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RESEARCH PAPER · CrystEngComm · 2015

A 5 RE 4 X[TO 4 ] 4 crystal growth and photoluminescence. Fluoride flux synthesis of sodium and potassium rare earth silicate oxyfluorides

Allison M. Latshaw, Branford O. Wilkins, Kendall D. Hughey, Jeongho Yeon, Derek E. Williams, T. Thao Tran, P. Shiv Halasyamani, Hans‐Conrad zur Loye

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A 5 RE 4 X[TO 4 ] 4 crystal growth and photoluminescence. Fluoride flux synthesis of sodium and potassium rare earth silicate oxyfluoridesOriginalInfluence of rare earth cation size on the crystal structure in rare earth silicates, Na2RESiO4(OH) (RE = Sc, Yb) and NaRESiO4 (RE = La, Yb)22Synthesis, structure, and polymorphism of A3LnSi2O7 (A=Na, K; Ln=Sm, Ho, Yb)12Intrinsic blue-white luminescence, luminescence color tunability, synthesis, structure, and polymorphism of K 3 YSi 2 O 734Flux Growth of [NaK6F][(UO2)3(Si2O7)2] and [KK6Cl][(UO2)3(Si2O7)2]: The Effect of Surface Area to Volume Ratios on Reaction Products37Single-crystal X-ray diffraction study of Cs2Er[Si6O14]F and Cs2Er[Si4O10]F7A5RE4X[TO4]4 crystal growth: Fluoride flux synthesis of Na5Ln4F[GeO4]4 (Ln=Pr, Nd), the first quaternary germanate oxyfluorides11Where Do New Materials Come From? Neither the Stork nor the Birds and the Bees! In Search of the Next “First Material”1Orthoborates LiCdRE 5 (BO 3 ) 6 (RE = Sm–Lu and Y) with Rare-Earth Ions on a Triangular Lattice: Synthesis, Crystal Structure, and Optical and Magnetic Properties24Observation of Intense X-ray Scintillation in a Family of Mixed Anion Silicates, Cs3RESi4O10F2 (RE = Y, Eu–Lu), Obtained via an Enhanced Flux Crystal Growth Technique59Crystal chemistry of compounds with lanthanide based microporous heteropolyhedral frameworks: Synthesis, crystal structures, and luminescence properties of novel potassium cerium and erbium silicates18Cs3REIIIGe3O9 (RE = Pr, Nd, and Sm–Yb) and Cs8TbIII2TbIVGe9O27: A Rare Example of a Mixed-Valent Tb(III)/Tb(IV) Oxide20Observation of the Same New Sheet Topology in Both the Layered Uranyl Oxide-Phosphate Cs11[(UO2)12(PO4)3O13] and the Layered Uranyl Oxyfluoride-Phosphate Rb11[(UO2)12(PO4)3O12F2] Prepared by Flux Crystal Growth13Polymorphism and photoluminescence properties of K3ErSi2O72Flux crystal growth of a new BaTa2O6 polymorph, and of the novel tantalum oxyfluoride salt inclusion phase [Ba3F]Ta4O12F: Flux dependent phase formation5Crystal structure of K3EuSi2O71Rb1.66Cs1.34Tb[Si5.43Ge0.57O15]·H2O, a New Member of the OD-Family of Natural and Synthetic Layered Silicates: Topology-Symmetry Analysis and Structure Prediction6Low-temperature phase transition and magnetic properties of K3YbSi2O73Synthesis, structure and property studies of a new series of rare earth (Ce, Tb) bismuth silicates2Luminescence and Scintillation in the Niobium Doped Oxyfluoride Rb4Ge5O9F6:Nb8Crystal structure determination and characterization of Sm3SiO5F32RE(OH) 2 NO 3 (RE = Tb, Dy, Ho, and Er): Synthesis and Nonlinear Optical Properties of Water-Resistant Lanthanide Hydroxide Nitrates15Comparative Study on Crystal Structures and Synthetic Techniques of Ternary Hafnium/Zirconium Fluorides7Rb2Ln[Si2O6]F (Ln = Y, Eu–Lu): Flux Synthesis, Structure Determination, and DFT-Calculated Formation Enthalpies of a Series of Mixed-Anion Rare Earth Cyclosilicates2Molten Salt Flux Synthesis of Two New Alkali Rare Earth Silicate Fluorides: Rb3sc2[Si4o12]F and Rb2sm[Si4o10]F0Large cryogenic magnetocaloric effect in Na5Gd4F(SiO4)46Molten salt flux synthesis of two new alkali rare earth silicate fluorides: Rb3Sc2[Si4O12]F and Rb2Sm[Si4O10]F1Achievement of an ultra-broadband deep red phosphor K3Ca0.3Y0.7Si2O7:Eu2+ (phase 1) for phytochrome matching plant-lighting12Synthesis of Mixed Anion Rare Earth Sulfate Fluorides LnSO4F·H2O (Ln = Nd, Tb, Dy, and Ho) and LnSO4F (Ln = Tb, Dy, and Ho)5A Mixed-Anion Design Approach for High-Efficiency X-ray Scintillators: A Study of KLn(SO4)F2 (Ln = Eu, Gd, Tb, Dy, Ho, and Tm)3

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  1. Influence of rare earth cation size on the crystal structure in rare earth silicates, Na2RESiO4(OH) (RE = Sc, Yb) and NaRESiO4 (RE = La, Yb)

    Solid State Sciences · 2015-11-25

    Allison M. Latshaw, Branford O. Wilkins, W. Michael Chance, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  2. Synthesis, structure, and polymorphism of A3LnSi2O7 (A=Na, K; Ln=Sm, Ho, Yb)

    Journal of Solid State Chemistry · 2015-12-17

    Allison M. Latshaw, Jeongho Yeon, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  3. Intrinsic blue-white luminescence, luminescence color tunability, synthesis, structure, and polymorphism of K 3 YSi 2 O 7

    CrystEngComm · 2016-01-01

    Allison M. Latshaw, Gregory W. Morrison, Karl D. zur Loye, Alexis R. Myers, Mark D. Smith, Hans‐Conrad zur Loye

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  4. Flux Growth of [NaK6F][(UO2)3(Si2O7)2] and [KK6Cl][(UO2)3(Si2O7)2]: The Effect of Surface Area to Volume Ratios on Reaction Products

    Crystal Growth & Design · 2016-02-02

    Gregory W. Morrison, Hans‐Conrad zur Loye

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  5. Single-crystal X-ray diffraction study of Cs2Er[Si6O14]F and Cs2Er[Si4O10]F

    Zeitschrift für Kristallographie - Crystalline Materials · 2016-03-01

    Predrag Dabić, Volker Kahlenberg, Daniela Schmidmair, Aleksandar Kremenović, Predrag J. Vulić

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  6. A5RE4X[TO4]4 crystal growth: Fluoride flux synthesis of Na5Ln4F[GeO4]4 (Ln=Pr, Nd), the first quaternary germanate oxyfluorides

    Journal of Solid State Chemistry · 2016-04-29

    Allison M. Latshaw, Branford O. Wilkins, Gregory W. Morrison, Mark D. Smith, Hans‐Conrad zur Loye

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  7. Where Do New Materials Come From? Neither the Stork nor the Birds and the Bees! In Search of the Next “First Material”

    Scholar Commons (University of South Carolina) · 2017-01-01

    Gregory W. Morrison, Dileka Abeysinghe, Justin B. Felder, Shani Egodawatte, Timothy Ferreira, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  8. Orthoborates LiCdRE 5 (BO 3 ) 6 (RE = Sm–Lu and Y) with Rare-Earth Ions on a Triangular Lattice: Synthesis, Crystal Structure, and Optical and Magnetic Properties

    Inorganic Chemistry · 2017-06-29

    Mingjun Xia, Kun Zhai, Jun Lü, Young Sun, Rukang K. Li

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  9. Observation of Intense X-ray Scintillation in a Family of Mixed Anion Silicates, Cs3RESi4O10F2 (RE = Y, Eu–Lu), Obtained via an Enhanced Flux Crystal Growth Technique

    Journal of the American Chemical Society · 2017-09-19

    Gregory W. Morrison, Allison M. Latshaw, Nicholas R. Spagnuolo, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  10. Crystal chemistry of compounds with lanthanide based microporous heteropolyhedral frameworks: Synthesis, crystal structures, and luminescence properties of novel potassium cerium and erbium silicates

    Microporous and Mesoporous Materials · 2019-04-08

    Sergey M. Aksenov, Stephanie A. Mackley, Dina V. Deyneko, Vladimir K. Taroev, В. Л. Таусон, Рамиза Кераровна Расцветаева, Peter Carman Burns

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  11. Cs3REIIIGe3O9 (RE = Pr, Nd, and Sm–Yb) and Cs8TbIII2TbIVGe9O27: A Rare Example of a Mixed-Valent Tb(III)/Tb(IV) Oxide

    Inorganic Chemistry · 2019-06-18

    Gregory W. Morrison, Nicholas R. Spagnuolo, S. Karakalos, Hans‐Conrad zur Loye

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  12. Observation of the Same New Sheet Topology in Both the Layered Uranyl Oxide-Phosphate Cs11[(UO2)12(PO4)3O13] and the Layered Uranyl Oxyfluoride-Phosphate Rb11[(UO2)12(PO4)3O12F2] Prepared by Flux Crystal Growth

    Frontiers in Chemistry · 2019-08-21

    Christian A. Juillerat, Vancho Kocevski, Theodore M. Besmann, Hans‐Conrad zur Loye

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  13. Polymorphism and photoluminescence properties of K3ErSi2O7

    Acta Crystallographica Section C Structural Chemistry · 2019-09-25

    Predrag Dabić, Marko G. Nikolić, Sabina Kovač, Aleksandar Kremenović

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  14. Flux crystal growth of a new BaTa2O6 polymorph, and of the novel tantalum oxyfluoride salt inclusion phase [Ba3F]Ta4O12F: Flux dependent phase formation

    Journal of Solid State Chemistry · 2020-10-27

    Ceren Kütahyalı Aslani, Vladislav V. Klepov, Hans‐Conrad zur Loye

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  15. Crystal structure of K3EuSi2O7

    Journal of the Serbian Chemical Society · 2021-01-01

    Sabina Kovač, Predrag Dabić, Aleksandar Kremenović

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  16. Rb1.66Cs1.34Tb[Si5.43Ge0.57O15]·H2O, a New Member of the OD-Family of Natural and Synthetic Layered Silicates: Topology-Symmetry Analysis and Structure Prediction

    Minerals · 2021-04-09

    Anastasiia Topnikova, Elena L. Belokoneva, Olga V. Dimitrova, Anatoly S. Volkov, Dina V. Deyneko

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  17. Low-temperature phase transition and magnetic properties of K3YbSi2O7

    Acta Crystallographica Section B Structural Science Crystal Engineering and Materials · 2021-07-23

    Predrag Dabić, Volker Kahlenberg, Biljana Krüger, Marko V. Rodić, Sabina Kovač, J. Blanuša, Zvonko Jagličić, Ljiljana Karanović, Václav Petříček, Aleksandar Kremenović

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  18. Synthesis, structure and property studies of a new series of rare earth (Ce, Tb) bismuth silicates

    Journal of Solid State Chemistry · 2021-09-11

    Ce Tao, Jianqiang Li, Rukang K. Li

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  19. Luminescence and Scintillation in the Niobium Doped Oxyfluoride Rb4Ge5O9F6:Nb

    Inorganics · 2022-06-16

    Darren Carone, Vladislav V. Klepov, Scott T. Misture, Joseph C. Schaeperkoetter, Luiz Gustavo Jacobsohn, Mina Aziziha, Juliano Schorne Pinto, Stuart A. J. Thomson, Adrian T. Hines, Theodore M. Besmann, Hans‐Conrad zur Loye

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  20. Crystal structure determination and characterization of Sm3SiO5F3

    Zeitschrift für Naturforschung B · 2022-08-08

    Fabian Zimmerhofer, Felix Netzer, Martina Tribus, Hubert Huppertz

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  21. RE(OH) 2 NO 3 (RE = Tb, Dy, Ho, and Er): Synthesis and Nonlinear Optical Properties of Water-Resistant Lanthanide Hydroxide Nitrates

    Inorganic Chemistry · 2022-11-01

    Min Chen, Zhengli Liang, Xiaoxiao Wang, Jiehua Li, Xingguo Chen, Xingxing Jiang, Zheshuai Lin, Zhen Ma, Hongming Liu

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  22. Comparative Study on Crystal Structures and Synthetic Techniques of Ternary Hafnium/Zirconium Fluorides

    Inorganic Chemistry · 2023-07-18

    Navindra Keerthisinghe, Gyanendra B. Ayer, Mark D. Smith, Hans‐Conrad zur Loye

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  23. Rb2Ln[Si2O6]F (Ln = Y, Eu–Lu): Flux Synthesis, Structure Determination, and DFT-Calculated Formation Enthalpies of a Series of Mixed-Anion Rare Earth Cyclosilicates

    Inorganic Chemistry · 2023-10-30

    Hunter B. Tisdale, Amir Mofrad, Gregory W. Morrison, Theodore M. Besmann, Hans‐Conrad zur Loye

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  24. Molten Salt Flux Synthesis of Two New Alkali Rare Earth Silicate Fluorides: Rb3sc2[Si4o12]F and Rb2sm[Si4o10]F

    SSRN Electronic Journal · 2024-01-01

    Hans‐Conrad zur Loye, Hunter B. Tisdale

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  25. Large cryogenic magnetocaloric effect in Na5Gd4F(SiO4)4

    Cryogenics · 2024-10-01

    Zuhua Chen, Shilin Yu, Guochun Zhang, Changkun Wang, Jiahao Gao, Yicai Zhang, Yanan Zhao, Zhenxing Li, Jun Shen, Heng Tu

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  26. Molten salt flux synthesis of two new alkali rare earth silicate fluorides: Rb3Sc2[Si4O12]F and Rb2Sm[Si4O10]F

    Solid State Sciences · 2024-12-07

    Hunter B. Tisdale, Hans‐Conrad zur Loye

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  27. Achievement of an ultra-broadband deep red phosphor K3Ca0.3Y0.7Si2O7:Eu2+ (phase 1) for phytochrome matching plant-lighting

    Journal of Rare Earths · 2025-01-28

    Xiaoshuai Zhang, Xi Wang, Tao Yin, Xuping Han, Panlai Li, Xiaoyan Yu, Zixuan Wang, Zixuan Wang, Chengrun Liu, Zhijun Wang, Zhijun Wang

    Read original paper ↗ ·

  28. Synthesis of Mixed Anion Rare Earth Sulfate Fluorides LnSO4F·H2O (Ln = Nd, Tb, Dy, and Ho) and LnSO4F (Ln = Tb, Dy, and Ho)

    Crystal Growth & Design · 2025-03-27

    Lakshani W. Masachchi, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  29. A Mixed-Anion Design Approach for High-Efficiency X-ray Scintillators: A Study of KLn(SO4)F2 (Ln = Eu, Gd, Tb, Dy, Ho, and Tm)

    Inorganic Chemistry · 2025-08-12

    Lakshani W. Masachchi, Patrick Belt, Nilah Whitfield, Mark D. Smith, Gopabandhu Panigrahi, Gregory W. Morrison, Luiz Gustavo Jacobsohn, Hans‐Conrad zur Loye

    Read original paper ↗ ·
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