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RESEARCH PAPER · Chemical Communications · 2007

Metallacrown-based compartments: selective encapsulation of three isonicotinate anions in non-centrosymmetric solids

Gellert Mezei, Jeff W. Kampf, Shilie Pan, Kenneth Reinhard Poeppelmeier, Byron Watkins, Vincent L. Pecoraro

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Metallacrown-based compartments: selective encapsulation of three isonicotinate anions in non-centrosymmetric solidsOriginalControlling the Polymorph of LnIII(NO3)3-x(OH)x[15-MCCuII(N)S-pheHA-5] Complexes through Solvent Type and LnIII Ion Choice38Structural and Functional Evolution of Metallacrowns504Crystal-to-crystal transformations in heterometallic yttrium( iii )–copper( i ) iodide derivatives in a confined solvent-free environment: Influence of solvated yttrium cations on the nuclearity and dimensionality of iodocuprate clusters43Rare example of a polynuclear heterometallic yttrium(III)–copper(I) iodide cluster with a [Y6(μ6-O)(μ3-OH)8]8+ core structure showing single crystal-to-single crystal transformation31Supramolecular coordination chemistry3Thermodynamics of binding of carboxylates to amphiphilic Eu3+/Cu2+ metallacrown41A new 3-D microporous Ln(III)–Cu(I) framework constructed by pyridine-3,5-dicarboxylate16Sodium and Potassium Ion Directed Self-Assembled Multinuclear Assembly of Divalent Nickel or Copper and l -Leucine Derived Ligand37Growth and Properties of Single Crystals of Noncentrosymmetric Na3VO2B6O1187Chiral Metallacrown Supramolecular Compartments that Template Nanochannels: Self‐Assembly and Guest Absorption51Supramolecular coordination chemistry9Thermodynamics of Core Metal Replacement and Self-Assembly of Ca2+ 15-Metallacrown-554Structural diversity and distinct photoluminescent properties of two new lanthanide-copper (I) frameworks based on mixed isonicontinate/oxalate ligands9Voltammetric Characterization of Redox‐Inactive Guest Binding to LnIII[15‐Metallacrown‐5] Hosts Based on Competition with a Redox Probe54Syntheses and Crystal Structures of LnIII–CuI Coordination Polymers14Construction of two 2D 3d-4f coordination complexes based on the linkages of left-and right-handed helical chains38Tri- and Tetranuclear Nickel(II) Inverse Metallacrown Complexes Involving Oximato Oxygen Linkers: Role of the Guest Anion (Oxo versus Alkoxo) in Controlling the Size of the Ring Topology22A Triple‐Decker Heptadecanuclear (CuII)15(CrIII)2 Complex Assembled from Pentanuclear Metallacrowns56Heterometallic coordination polymers containing unique inorganic chain of [Lniii2Cuii3(OH)4]: syntheses, structures and magnetism22Synthesis, Crystal Structures, and Photoluminescence of Lanthanide Coordination Polymers with 4‐Acetamidobenzoate8Gd(III)[15-Metallacrown-5] Recognition of Chiral α-Amino Acid Analogues66Metallacrowns of copper(II) and aminohydroxamates: Thermodynamics of self assembly and host–guest equilibria133In Situ Tetrazole Ligand Synthesis of Two‐Fold Interpenetrating Zinc Coordination Frameworks27Effects of the Central Lanthanide Ion Crystal Radius on the 15-MCCuII(N)pheHA-5 Structure49Assembly of Near‐Infrared Luminescent Lanthanide Host(Host–Guest) Complexes With a Metallacrown Sandwich Motif170Assembly of Near‐Infrared Luminescent Lanthanide Host(Host–Guest) Complexes With a Metallacrown Sandwich Motif19Heterometallic cubane-like {M 2 Ln 2 } (M = Ni, Zn; Ln =, Gd, Dy) and {Ni 2 Y 2 } aggregates. Synthesis, structures and magnetic properties68A novel deep UV nonlinear optical crystal Ba3B6O11F2, with a new fundamental building block, B6O14 group180Syntheses, structure, and magnetic properties of hexanuclear MnIII2MIII4 (M = Y, Gd, Tb, Dy) complexes20Influencing the Size and Anion Selectivity of Dimeric Ln3+[15-Metallacrown-5] Compartments through Systematic Variation of the Host Side Chains and Central Metal59Enhanced Guest Affinity and Enantioselectivity through Variation of the Gd3+[15-Metallacrown-5] Side Chain41Insight into the structural versatility of the Ln(III)[15-metallacrown-5] platform by comparing analogs with Ni(II), Cu(II), and Zn(II) ring ions30Clarifying the Mechanism of Cation Exchange in Ca(II)[15-MCCu(II)Ligand-5] Complexes30Syntheses and Structures of Terpyridine‐Metal Complexes16Stoichiometric diversity of Ni(ii) metallacrowns with β-alaninehydroxamic acid in aqueous solution11Synthesis, crystal structure and magnetic properties of dinuclear NiIILnIII complexes based on a flexible polydentate ligand25Isolation of Elusive Tetranuclear and Pentanuclear M(II)–Hydroximate Intermediates in the Assembly of Lanthanide [15-Metallacrown-5] Complexes33Heterodinuclear MII–LnIII single molecule magnets constructed from exchange-coupled single ion magnets41Controllable Formation of Heterotrimetallic Coordination Compounds: Systematically Incorporating Lanthanide and Alkali Metal Ions into the Manganese 12-Metallacrown-4 Framework72Synthesis, crystal structures and magnetic properties of a novel fused 9-metallacrown-3 and a high/low spin [Fe(pao)2]3·H2O4A novel [Na6Co6] metallacrown with [24-MCNa-6] periphery encapsulating the [12-MCCo-6] inner core: Synthesis, structure, and magnetic properties2Heterometallic Mixed3d-4fMetallacrowns: Structural Versatility, Luminescence, and Molecular Magnetism55Facile carboxylate ligand variation of heterotrimetallic 12-metallacrown-4 complexes20Topological Aspects of 3d/4f Polynuclear Coordination Clusters0Design of 2D Porous Coordination Polymers Based on Metallacrown Units22Metallacrowns: From Discovery to Potential Applications in Biomolecular Imaging7Four Mixed 3d-4f 12-Metallacrown-4 Complexes: Syntheses, Structures and Magnetic Properties13Anion Encapsulation Drives the Formation of Dimeric GdIII[15-metallacrown-5]3+ Complexes in Aqueous Solution19Stepwise Investigation of the Influences of Steric Groups versus Counterions To Target Cu/Dy Complexes16High Nuclearity Assemblies and One-Dimensional (1D) Coordination Polymers Based on Lanthanide–Copper 15-Metallacrown-5 Complexes (LnIII = Pr, Nd, Sm, Eu)21Metallacrown Complexes Reaching the Nanosize Regime1Metallacrowns: Supramolecular Constructs With Potential in Extended Solids, Solution-State Dynamics, Molecular Magnetism, and Imaging25Monomer, chain, layer and 3-D framework constructed by linear 4′-(4-carboxyphenyl)-2,2′:6′,2″-terpyridine10Opening Magnetic Hysteresis by Axial Ferromagnetic Coupling: From Mono‐Decker to Double‐Decker Metallacrown119Opening Magnetic Hysteresis by Axial Ferromagnetic Coupling: From Mono‐Decker to Double‐Decker Metallacrown13Lanthanides1Aspects of NMR Characterization of Metallacrowns1Host–Guest Chemistry of Metallacrowns4Water-Soluble 15-Metallacrown-5 Complexes: Molecular Structures and Properties3Benzene–Ni10S20 Interaction. Host–Guest Features and Nuclear Magnetic Resonance Patterns toward Prototypical Metal-Based Active Cavities0Discrete metallosupramolecular architectures with amino acids22

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  1. Controlling the Polymorph of LnIII(NO3)3-x(OH)x[15-MCCuII(N)S-pheHA-5] Complexes through Solvent Type and LnIII Ion Choice

    Crystal Growth & Design · 2007-05-12

    Curtis M. Zaleski, Annabel D. Cutland-Van Noord, Jeff W. Kampf, Vincent L. Pecoraro

    Read original paper ↗ ·

  2. Structural and Functional Evolution of Metallacrowns

    Chemical Reviews · 2007-11-01

    Gellert Mezei, Curtis M. Zaleski, Vincent L. Pecoraro

    Read original paper ↗ ·

  3. Crystal-to-crystal transformations in heterometallic yttrium( iii )–copper( i ) iodide derivatives in a confined solvent-free environment: Influence of solvated yttrium cations on the nuclearity and dimensionality of iodocuprate clusters

    Dalton Transactions · 2008-01-01

    Shashank Mishra, Erwann Jeanneau, Henry Chermette, S. Danièle, Liliane G. Hubert-Pfalzgraf

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  4. Rare example of a polynuclear heterometallic yttrium(III)–copper(I) iodide cluster with a [Y6(μ6-O)(μ3-OH)8]8+ core structure showing single crystal-to-single crystal transformation

    CrystEngComm · 2008-01-01

    Shashank Mishra, Erwann Jeanneau, S. Danièle, Liliane G. Hubert-Pfalzgraf

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  5. Supramolecular coordination chemistry

    Annual Reports Section A (Inorganic Chemistry) · 2008-01-01

    Paul J. Lusby

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  6. Thermodynamics of binding of carboxylates to amphiphilic Eu3+/Cu2+ metallacrown

    Dalton Transactions · 2009-01-01

    Matteo Tegoni, Manuel Tropiano, Luciano Marchiò

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  7. A new 3-D microporous Ln(III)–Cu(I) framework constructed by pyridine-3,5-dicarboxylate

    Journal of Coordination Chemistry · 2009-03-26

    Jianglong Yi, Zhiyong Fu, Shijun Liao

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  8. Sodium and Potassium Ion Directed Self-Assembled Multinuclear Assembly of Divalent Nickel or Copper and l -Leucine Derived Ligand

    Inorganic Chemistry · 2009-09-11

    Mrigendra Dubey, Rik Rani Koner, Manabendra Ray

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  9. Growth and Properties of Single Crystals of Noncentrosymmetric Na3VO2B6O11

    Crystal Growth & Design · 2009-12-01

    Xiaoyun Fan, Shilie Pan, Xueling Hou, Xuelin Tian, Jian Wei Han, Jacob M. Haag, Kenneth Reinhard Poeppelmeier

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  10. Chiral Metallacrown Supramolecular Compartments that Template Nanochannels: Self‐Assembly and Guest Absorption

    Chemistry - An Asian Journal · 2009-12-23

    Choong‐Sun Lim, Joseph Jankolovits, Jeff W. Kampf, Vincent L. Pecoraro

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  11. Supramolecular coordination chemistry

    Annual Reports Section A (Inorganic Chemistry) · 2010-01-01

    Paul J. Lusby

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  12. Thermodynamics of Core Metal Replacement and Self-Assembly of Ca2+ 15-Metallacrown-5

    Inorganic Chemistry · 2010-04-29

    Matteo Tegoni, Michele Furlotti, Manuel Tropiano, Choong Sun Lim, Vincent L. Pecoraro

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  13. Structural diversity and distinct photoluminescent properties of two new lanthanide-copper (I) frameworks based on mixed isonicontinate/oxalate ligands

    Inorganic Chemistry Communications · 2010-05-11

    Yao Kang, Fei Wang, Jian Zhang

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  14. Voltammetric Characterization of Redox‐Inactive Guest Binding to LnIII[15‐Metallacrown‐5] Hosts Based on Competition with a Redox Probe

    Chemistry - A European Journal · 2010-05-12

    Joseph Jankolovits, Jeff W. Kampf, Stephen Maldonado, Vincent L. Pecoraro

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  15. Syntheses and Crystal Structures of LnIII–CuI Coordination Polymers

    Zeitschrift für anorganische und allgemeine Chemie · 2010-07-06

    Man‐Bo Zhang, Hao‐Min Chen, Rui‐Xiang Hu

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  16. Construction of two 2D 3d-4f coordination complexes based on the linkages of left-and right-handed helical chains

    Inorganic Chemistry Communications · 2010-07-22

    Li-Cai Zhu, Yi Zhao, Shujuan Yu, Mouming Zhao

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  17. Tri- and Tetranuclear Nickel(II) Inverse Metallacrown Complexes Involving Oximato Oxygen Linkers: Role of the Guest Anion (Oxo versus Alkoxo) in Controlling the Size of the Ring Topology

    Inorganic Chemistry · 2010-08-27

    Anandalok Audhya, Manoranjan Maity, Kisholoy Bhattacharya, Rodolphe Clérac, Muktimoy Chaudhury

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  18. A Triple‐Decker Heptadecanuclear (CuII)15(CrIII)2 Complex Assembled from Pentanuclear Metallacrowns

    European Journal of Inorganic Chemistry · 2010-09-07

    Anna V. Pavlishchuk, Sergey V. Kolotilov, Mat­thias Zeller, Laurence Kenneth Thompson, Igor O. Fritsky, Anthony William Addison, Allen D. Hunter

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  19. Heterometallic coordination polymers containing unique inorganic chain of [Lniii2Cuii3(OH)4]: syntheses, structures and magnetism

    CrystEngComm · 2011-01-01

    Man‐Bo Zhang, Haomin Chen, Rui‐Xiang Hu, Zilu Chen

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  20. Synthesis, Crystal Structures, and Photoluminescence of Lanthanide Coordination Polymers with 4‐Acetamidobenzoate

    Zeitschrift für anorganische und allgemeine Chemie · 2011-03-24

    Xia Yin, Jun Yan Fan, Zhihong Wang, Wei‐Guang Zhang

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  21. Gd(III)[15-Metallacrown-5] Recognition of Chiral α-Amino Acid Analogues

    Inorganic Chemistry · 2011-05-03

    Choong‐Sun Lim, Joseph Jankolovits, Peng Jun Zhao, Jeff W. Kampf, Vincent L. Pecoraro

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  22. Metallacrowns of copper(II) and aminohydroxamates: Thermodynamics of self assembly and host–guest equilibria

    Coordination Chemistry Reviews · 2011-06-26

    Matteo Tegoni, Maurizio Remelli

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  23. In Situ Tetrazole Ligand Synthesis of Two‐Fold Interpenetrating Zinc Coordination Frameworks

    European Journal of Inorganic Chemistry · 2011-07-06

    Li Ma, Yongcai Qiu, Guo Peng, Jin‐Biao Cai, Hong Quan Deng

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  24. Effects of the Central Lanthanide Ion Crystal Radius on the 15-MCCuII(N)pheHA-5 Structure

    Inorganic Chemistry · 2011-07-18

    Curtis M. Zaleski, Choong‐Sun Lim, Annabel D. Cutland-Van Noord, Jeff W. Kampf, Vincent L. Pecoraro

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  25. Assembly of Near‐Infrared Luminescent Lanthanide Host(Host–Guest) Complexes With a Metallacrown Sandwich Motif

    Angewandte Chemie International Edition · 2011-09-12

    Joseph Jankolovits, Christopher M. Andolina, Jeff W. Kampf, Kenneth N. Raymond, Vincent L. Pecoraro

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  26. Assembly of Near‐Infrared Luminescent Lanthanide Host(Host–Guest) Complexes With a Metallacrown Sandwich Motif

    Angewandte Chemie · 2011-09-12

    Joseph Jankolovits, Christopher M. Andolina, Jeff W. Kampf, Kenneth N. Raymond, Vincent L. Pecoraro

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  27. Heterometallic cubane-like {M 2 Ln 2 } (M = Ni, Zn; Ln =, Gd, Dy) and {Ni 2 Y 2 } aggregates. Synthesis, structures and magnetic properties

    Dalton Transactions · 2011-12-21

    Zhao‐Sha Meng, Fu-Sheng Guo, Jun‐Liang Liu, Ji‐Dong Leng, Ming‐Liang Tong

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  28. A novel deep UV nonlinear optical crystal Ba3B6O11F2, with a new fundamental building block, B6O14 group

    Journal of Materials Chemistry · 2012-01-01

    Hongwei Yu, Hongping Wu, Shilie Pan, Zhihua Yang, Xin Su, Fangfang Zhang

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  29. Syntheses, structure, and magnetic properties of hexanuclear MnIII2MIII4 (M = Y, Gd, Tb, Dy) complexes

    Dalton Transactions · 2012-01-01

    Qi-Wei Xie, Ai‐Li Cui, Jun Tao, Hui‐Zhong Kou

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  30. Influencing the Size and Anion Selectivity of Dimeric Ln3+[15-Metallacrown-5] Compartments through Systematic Variation of the Host Side Chains and Central Metal

    Inorganic Chemistry · 2012-02-06

    Joseph Jankolovits, Choong‐Sun Lim, Gellert Mezei, Jeff W. Kampf, Vincent L. Pecoraro

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  31. Enhanced Guest Affinity and Enantioselectivity through Variation of the Gd3+[15-Metallacrown-5] Side Chain

    Inorganic Chemistry · 2012-05-02

    Joseph T. Grant, Joseph Jankolovits, Vincent L. Pecoraro

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  32. Insight into the structural versatility of the Ln(III)[15-metallacrown-5] platform by comparing analogs with Ni(II), Cu(II), and Zn(II) ring ions

    Polyhedron · 2012-08-31

    Joseph Jankolovits, Jeff W. Kampf, Vincent L. Pecoraro

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  33. Clarifying the Mechanism of Cation Exchange in Ca(II)[15-MCCu(II)Ligand-5] Complexes

    Inorganic Chemistry · 2012-10-17

    Choong‐Sun Lim, Matteo Tegoni, Tamás Jakusch, Jeff W. Kampf, Vincent L. Pecoraro

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  34. Syntheses and Structures of Terpyridine‐Metal Complexes

    Zeitschrift für anorganische und allgemeine Chemie · 2012-11-13

    Na Zhang, Juan Yang, Rui‐Xiang Hu, Man‐Bo Zhang

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  35. Stoichiometric diversity of Ni(ii) metallacrowns with β-alaninehydroxamic acid in aqueous solution

    Dalton Transactions · 2013-01-01

    Maurizio Remelli, Dimitri Bacco, Francesco Dallavalle, E. Lazzari, Nicola Marchetti, Matteo Tegoni

    Read original paper ↗ ·

  36. Synthesis, crystal structure and magnetic properties of dinuclear NiIILnIII complexes based on a flexible polydentate ligand

    Dalton Transactions · 2013-01-01

    Qi-Wei Xie, Shu‐Qi Wu, Cai‐Ming Liu, Ai-Li Cui, Hui‐Zhong Kou

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  37. Isolation of Elusive Tetranuclear and Pentanuclear M(II)–Hydroximate Intermediates in the Assembly of Lanthanide [15-Metallacrown-5] Complexes

    Inorganic Chemistry · 2013-04-11

    Joseph Jankolovits, Jeff W. Kampf, Vincent L. Pecoraro

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  38. Heterodinuclear MII–LnIII single molecule magnets constructed from exchange-coupled single ion magnets

    Dalton Transactions · 2014-01-01

    Qi-Wei Xie, Shu‐Qi Wu, Wen-Bo Shi, Cai‐Ming Liu, Ai-Li Cui, Hui‐Zhong Kou

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  39. Controllable Formation of Heterotrimetallic Coordination Compounds: Systematically Incorporating Lanthanide and Alkali Metal Ions into the Manganese 12-Metallacrown-4 Framework

    Inorganic Chemistry · 2014-01-13

    Michael R. Azar, Thaddeus T. Boron, Jacob C. Lutter, Connor I. Daly, Kelcie A. Zegalia, Ruthairat Nimthong, Gregory M. Ferrence, Mat­thias Zeller, Jeff W. Kampf, Vincent L. Pecoraro, Curtis M. Zaleski

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  40. Synthesis, crystal structures and magnetic properties of a novel fused 9-metallacrown-3 and a high/low spin [Fe(pao)2]3·H2O

    Inorganica Chimica Acta · 2014-03-14

    Dong Li, Ming-Li Liu

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  41. A novel [Na6Co6] metallacrown with [24-MCNa-6] periphery encapsulating the [12-MCCo-6] inner core: Synthesis, structure, and magnetic properties

    Inorganic Chemistry Communications · 2014-05-29

    Ming Fang, Tao Wang

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  42. Heterometallic Mixed3d-4fMetallacrowns: Structural Versatility, Luminescence, and Molecular Magnetism

    Comments on Inorganic Chemistry · 2014-12-31

    Chun Y. Chow, Evan R. Trivedi, Vincent L. Pecoraro, Curtis M. Zaleski

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  43. Facile carboxylate ligand variation of heterotrimetallic 12-metallacrown-4 complexes

    Polyhedron · 2015-09-12

    Jordan R. Travis, Mat­thias Zeller, Curtis M. Zaleski

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  44. Topological Aspects of 3d/4f Polynuclear Coordination Clusters

    Elsevier eBooks · 2016-01-01

    George E. Κostakis

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  45. Design of 2D Porous Coordination Polymers Based on Metallacrown Units

    Chemistry - A European Journal · 2016-03-08

    Corrado Atzeri, Luciano Marchiò, Chun Y. Chow, Jeff W. Kampf, Vincent L. Pecoraro, Matteo Tegoni

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  46. Metallacrowns: From Discovery to Potential Applications in Biomolecular Imaging

    Elsevier eBooks · 2016-09-23

    Tu N. Nguyen, V.L. Pecoraro

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  47. Four Mixed 3d-4f 12-Metallacrown-4 Complexes: Syntheses, Structures and Magnetic Properties

    Journal of Cluster Science · 2016-09-29

    Yaru Qin, Qian Gao, Yanmei Chen, Wei Liu, Feng Lin, Xiang-Fei Zhang, Yaping Dong, Yahong Li

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  48. Anion Encapsulation Drives the Formation of Dimeric GdIII[15-metallacrown-5]3+ Complexes in Aqueous Solution

    Inorganic Chemistry · 2017-04-17

    Carmelo Sgarlata, Alessandro Giuffrida, Evan R. Trivedi, Vincent L. Pecoraro, Giuseppe Arena

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  49. Stepwise Investigation of the Influences of Steric Groups versus Counterions To Target Cu/Dy Complexes

    Crystal Growth & Design · 2017-07-11

    Irina A. Kühne, Kieran Griffiths, Amy-Jayne Hutchings, Oliver P. E. Townrow, Andreas Eichhöfer, Christopher E. Anson, George E. Κostakis, Annie K. Powell

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  50. High Nuclearity Assemblies and One-Dimensional (1D) Coordination Polymers Based on Lanthanide–Copper 15-Metallacrown-5 Complexes (LnIII = Pr, Nd, Sm, Eu)

    Inorganic Chemistry · 2017-10-25

    Anna V. Pavlishchuk, Sergey V. Kolotilov, Mat­thias Zeller, S. E. Lofland, Laurence Kenneth Thompson, Anthony William Addison, Allen D. Hunter

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