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RESEARCH PAPER · Inorganic Chemistry · 2000

Preparation of a Chiral, 2-Dimensional Network Containing Metallacrown and Copper Benzoate Building Blocks

Jeffrey J. Bodwin, Vincent L. Pecoraro

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Preparation of a Chiral, 2-Dimensional Network Containing Metallacrown and Copper Benzoate Building BlocksOriginalPreparation of Site-Differentiated Mixed Ligand and Mixed Ligand/Mixed Metal Metallacrowns97The development of chiral metallacrowns into anion recognition agents and porous materials202Synthesis, Structure, and Properties of a Novel Heterooctametallic Complex Containing a Cyclic Ru4Ni4 Core68Synthesis, Structure, and Properties of a Novel Heterooctametallic Complex Containing a Cyclic Ru4Ni4 Core13Quantitative structural determination of the high coverage phase of the benzoate species on Cu(110)30Cu(2-methylpyrazine-5-carboxylate)2 hydrate: a metal-containing-ligand for the construction of organic–inorganic framework materials. Four new one-, two- and three-dimensional mixed-valent CuI–CuII coordination polymers34Enantioseparation of Racemic Organic Molecules by a Zeolite Analogue7018 Supramolecular coordination chemistry20Copper(ii) and cobalt(ii) coordination polymers with bridging 1,2,4,5-benzenetetracarboxylate and N-methylimidazole: coordination number-determined sheet topology53Pseudohalide complexation by manganese 12-metallacrowns-4 complexes56Rational Design of Homochiral Solids Based on Two-Dimensional Metal Carboxylates207Rational Design of Homochiral Solids Based on Two-Dimensional Metal Carboxylates20Two Chiral Coordination Polymers: Preparation and X-ray Structures of Mono(4-sulfo- l -phenylalanine)(diaqua) Zinc(II) and Copper(II) Complexes52Synthesis and crystal structure of a mixed-ligand lanthanum complex of phenanthroline H-bonded with benzo-15-crown-53Pentacopper(II) 12-metallacrown-4 complexes with α- and β-aminohydroxamic acids in aqueous solution: a reinvestigation60Nature of the Reactants and Influence of Water on the Supramolecular Assembly59Synthesis and Magnetic Properties of a Metallacryptate that Behaves as a Single‐Molecule Magnet134Synthesis and Magnetic Properties of a Metallacryptate that Behaves as a Single‐Molecule Magnet22An Unprecedented 8-Fold Interpenetrating Diamondoid-like Coordination Polymer Containing a Cu+4(RCO2)4 Cluster as Connecting Node43Chiral porous coordination networks: rational design and applications in enantioselective processes885Homochiral Zn and Cd Coordination Polymers Containing Amino Acid−Tetrazole Ligands121From Achiral Ligands to Chiral Coordination Polymers: Spontaneous Resolution, Weak Ferromagnetism, and Topological Ferrimagnetism525Interweaving 3D Network with Double Helical Tubes Filled by 1D Coordination Polymer Chains87The First Metal (Nd3+, Mn2+, and Pb2+) Coordination Compounds of 3,5‐Dinitrotyrosine and their Nonlinear Optical Properties51Formation of [2 + 2] diruthenium(ii) metallomacrocycles from ligands containing 2,2′:6′,2″-terpyridine domains linked through flexible polyethyleneoxy spacers41Di‐2‐pyridyl Ketone Oxime in Zinc Chemistry: Inverse 12‐Metallacrown‐4 Complexes and Cationic Pentanuclear Clusters53Synthesis and Structural Characterization of a Nonplanar Neutral [36]Metallacrown-12 Nickel Compound [Ni(C13H9N3O2)(CH3OH)]1257The coordination chemistry of pyridyl oximes323Metallacryptate Single-Molecule Magnets: Effect of Lower Molecular Symmetry on Blocking Temperature110Synthesis and structure of [ 18 - MC Cu II ( N ) pko - 6 ] 6 + : A new member of anion encapsulating metallamacrocyles26Resolution of a Racemic Small Molecular Alcohol by a Chiral Metal−Organic Coordination Polymer through Intercalation59First mixed hydrazide/hydroxylamide metal aggregates21“Isomerism” of Coordination Modes and Numbers in Pentanuclear Organozinc Hydroxylamides: An Exercise in Subtle Substituent Size Effects25Synthesis, Characterization, and Crystal Structure of Two Manganese Metallacrowns: 30‐Metallacrown‐10 and 18‐Metallacrown‐6 with Ligands Derived from 3‐Hydroxy‐2‐naphthalenecarbohydrazide50Synthesis, Solution Thermodynamics, and X‐ray Study of CuII [12]Metallacrown‐4 with GABA Hydroxamic Acid: An Unprecedented Crystal Structure of a [12]MC‐4 with a γ‐Aminohydroxamate33A new Cu(ii) [12]metallocrown-4 pentanuclear complex based on a Cu(ii)-malonomonohydroxamic acid unit39Metallacrown-based compartments: selective encapsulation of three isonicotinate anions in non-centrosymmetric solids61Old materials with new tricks: multifunctional open-framework materials1073Two novel 18-metallacrown-6 complexes: Synthesis, structural characterization and bioactivity20Controlling the Polymorph of LnIII(NO3)3-x(OH)x[15-MCCuII(N)S-pheHA-5] Complexes through Solvent Type and LnIII Ion Choice38Structural and Functional Evolution of Metallacrowns504Porous Crystal Derived from a Tricarboxylate Linker with Two Distinct Binding Motifs229A novel 3-dimensional metallacrown supramolecule: Synthesis, crystal structure and magnetic properties3Synthesis, crystal structure and magnetic properties of a novel cross-net-shaped metallamacrocycle [ Mn 10 III Mn 4 II ( L ) 8 ( HL ) 2 ( H 2 O ) 2 ( CH 3 OH ) 14 ] · 8 H 2 O · 8 CH 3 OH9Copper(II)–lanthanide(III) 15-metallacrown-5 complexes based on pyrazinohydroxamic acid as new multiple-binding pentagonal platforms with Lewis amphoteric nature19A mixed carboxylate polymer as an intermediate during synthesis of mononuclear bis -3, 5-dimethylpyrazole copper(II) benzoates15A 2D Layered Metal–Organic Framework Constructed by Using a Hexanuclear Manganese Metallamacrocycle as a Supramolecular Building Block24Iron( iii ) coordination induced novel 18-metallacrown-6 complex: esterification and isolation of the ligand15Construction of a Three-Dimensional Polynuclear Zinc Compound Based on Unique Metallophthalocyanine-like Subunits432D Layered metal–organic frameworks built using a hexanuclear metallamacrocycle and an octanuclear metallamacrocycle as supramolecular building blocks24Supramolecular Isomerism of Metal−Organic Frameworks Derived from a Bicarboxylate Linker with Two Distinct Binding Motifs33Metal−Organic Polyhedron Based on a CuII Paddle-Wheel Secondary Building Unit at the Truncated Octahedron Corners62Synthesis, crystal structure and esterification of a novel iron(III) 18-metallacrown-6 complex7A novel 18-metallacrown-6 complex: Synthesis, structural characterization and magnetic properties6A series of novel chiral lanthanide coordination polymers with channels constructed from 16Ln-based cage-like building units39A 2-D metal-organic framework of the iron-based 18-metallacrown-6 with N-(methyl-maleamic ester) terminal ligand4Chiral Metallacrown Supramolecular Compartments that Template Nanochannels: Self‐Assembly and Guest Absorption51Use of 2-pyrimidineamidoxime to generate polynuclear homo-/heterometallic assemblies: synthesis, crystal structures and magnetic study with theoretical investigations on the exchange mechanism32Self-assembly of one Ag(I) 2D metallacrown polymer with bis-bidentate Schiff-base ligand N,N′-bis(furan-2-ylmethylene)hydrazine: Synthesis, crystal structures and luminescent properties15Thermodynamics of Core Metal Replacement and Self-Assembly of Ca2+ 15-Metallacrown-554Voltammetric Characterization of Redox‐Inactive Guest Binding to LnIII[15‐Metallacrown‐5] Hosts Based on Competition with a Redox Probe54A Triple‐Decker Heptadecanuclear (CuII)15(CrIII)2 Complex Assembled from Pentanuclear Metallacrowns56Esterification and isolation of the carboxylic acid with salicyl-bis-hydrazide via coordination of iron(III) 18-metallacrown-6 complex5One new 2D cadmium-organic framework containing 2,4′-biphenyldicarboxylate ligand11Homochiral, Helical Supramolecular Metal−Organic Frameworks Organized by Strong π···π Stacking Interactions: Single-Crystal to Single-Crystal Transformations in Closely Packed Solids79Organozinc hydroxylamides: on the bulk-dependent interplay of nuclearity, structure and dynamics4A three-dimensional copper(ii) 12-metallacrown-4 complex with malonomonohydroxamic acid (H3mmh) as a ligand26Homochiral 3D metal–organic frameworks from chiral 1D rods: 6-way helical packing23Bis(tetraethylammonium) bis(dimethylformamide)tetrakis(μ-N,2-dioxidobenzene-1-carboximidato)pentacopper(II)5Gd(III)[15-Metallacrown-5] Recognition of Chiral α-Amino Acid Analogues66Metallacrowns of copper(II) and aminohydroxamates: Thermodynamics of self assembly and host–guest equilibria133Effects of the Central Lanthanide Ion Crystal Radius on the 15-MCCuII(N)pheHA-5 Structure49A Unique Independent One-Dimensional Green Luminescent Coordination Polymer Nanotube Based on an Unsymmetric Tricarboxylate Linker67Assembly of Near‐Infrared Luminescent Lanthanide Host(Host–Guest) Complexes With a Metallacrown Sandwich Motif170Assembly of Near‐Infrared Luminescent Lanthanide Host(Host–Guest) Complexes With a Metallacrown Sandwich Motif19Magnetic and Sorption Properties of Supramolecular Systems Based on Pentanuclear Copper(II) 12‐Metallacrown‐4 Complexes and Isomeric Phthalates: Structural Modeling of the Different Stages of Alcohol Sorption51Esterification of the ligand: Synthesis, characterization and crystal structure of a iron(III) 18-metallacrown-6 complex with methyl 4-(5′-chlorosalicylhydrazinocarbonyl) butyrate6A homochiral network constructed by supramolecular packing of 2D chiral bilayer: synthesis, structure and property of metal(ii) complex based on achiral 3,3′,4,4′-oxydiphthalate and coligand123D Coordination Polymers with Chiral Structures, [Ln2(tda)2(H2O)3]·5H2O: Hydrothermal Synthesis, Structural Characterization, and Luminescent Properties9Insight into the structural versatility of the Ln(III)[15-metallacrown-5] platform by comparing analogs with Ni(II), Cu(II), and Zn(II) ring ions30Hydrothermal Synthesis, Structure, Magnetic, and Photoluminescent Properties of a Heterometallic Cobalt(II)/Cerium(III) Coordination Compound with the Ligand Pyrazine 2, 3‐dicarboxylic Acid15Clarifying the Mechanism of Cation Exchange in Ca(II)[15-MCCu(II)Ligand-5] Complexes30Structures and magnetism of two manganese crowns assembled with 2,4-dihydroxyacetophenone oxime5Progressive decoration of pentanuclear Cu(ii) 12-metallacrown-4 nodes towards targeted 1- and 2D extended networks29Stoichiometric diversity of Ni(ii) metallacrowns with β-alaninehydroxamic acid in aqueous solution11Isolation of Elusive Tetranuclear and Pentanuclear M(II)–Hydroximate Intermediates in the Assembly of Lanthanide [15-Metallacrown-5] Complexes33Controllable Formation of Heterotrimetallic Coordination Compounds: Systematically Incorporating Lanthanide and Alkali Metal Ions into the Manganese 12-Metallacrown-4 Framework72Solvent Dependent Assembly of Lanthanide Metallacrowns Using Building Blocks with Incompatible Symmetry Preferences48A series of 3D metal organic frameworks based on [24-MC-6] metallacrown clusters: structure, magnetic and luminescence properties2522-Azametallacrown-8 complex with a triazole-bridged ligand: synthesis, structure and magnetic properties13One-Dimensional Coordination Polymers of 12-Metallacrown-4 Complexes: {Na2(L)2[12- ${\rm{M}}{{\rm{C}}_{{\rm{M}}{{\rm{n}}^{{\rm{III}}}}{\rm{(N)shi}}}}$ M C M n III ( N ) shi -4]} n , where L is Either −O2CCH2CH3 or −O2CCH2CH2CH3912-MC-4 metallacrowns as versatile tools for SMM research94Facile carboxylate ligand variation of heterotrimetallic 12-metallacrown-4 complexes20Tetra-Fe( iii ) and deca-Mn( iii ) metallacrowns built from bis-salicylhydrazide ligands: synthesis, structures and magnetic properties6Structures and spectroscopic properties of Ni(II) and Mn(II) complexes based on 5-(3′, 5′-dicarboxylphenyl) picolinic acid ligand10Design of 2D Porous Coordination Polymers Based on Metallacrown Units22Metallacrown-based compounds: Applications in catalysis, luminescence, molecular magnetism, and adsorption104Four Mixed 3d-4f 12-Metallacrown-4 Complexes: Syntheses, Structures and Magnetic Properties13Supramolecular Maleate Adducts of Copper(II) 12‐Metallacrown‐4: Magnetism, EPR, and Alcohol Sorption Properties17Metallacrown Complexes Reaching the Nanosize Regime1The synthetic strategies of metal–organic framework membranes, films and 2D MOFs and their applications in devices124Three-Dimensional Porous Architectures Based on MnII/III Three-Blade Paddle Wheel Metallacryptates7A New Family of 2D Coordination Polymers Based on 3d‐4f 15‐Metallacrown‐5 Units: Synthesis, Structure, and Single‐Molecule Magnet Behavior18Synthesis and crystal structure of a pentacopper(II) 12-metallacrown-4: cis-diaquatetrakis(dimethylformamide-κO)manganese(II) tetrakis(μ3-N,2-dioxidobenzene-1-carboximidate)pentacopper(II) dimethylformamide monosolvate1Research Progress of Metallacrown-Based Complexes2A family of 1D coordination polymers based on Ln–Cu 15-metallacrown-5 units with two topological sorting: syntheses, structures, and single-chain magnet behaviour5Structural and Magnetic Properties of a {GdCu5}2 Metallacrown Dimer with a Disulfonate Linker5Magnetocaloric effect in 1D-polymers bearing 15-metallacrown-5 {GdCu 5 } 3+ units and anionic oxalate complexes3Features of the Crystal Structure of Polynuclear Metallamacrocyclic Copper (II) Complexes Containing Polycarboxylate Anions4

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  1. Preparation of Site-Differentiated Mixed Ligand and Mixed Ligand/Mixed Metal Metallacrowns

    Inorganic Chemistry · 2001-02-23

    George Psomas, Ann Joern Stemmler, C. Dendrinou-Samara, Jeffrey J. Bodwin, Manuela Schneider, Maria V. Alexiou, Jeff W. Kampf, Dimitris P. Kessissoglou, Vincent L. Pecoraro

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  2. The development of chiral metallacrowns into anion recognition agents and porous materials

    Coordination Chemistry Reviews · 2001-06-01

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  3. Synthesis, Structure, and Properties of a Novel Heterooctametallic Complex Containing a Cyclic Ru4Ni4 Core

    Angewandte Chemie International Edition · 2001-08-03

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  4. Synthesis, Structure, and Properties of a Novel Heterooctametallic Complex Containing a Cyclic Ru4Ni4 Core

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    Indrani Pal, Falguni Basuli, Thomas C. W. Mak, Samaresh Bhattacharya

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  5. Quantitative structural determination of the high coverage phase of the benzoate species on Cu(110)

    Surface Science · 2001-10-01

    M. Pascal, Christine L. A. Lamont, M. Kittel, J.T. Hoeft, Ralf Terborg, Martin Polcik, J.–H. Kang, Rachel L. Toomes, David Phillip Woodruff

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  6. Cu(2-methylpyrazine-5-carboxylate)2 hydrate: a metal-containing-ligand for the construction of organic–inorganic framework materials. Four new one-, two- and three-dimensional mixed-valent CuI–CuII coordination polymers

    Inorganica Chimica Acta · 2001-11-01

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  7. Enantioseparation of Racemic Organic Molecules by a Zeolite Analogue

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  8. 18 Supramolecular coordination chemistry

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  9. Copper(ii) and cobalt(ii) coordination polymers with bridging 1,2,4,5-benzenetetracarboxylate and N-methylimidazole: coordination number-determined sheet topology

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  10. Pseudohalide complexation by manganese 12-metallacrowns-4 complexes

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  11. Rational Design of Homochiral Solids Based on Two-Dimensional Metal Carboxylates

    Angewandte Chemie International Edition · 2002-04-02

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  12. Rational Design of Homochiral Solids Based on Two-Dimensional Metal Carboxylates

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  13. Two Chiral Coordination Polymers: Preparation and X-ray Structures of Mono(4-sulfo- l -phenylalanine)(diaqua) Zinc(II) and Copper(II) Complexes

    Inorganic Chemistry · 2002-05-24

    Yong‐Rong Xie, Ren‐Gen Xiong, Xiang Xue, Xue-Tai Chen, Zi‐Ling Xue, Xiao‐Zeng You

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  14. Synthesis and crystal structure of a mixed-ligand lanthanum complex of phenanthroline H-bonded with benzo-15-crown-5

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    Zhen-Ping Ji, Yanni Chen, Xiang Cheng, Gongzhen Cheng

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  15. Pentacopper(II) 12-metallacrown-4 complexes with α- and β-aminohydroxamic acids in aqueous solution: a reinvestigation

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  16. Nature of the Reactants and Influence of Water on the Supramolecular Assembly

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  17. Synthesis and Magnetic Properties of a Metallacryptate that Behaves as a Single‐Molecule Magnet

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  18. Synthesis and Magnetic Properties of a Metallacryptate that Behaves as a Single‐Molecule Magnet

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  19. An Unprecedented 8-Fold Interpenetrating Diamondoid-like Coordination Polymer Containing a Cu+4(RCO2)4 Cluster as Connecting Node

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  20. Chiral porous coordination networks: rational design and applications in enantioselective processes

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  21. Homochiral Zn and Cd Coordination Polymers Containing Amino Acid−Tetrazole Ligands

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  22. From Achiral Ligands to Chiral Coordination Polymers: Spontaneous Resolution, Weak Ferromagnetism, and Topological Ferrimagnetism

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  23. Interweaving 3D Network with Double Helical Tubes Filled by 1D Coordination Polymer Chains

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  24. The First Metal (Nd3+, Mn2+, and Pb2+) Coordination Compounds of 3,5‐Dinitrotyrosine and their Nonlinear Optical Properties

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  25. Formation of [2 + 2] diruthenium(ii) metallomacrocycles from ligands containing 2,2′:6′,2″-terpyridine domains linked through flexible polyethyleneoxy spacers

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  26. Di‐2‐pyridyl Ketone Oxime in Zinc Chemistry: Inverse 12‐Metallacrown‐4 Complexes and Cationic Pentanuclear Clusters

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  27. Synthesis and Structural Characterization of a Nonplanar Neutral [36]Metallacrown-12 Nickel Compound [Ni(C13H9N3O2)(CH3OH)]12

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  28. The coordination chemistry of pyridyl oximes

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  29. Metallacryptate Single-Molecule Magnets: Effect of Lower Molecular Symmetry on Blocking Temperature

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  30. Synthesis and structure of [ 18 - MC Cu II ( N ) pko - 6 ] 6 + : A new member of anion encapsulating metallamacrocyles

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  31. Resolution of a Racemic Small Molecular Alcohol by a Chiral Metal−Organic Coordination Polymer through Intercalation

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  32. First mixed hydrazide/hydroxylamide metal aggregates

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    Surajit Jana, Raphael J. F. Berger, Roland Fröhlich, Norbert W. Mitzel

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  33. “Isomerism” of Coordination Modes and Numbers in Pentanuclear Organozinc Hydroxylamides: An Exercise in Subtle Substituent Size Effects

    European Journal of Inorganic Chemistry · 2006-09-14

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  34. Synthesis, Characterization, and Crystal Structure of Two Manganese Metallacrowns: 30‐Metallacrown‐10 and 18‐Metallacrown‐6 with Ligands Derived from 3‐Hydroxy‐2‐naphthalenecarbohydrazide

    European Journal of Inorganic Chemistry · 2006-10-10

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  35. Synthesis, Solution Thermodynamics, and X‐ray Study of CuII [12]Metallacrown‐4 with GABA Hydroxamic Acid: An Unprecedented Crystal Structure of a [12]MC‐4 with a γ‐Aminohydroxamate

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  36. A new Cu(ii) [12]metallocrown-4 pentanuclear complex based on a Cu(ii)-malonomonohydroxamic acid unit

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    Elżbieta Gumienna‐Kontecka, Irina A. Golenya, Nikolay M. Dudarenko, Agnieszka Dobosz, Matti Haukka, Igor O. Fritsky, Jolanta Świa̧tek-Kozłowska

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  37. Metallacrown-based compartments: selective encapsulation of three isonicotinate anions in non-centrosymmetric solids

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    Gellert Mezei, Jeff W. Kampf, Shilie Pan, Kenneth Reinhard Poeppelmeier, B. Watkins, Vincent L. Pecoraro

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  38. Old materials with new tricks: multifunctional open-framework materials

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  39. Two novel 18-metallacrown-6 complexes: Synthesis, structural characterization and bioactivity

    Polyhedron · 2007-01-27

    Feng‐Ping Xiao, Long‐Fei Jin, Gongzhen Cheng, Zhen-Ping Ji

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  40. Controlling the Polymorph of LnIII(NO3)3-x(OH)x[15-MCCuII(N)S-pheHA-5] Complexes through Solvent Type and LnIII Ion Choice

    Crystal Growth & Design · 2007-05-12

    Curtis M. Zaleski, Annabel D. Cutland-Van Noord, Jeff W. Kampf, Vincent L. Pecoraro

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  41. Structural and Functional Evolution of Metallacrowns

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    Gellert Mezei, Curtis M. Zaleski, Vincent L. Pecoraro

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  42. Porous Crystal Derived from a Tricarboxylate Linker with Two Distinct Binding Motifs

    Journal of the American Chemical Society · 2007-12-01

    Antek G. Wong‐Foy, Olivier Lebel, Adam J. Matzger

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  43. A novel 3-dimensional metallacrown supramolecule: Synthesis, crystal structure and magnetic properties

    Solid State Sciences · 2008-01-26

    Feng‐Ping Xiao, Long‐Fei Jin, Wei Luo, Gongzhen Cheng, Zhen-Ping Ji

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  44. Synthesis, crystal structure and magnetic properties of a novel cross-net-shaped metallamacrocycle [ Mn 10 III Mn 4 II ( L ) 8 ( HL ) 2 ( H 2 O ) 2 ( CH 3 OH ) 14 ] · 8 H 2 O · 8 CH 3 OH

    Inorganic Chemistry Communications · 2008-03-17

    Feng‐Ping Xiao, Long‐Fei Jin

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  45. Copper(II)–lanthanide(III) 15-metallacrown-5 complexes based on pyrazinohydroxamic acid as new multiple-binding pentagonal platforms with Lewis amphoteric nature

    Polyhedron · 2008-06-09

    E.V. Govor, A.B. Lysenko, Alexander N. Chernega, Judith A. K. Howard, Andriy A. Mokhir, Joachim Sieler, K.V. Domasevitch

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  46. A mixed carboxylate polymer as an intermediate during synthesis of mononuclear bis -3, 5-dimethylpyrazole copper(II) benzoates

    Journal of Coordination Chemistry · 2008-07-24

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  47. A 2D Layered Metal–Organic Framework Constructed by Using a Hexanuclear Manganese Metallamacrocycle as a Supramolecular Building Block

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  48. Iron( iii ) coordination induced novel 18-metallacrown-6 complex: esterification and isolation of the ligand

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  49. Construction of a Three-Dimensional Polynuclear Zinc Compound Based on Unique Metallophthalocyanine-like Subunits

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  50. 2D Layered metal–organic frameworks built using a hexanuclear metallamacrocycle and an octanuclear metallamacrocycle as supramolecular building blocks

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