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RESEARCH PAPER · Inorganic Chemistry · 2009

Use of Hydrazine in the Hydrothermal Synthesis of Chalcogenides: the Neutral Framework Material [Mn 2 SnS 4 (N 2 H 4 ) 2 ]

Manolis J. Manos, Mercouri G. Kanatzidis

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Use of Hydrazine in the Hydrothermal Synthesis of Chalcogenides: the Neutral Framework Material [Mn 2 SnS 4 (N 2 H 4 ) 2 ]OriginalChemInform Abstract: Use of Hydrazine in the Hydrothermal Synthesis of Chalcogenides: The Neutral Framework Material [Mn2SnS4(N2H4)2].0Small organic molecule templating synthesis of organic–inorganic hybrid materials: their nanostructures and properties101Stabilization of (SnS4)4− anion by coordinating to [TM(π-conjugated-ligand)m]n+ complex: a chain-like thiostannate(iv) {[Mn(phen)]2(SnS4)}n·nH2O exhibiting an unprecedented link mode of the (SnS4)4− anion30Solid state coordination chemistry of polyoxomolybdate clusters: Hydrothermal synthesis and structures of [ { Cu 3 II ( 4 -pt ) 2 ( 4 -Hpt ) 2 ( H 2 O ) 2 } { Mo 8 O 26 } ] · 2 H 2 O and [ { Cu 10 I ( 4 -pt )34Hydrazine-cadmium tellurite hybrid microcrystals: An efficient precursor to porous cadmium telluride and tellurium architectures through its thermal decomposition9Semiconductor Nanocrystals Functionalized with Antimony Telluride Zintl Ions for Nanostructured Thermoelectrics156Five dimeric thiogermanates with transition metal complexes of multidentate chelating amines: Syntheses, structures, magnetism and photoluminescence41Hydrazine-hydrothermal method to synthesize three-dimensional chalcogenide framework for photocatalytic hydrogen generation132A new hydrazine-bridged thioantimonate Mn2Sb4S8(N2H4)2: Synthesis, structure, optical and magnetic properties43Layered Hydrazinium Titanate: Advanced Reductive Adsorbent and Chemical Toolkit for Design of Titanium Dioxide Nanomaterials34Synthesis and photosensitivity of SnS nanobelts44Structural Diversity, Optical and Magnetic Properties of a Series of Manganese Thioarsenates with 1,10-Phenanthroline or 2,2′-Bipyridine Ligands: Using Monodentate Methylamine as an Alkalinity Regulator47Synthesis and characterization of (H2dab)2Cu8Ge4S14·2H2O: An expanded framework based on icosahedral Cu8S12 cluster24Electronic structure and solution behavior of a tris(N,N′-diphenylhydrazido)manganese(iv) propeller complex6Reaction pathways for the formation of Cu2ZnSn(Se,S)4 absorber materials from liquid-phase hydrazine-based precursor inks60The First Tetradentate μ‐1κ2:2κ2‐Sn2Se6 Ligand to a Lanthanide(III) Center: Solvothermal Syntheses and Characterizations of Lanthanide Selenidostannate Polymers with Tetraethylenepentamine as a Second Ligand13A new synthetic approach to force bond formation between a transition metal complex and a thiostannate anion: solvothermal synthesis and crystal structure of [Co2(cyclam)2Sn2S6]·2H2O24Nanostructured Inorganic–Organic Hybrid Semiconductor Materials3Complexation of Sn2Se6 with lanthanide(III) centers influenced by ethylene polyamines: Solvothermal syntheses, crystal structures, and optical properties of lanthanide selenidostannates14Syntheses, crystal structures, and properties of two new one-dimensional heterometallic selenides: [DBNH]4[M3Sn4Se11(Se2)2] (M = Cd, Hg)14Surfactant–Thermal Method to Synthesize a Novel Two‐Dimensional Oxochalcogenide79New strategies to prepare crystalline chalcogenides165Novel thioarsenates {[Mn(2,2′-bipy) 2 (SCN)][Mn(2,2′-bipy)](As V S 4 )} 2 and {[Mn(2,2′-bipy) 2 (SCN)] 2 [As III 2 (S 2 ) 2 S 2 ]}: introducing an anionic second ligand to modify Mn II complex cations of 2,2′-bipyridine20Processing-Dependent Growth Mechanisms and Performance Improvement of Kesterite Solar Cells1New μ-SnTe4 and μ-Sn2Te6 ligands to transition metal: Solvothermal syntheses and characterizations of zinc tellurostannates containing polyamine ligands18Influence of the Synthesis Parameters onto Nucleation and Crystallization of Five New Tin–Sulfur Containing Compounds33Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials15Novel One-, Two-, and Three-Dimensional Selenidostannates Templated by Iron(II) Complex Cation23Surfactant-thermal method to prepare two novel two-dimensional Mn–Sb–S compounds for photocatalytic applications32Surfactant-Thermal Syntheses, Structures, and Magnetic Properties of Mn–Ge–Sulfides/Selenides45[Mn(dien) 2 ]MnSnS 4 , [Mn(1,2-dap)] 2 Sn 2 S 6 and [Mn(en) 2 ]MnGeS 4 : from 1D anionic and neutral chains to 3D neutral frameworks33Expanding the structural versatility of thiostannate( iv ) complexes15Soft template mediated synthesis of Bi–In–Zn–S and its efficient visible-light-driven decomposition of methylene blue10Hydrazine-Hydrothermal Synthesis and Characterization of the Two New Quaternary Thioantimonates(III) BaAgSbS3 and BaAgSbS3·H2O40Two Quaternary Copper Thiostannates with Lanthanum(III) Complexes13Unsaturated Mn complex decorated hybrid thioarsenates: Syntheses, crystal structures and physical properties11Facile Hydrazine‐Hydrothermal Syntheses and Characterizations of Two Quaternary Thioarsenates(III): Two‐Dimensional SrAg4As2S6⋅2 H2O and One‐Dimensional BaAgAsS320Unprecedented 3D and 2D Frameworks of Manganese Thioarsenates Based on Heterometallic Cubic Cluster [Mn6(µ6‐S)(AsS3)4] and Covalent Linker N2H46A novel 2-D Mn selenidostannate( iv ) incorporating high-nuclear Mn clusters with spin canting behavior8Hydrazine-Assisted Syntheses and Properties of Mercury Tellurides Containing Transition-Metal Complexes20A series of new hybrid selenidostannates with metal complexes prepared in alkylol amines13Hydrazine-solvothermal methods to synthesize polymeric thioarsenates from one-dimensional chains to a three-dimensional framework8Complexations of Mn(II) with SbS4 and SbS3 ligands: Hydrazine-solvothermal syntheses, crystal structures and photocatalytic properties of manganese thioantimonates8Crystalline chalcogenidometalate-based compounds from uncommon reaction media12All-Inorganic Open-Framework Chalcogenides, A3Ga5S9·xH2O (A = Rb and Cs), Exhibiting Ultrafast Uranyl Remediation and Illustrating a Novel Post-Synthetic Preparation of Open-Framework Oxychalcogenides11A crystalline organic hybrid indium antimony sulfide for high performance lithium/sodium storage11Advances in Chalcogenide Crystal Growth: Flux and Solution Syntheses, and Approaches for Postsynthetic Modifications13Hydrazine-thermal syntheses, structures, and photocatalytic properties of tellurostannate hybrids with iron (II) complex unit2Ligand-functionalized and ligand-bridged or organyl-separated chalcogenido metalate-based clusters15Hydrazine-Assisted Synthesis, Structures, Photoelectricity, and Photocatalysis of Ternary Mercury–Tellurostannate Hybrids with Transition-Metal Complexes4Nickel-incorporated Cu2Te nanorods for enhanced charge storage in advanced supercapacitors2Transition Metal Chalcogenides: Perspectives on Their Applications for Nitrate Reduction0

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  1. ChemInform Abstract: Use of Hydrazine in the Hydrothermal Synthesis of Chalcogenides: The Neutral Framework Material [Mn2SnS4(N2H4)2].

    ChemInform · 2009-07-30

    Manolis J. Manos, Mercouri G. Kanatzidis

    Read original paper ↗ ·

  2. Small organic molecule templating synthesis of organic–inorganic hybrid materials: their nanostructures and properties

    Nanoscale · 2009-12-01

    Hong‐Bin Yao, Min‐Rui Gao, Shu‐Hong Yu

    Read original paper ↗ ·

  3. Stabilization of (SnS4)4− anion by coordinating to [TM(π-conjugated-ligand)m]n+ complex: a chain-like thiostannate(iv) {[Mn(phen)]2(SnS4)}n·nH2O exhibiting an unprecedented link mode of the (SnS4)4− anion

    CrystEngComm · 2010-01-01

    Guang‐Ning Liu, Guo‐Cong Guo, Feng Chen, Sheng‐Ping Guo, Xiao‐Ming Jiang, Chen Yang, Ming‐Sheng Wang, Mei‐Feng Wu, Jin‐Shun Huang

    Read original paper ↗ ·

  4. Solid state coordination chemistry of polyoxomolybdate clusters: Hydrothermal synthesis and structures of [ { Cu 3 II ( 4 -pt ) 2 ( 4 -Hpt ) 2 ( H 2 O ) 2 } { Mo 8 O 26 } ] · 2 H 2 O and [ { Cu 10 I ( 4 -pt )

    Inorganic Chemistry Communications · 2010-01-08

    Stephanie Jones, Hongxue Liu, Charles C. O’Connor, Jon A. Zubieta

    Read original paper ↗ ·

  5. Hydrazine-cadmium tellurite hybrid microcrystals: An efficient precursor to porous cadmium telluride and tellurium architectures through its thermal decomposition

    Nano Research · 2010-02-01

    Hong‐Bin Yao, Xiaobo Li, Si-Yuan Ai, Shu‐Hong Yu

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  6. Semiconductor Nanocrystals Functionalized with Antimony Telluride Zintl Ions for Nanostructured Thermoelectrics

    Journal of the American Chemical Society · 2010-04-27

    Maksym V. Kovalenko, Boris Spokoyny, Jong‐Soo Lee, Marcus Scheele, Andrew Weber, Susanthri C. Perera, Daniel B. Landry, Dmitri V. Talapin

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  7. Five dimeric thiogermanates with transition metal complexes of multidentate chelating amines: Syntheses, structures, magnetism and photoluminescence

    Journal of Molecular Structure · 2010-08-27

    Guang‐Ning Liu, Guo‐Cong Guo, Ming‐Sheng Wang, Li‐Zhen Cai, Jin‐Shun Huang

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  8. Hydrazine-hydrothermal method to synthesize three-dimensional chalcogenide framework for photocatalytic hydrogen generation

    Journal of Solid State Chemistry · 2010-09-18

    Yi Liu, Pushkar D. Kanhere, Chui Ling Wong, Yuefeng Tian, Yuhua Feng, Freddy Boey, Tom Wu, Hongyu Chen, Timothy John White, Zhong Chen, Qichun Zhang

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  9. A new hydrazine-bridged thioantimonate Mn2Sb4S8(N2H4)2: Synthesis, structure, optical and magnetic properties

    Inorganic Chemistry Communications · 2011-03-16

    Yi Liu, Yufeng Tian, Fengxia Wei, Michael Ser Chong Ping, Chuanwei Huang, Freddy Boey, Christian Kloc, Lang Chen, Tom Wu, Qichun Zhang

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  10. Layered Hydrazinium Titanate: Advanced Reductive Adsorbent and Chemical Toolkit for Design of Titanium Dioxide Nanomaterials

    Journal of the American Chemical Society · 2011-05-25

    Sergey N. Britvin, Andriy Lotnyk, Lorenz Kienle, Sergey V. Krivovichev, Wulf Depmeier

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  11. Synthesis and photosensitivity of SnS nanobelts

    Journal of Alloys and Compounds · 2011-10-15

    Hulin Zhang, Chenguo Hu, Xue Wang, Yi Xi, Xiaoyan Li

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  12. Structural Diversity, Optical and Magnetic Properties of a Series of Manganese Thioarsenates with 1,10-Phenanthroline or 2,2′-Bipyridine Ligands: Using Monodentate Methylamine as an Alkalinity Regulator

    Inorganic Chemistry · 2011-12-08

    Guang‐Ning Liu, Guo‐Cong Guo, Feng Chen, Shuai‐Hua Wang, Jing Zhi Sun, Jin‐Shun Huang

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  13. Synthesis and characterization of (H2dab)2Cu8Ge4S14·2H2O: An expanded framework based on icosahedral Cu8S12 cluster

    Journal of Solid State Chemistry · 2011-12-11

    Ren‐Chun Zhang, Chi Zhang, Shou‐Hua Ji, Min Ji, Yong‐Lin An

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  14. Electronic structure and solution behavior of a tris(N,N′-diphenylhydrazido)manganese(iv) propeller complex

    Dalton Transactions · 2012-01-01

    S.K. Kondaveeti, Shivaiah Vaddypally, Jeffrey D. McCall, Michael J. Zdilla

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  15. Reaction pathways for the formation of Cu2ZnSn(Se,S)4 absorber materials from liquid-phase hydrazine-based precursor inks

    Energy & Environmental Science · 2012-01-01

    Wan‐Ching Hsu, Brion Bob, Wenbing Yang, Choong‐Heui Chung, Yang Yang

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  16. The First Tetradentate μ‐1κ2:2κ2‐Sn2Se6 Ligand to a Lanthanide(III) Center: Solvothermal Syntheses and Characterizations of Lanthanide Selenidostannate Polymers with Tetraethylenepentamine as a Second Ligand

    European Journal of Inorganic Chemistry · 2012-09-12

    Weiwei Tang, Ruihong Chen, Wenqing Jiang, Yong Zhang, Dingxian Jia

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  17. A new synthetic approach to force bond formation between a transition metal complex and a thiostannate anion: solvothermal synthesis and crystal structure of [Co2(cyclam)2Sn2S6]·2H2O

    CrystEngComm · 2013-01-01

    Christoph Zeisler, Christian Näther, Wolfgang Bensch

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  18. Nanostructured Inorganic–Organic Hybrid Semiconductor Materials

    Elsevier eBooks · 2013-01-01

    Jing Li, R. Zhang

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  19. Complexation of Sn2Se6 with lanthanide(III) centers influenced by ethylene polyamines: Solvothermal syntheses, crystal structures, and optical properties of lanthanide selenidostannates

    Journal of Solid State Chemistry · 2013-05-24

    Chunying Tang, Fang Wang, Ruihong Chen, Wenqing Jiang, Yong Zhang, Dingxian Jia

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  20. Syntheses, crystal structures, and properties of two new one-dimensional heterometallic selenides: [DBNH]4[M3Sn4Se11(Se2)2] (M = Cd, Hg)

    Inorganic Chemistry Communications · 2013-07-31

    Wei‐Wei Xiong, Kaiqi Ye, Ling Ye, Qichun Zhang

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  21. Surfactant–Thermal Method to Synthesize a Novel Two‐Dimensional Oxochalcogenide

    Chemistry - An Asian Journal · 2013-10-15

    Junkuo Gao, Qiuling Tay, Pei‐Zhou Li, Wei‐Wei Xiong, Yanli Zhao, Zhong Chen, Qichun Zhang

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  22. New strategies to prepare crystalline chalcogenides

    Inorganic Chemistry Frontiers · 2014-01-01

    Wei‐Wei Xiong, Guodong Zhang, Qichun Zhang

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  23. Novel thioarsenates {[Mn(2,2′-bipy) 2 (SCN)][Mn(2,2′-bipy)](As V S 4 )} 2 and {[Mn(2,2′-bipy) 2 (SCN)] 2 [As III 2 (S 2 ) 2 S 2 ]}: introducing an anionic second ligand to modify Mn II complex cations of 2,2′-bipyridine

    Dalton Transactions · 2014-01-01

    Guang‐Ning Liu, Guo‐Cong Guo, Ming‐Sheng Wang, Jin‐Shun Huang

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  24. Processing-Dependent Growth Mechanisms and Performance Improvement of Kesterite Solar Cells

    eScholarship (California Digital Library) · 2014-01-01

    Wan‐Ching Hsu

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  25. New μ-SnTe4 and μ-Sn2Te6 ligands to transition metal: Solvothermal syntheses and characterizations of zinc tellurostannates containing polyamine ligands

    Journal of Solid State Chemistry · 2014-05-14

    Jialin Lu, Fang Wang, Yali Shen, Chunying Tang, Yong Zhang, Dingxian Jia

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  26. Influence of the Synthesis Parameters onto Nucleation and Crystallization of Five New Tin–Sulfur Containing Compounds

    Inorganic Chemistry · 2014-05-20

    Jessica Hilbert, Christian Näther, Wolfgang Bensch

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  27. Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials

    Inorganic Chemistry · 2014-06-25

    Justin N. Cross, Eric M. Villa, Victoria R. Darling, Matthew J. Polinski, Jian Hung Lin, Xiaoyan Tan, Naoki Kikugawa, Michael Shatruk, Ryan Baumbach, Thomas E. Albrecht‐Schmitt

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  28. Novel One-, Two-, and Three-Dimensional Selenidostannates Templated by Iron(II) Complex Cation

    Inorganic Chemistry · 2014-08-13

    Chunying Tang, Fang Wang, Jialin Lu, Dingxian Jia, Wenqing Jiang, Yong Zhang

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  29. Surfactant-thermal method to prepare two novel two-dimensional Mn–Sb–S compounds for photocatalytic applications

    Journal of Solid State Chemistry · 2014-08-26

    Lina Nie, Wei‐Wei Xiong, Pei‐Zhou Li, Jianyu Han, Guodong Zhang, Shengming Yin, Yanli Zhao, Rong Qing Xu, Qichun Zhang

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  30. Surfactant-Thermal Syntheses, Structures, and Magnetic Properties of Mn–Ge–Sulfides/Selenides

    Inorganic Chemistry · 2014-09-10

    Guodong Zhang, Pei‐Zhou Li, Junfeng Ding, Yi Liu, Wei‐Wei Xiong, Lina Nie, Tom Wu, Yanli Zhao, Alfred Iing Yoong Tok, Qichun Zhang

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  31. [Mn(dien) 2 ]MnSnS 4 , [Mn(1,2-dap)] 2 Sn 2 S 6 and [Mn(en) 2 ]MnGeS 4 : from 1D anionic and neutral chains to 3D neutral frameworks

    CrystEngComm · 2014-11-19

    Cheng‐Yang Yue, Xiao‐Wu Lei, Ling Yin, Xiurong Zhai, Zhong‐Ren Ba, Yan-Qiang Niu, Yue-Peng Li

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  32. Expanding the structural versatility of thiostannate( iv ) complexes

    CrystEngComm · 2015-01-01

    Peter Nørby, Espen Z. Eikeland, Jacob Overgaard, Simon Johnsen, Bo B. Iversen

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  33. Soft template mediated synthesis of Bi–In–Zn–S and its efficient visible-light-driven decomposition of methylene blue

    RSC Advances · 2015-01-01

    Aniruddha Molla, Meenakshi Sahu, Yogendra Kumar, Sahid Hussain

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  34. Hydrazine-Hydrothermal Synthesis and Characterization of the Two New Quaternary Thioantimonates(III) BaAgSbS3 and BaAgSbS3·H2O

    Inorganic Chemistry · 2015-09-02

    Chang Liu, Yaying Shen, Peipei Hou, Mingjia Zhi, Chunmei Zhou, Wen‐Xiang Chai, Jian‐Wen Cheng, Yi Liu

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  35. Two Quaternary Copper Thiostannates with Lanthanum(III) Complexes

    Journal of Cluster Science · 2015-09-22

    Xiao-Feng Tan, Xing Liu, Jian Zhou, Li‐Gang Zhu, Rong-Qing Zhao, Qian Huang

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  36. Unsaturated Mn complex decorated hybrid thioarsenates: Syntheses, crystal structures and physical properties

    Journal of Solid State Chemistry · 2016-01-04

    Cheng‐Yang Yue, Xiao‐Wu Lei, Ya-Wei Tian, Jing Hua Xu, Yiqun Bai, Fei Wang, Pengfei Zhou, Xiaofan Liu, Fei‐Yan Yi

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  37. Facile Hydrazine‐Hydrothermal Syntheses and Characterizations of Two Quaternary Thioarsenates(III): Two‐Dimensional SrAg4As2S6⋅2 H2O and One‐Dimensional BaAgAsS3

    Chemistry - An Asian Journal · 2016-04-28

    Dongming Yan, Chang Liu, Wen‐Xiang Chai, Xuerong Zheng, Luodong Zhang, Mingjia Zhi, Chunmei Zhou, Qichun Zhang, Yi Liu

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  38. Unprecedented 3D and 2D Frameworks of Manganese Thioarsenates Based on Heterometallic Cubic Cluster [Mn6(µ6‐S)(AsS3)4] and Covalent Linker N2H4

    European Journal of Inorganic Chemistry · 2016-07-22

    Chunying Tang, Yali Shen, Peipei Sun, ShuZhen Liu, Jingyu Han, Yun Liu, Hui Sun, Dingxian Jia

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  39. A novel 2-D Mn selenidostannate( iv ) incorporating high-nuclear Mn clusters with spin canting behavior

    Dalton Transactions · 2017-01-01

    Jian Zhou, Hong Ping Xiao, Hua‐Hong Zou, Xing Liu

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  40. Hydrazine-Assisted Syntheses and Properties of Mercury Tellurides Containing Transition-Metal Complexes

    Inorganic Chemistry · 2017-05-11

    Peipei Sun, Shuzhen Liu, Shufen Li, Limei Zhang, Hui Sun, Dingxian Jia

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  41. A series of new hybrid selenidostannates with metal complexes prepared in alkylol amines

    Dalton Transactions · 2018-01-01

    Hai-Ying Luo, Jian Zhou

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  42. Hydrazine-solvothermal methods to synthesize polymeric thioarsenates from one-dimensional chains to a three-dimensional framework

    RSC Advances · 2018-01-01

    Jingyu Han, Shufen Li, Chunying Tang, Wei Zheng, Wenqing Jiang, Dingxian Jia

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  43. Complexations of Mn(II) with SbS4 and SbS3 ligands: Hydrazine-solvothermal syntheses, crystal structures and photocatalytic properties of manganese thioantimonates

    Journal of Solid State Chemistry · 2018-10-09

    Shufen Li, Jingyu Han, Limei Zhang, Wenqing Jiang, Dingxian Jia

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  44. Crystalline chalcogenidometalate-based compounds from uncommon reaction media

    Chemical Communications · 2022-01-01

    Zhou Wu, Gina Stuhrmann, Stefanie Dehnen

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  45. All-Inorganic Open-Framework Chalcogenides, A3Ga5S9·xH2O (A = Rb and Cs), Exhibiting Ultrafast Uranyl Remediation and Illustrating a Novel Post-Synthetic Preparation of Open-Framework Oxychalcogenides

    Chemistry of Materials · 2022-09-08

    Anna A. Berseneva, Mina Aziziha, Juliano Schorne Pinto, Theodore M. Besmann, Hans‐Conrad zur Loye

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  46. A crystalline organic hybrid indium antimony sulfide for high performance lithium/sodium storage

    Journal of Solid State Chemistry · 2022-10-03

    Longfei Zhai, Ji-Ming Yu, Shanqing Jia, Ting Yang, Chuang Yang, Wei Liu, Erzhuo Zhang, Bing Zheng, Wei‐Wei Xiong

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  47. Advances in Chalcogenide Crystal Growth: Flux and Solution Syntheses, and Approaches for Postsynthetic Modifications

    Crystal Growth & Design · 2023-07-10

    Anna A. Berseneva, Hans‐Conrad zur Loye

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  48. Hydrazine-thermal syntheses, structures, and photocatalytic properties of tellurostannate hybrids with iron (II) complex unit

    Polyhedron · 2023-08-07

    Xiao Yang, Taohong Ren, Jiahua Zhang, Dingxian Jia

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  49. Ligand-functionalized and ligand-bridged or organyl-separated chalcogenido metalate-based clusters

    Coordination Chemistry Reviews · 2023-09-26

    Zhou Wu, Mirko Tallu, Gina Stuhrmann, Stefanie Dehnen

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  50. Hydrazine-Assisted Synthesis, Structures, Photoelectricity, and Photocatalysis of Ternary Mercury–Tellurostannate Hybrids with Transition-Metal Complexes

    Inorganic Chemistry · 2024-04-01

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