xiaohui Wang

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  20. Seed-Assisted Hydrothermal Treatment with Composite Silicon–Aluminum Additive for Solidification of Heavy Metals in Municipal Solid Waste Incineration Fly Ash

    Energy & Fuels · 2016-10-31

    Dezhi Shi, Chao Zhang, Jinlu Zhang, Pengfei Li, Yunmei Wei

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  21. Influence of addition of calcium sulfate dihydrate on drying of autoclaved aerated concrete

    Open Engineering · 2017-11-04

    Dorota Małaszkiewicz, Jacek Chojnowski

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  22. Alkali-reinforced hydrothermal synthesis of lathy tobermorite fibers using mixture of coal fly ash and lime

    Construction and Building Materials · 2019-12-09

    Pengxu Cao, Guanghui Li, Jun Luo, Mingjun Rao, Hao Jiang, Zhiwei Peng, Tao Jiang

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  23. THE HYDROTHERMAL SYNTHESIS OF 1.13 nm TOBERMORITE FROM GRANITE SAWING POWDER WASTE

    Ceramics - Silikaty · 2020-02-18

    G. Smalakys

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  24. In situ monitoring of hydrothermal reactions by X-ray diffraction with Bragg–Brentano geometry

    Journal of Applied Crystallography · 2020-06-18

    Karsten Mesecke, Winfried Malorny, Laurence Noel Warr

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  25. Microstructure and properties of fly ash/cement-based pastes activated with MgO and CaO under hydrothermal conditions

    Cement and Concrete Composites · 2020-07-26

    Zhiguang Zhao, Xiaoling Qu, Jinhe Li

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  26. Influence of foreign ions on calcium silicate hydrate under hydrothermal conditions: A review

    Construction and Building Materials · 2021-07-02

    Hongwei Tian, Dietmar A. Stephan, Barbara Lothenbach, C.W. Lehmann

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  27. Determining the disordered nanostructure of calcium silicate hydrate (C‐S‐H) from broad X‐ray diffractograms

    Journal of the American Ceramic Society · 2021-09-16

    Felipe Basquiroto de Souza, Kwesi Sagoe‐Crentsil, Wenhui Duan

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  28. Insight into the local C-S-H structure and its evolution mechanism controlled by curing regime and Ca/Si ratio

    Construction and Building Materials · 2022-04-09

    Zhongping Wang, Yuting Chen, Linglin Xu, Zheyu Zhu, Yue Bo Zhou, Pan Feng, Kai Wu

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  29. Synthesis of High Crystallinity 1.13 nm Tobermorite and Xonotlite from Natural Rocks, Their Properties and Application for Heat-Resistant Products

    Materials · 2022-05-12

    Raimundas Šiaučiūnas, G. Smalakys, Anatolijus Eisinas, Edita Prichockiene

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  30. Solubility and characterization of synthesized 11 Å Al-tobermorite

    Cement and Concrete Research · 2022-06-16

    Barbara Lothenbach, Daniel C. Jansen, Yiru Yan, Juergen Schreiner

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  31. Hydrophobicity/Oleophilicity of Autoclaved Aerated Concrete (AAC) Grains Coated with Oleic and Stearic Acids for Application as Oil/Water Separating Filtration and Adsorbent Materials in Vietnam

    Environments · 2022-08-10

    Akihiro Matsuno, Ken Kawamoto

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  32. Understanding the effect of sulfate ions on the hydrothermal curing of autoclaved aerated concrete

    Cement and Concrete Research · 2022-12-02

    Karsten Mesecke, Winfried Malorny, Laurence Noel Warr

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  33. Carbonation of photocatalytic aluminosilicate cement composites: Evolution of self-cleaning and radiative cooling properties

    Cement and Concrete Composites · 2024-06-12

    Daoru Liu, J.C.O. Zepper, Yuxuan Chen, Lulu Cheng, Qingliang Yu

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  34. Effect of waste glass powder on quartz sand autoclaved material: strength, hydration products and microstructure

    Materials and Structures · 2024-08-13

    Yaomin Gao, Jiwei Cai, Gelong Xu, Qing Tian, Weiguo Shen, Ruixue Liu, Jiaqi Zhang

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  35. The Usability of Metallurgical Production Waste as a Siliceous Component in Autoclaved Aerated Concrete Technology

    Buildings · 2024-10-03

    Lenka Mészárosová, Vít Černý, Jindřich Melichar, Pavlína Ondříčková, Rostislav Drochytka

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  36. Kinetic Investigation of Tobermorite Synthesis for the Recovery of Carcinogenic Respirable Crystalline Silica (RCS)

    ACS Omega · 2025-10-23

    Daniele Malferrari, Giulio Galamini, Maddalena Bernini, Riccardo Fantini, Giulia Malvolti, Alessandro Francesco Gualtieri

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  37. Mechanisms of acid modified magnesium slag as a calcium source in regulating slurry behavior, pore structure, and tobermorite formation in fly ash-based autoclaved aerated concrete

    Construction and Building Materials · 2026-09-15

    Qing Zhao, Tingshu He, Yongqi Da, Chen Shi, Zeyin He, Yuliang Ke, Hang Wen, Jinliang Guo

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