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RESEARCH PAPER · Chem · 2021

Design principles for intrinsically circular polymers with tunable properties

Changxia Shi, Liam T. Reilly, Sai Phani Kumar Vangala, Matthew W. Coile, Scott R. Nicholson, Linda J. Broadbelt, Gregg T. Beckham, Eugene Y.‐X. Chen

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Design principles for intrinsically circular polymers with tunable propertiesOriginalAccess to high-molecular-weight poly(γ-butyrolactone) by using simple commercial catalysts13Closed-loop chemical recycling of poly(ε-caprolactone) by tuning reaction parameters50Depolymerizable semi-fluorinated polymers for sustainable functional materials21Facile synthesis of eight-membered cyclic(ester-amide)s and their organocatalytic ring-opening polymerizations9Recent Advances in Monomer Design for Recyclable Polymers37Closing the “One Monomer–Two Polymers–One Monomer” Loop via Orthogonal (De)polymerization of a Lactone/Olefin Hybrid146Advancing the Development of Recyclable Aromatic Polyesters by Functionalization and Stereocomplexation112Advancing the Development of Recyclable Aromatic Polyesters by Functionalization and Stereocomplexation14Redesigned Hybrid Nylons with Optical Clarity and Chemical Recyclability127Critical advances and future opportunities in upcycling commodity polymers1324Stereoselective Ring-Opening Polymerization of Lactones with a Fused Ring Leading to Semicrystalline Polyesters39Zinc-Mediated Allylation-Lactonization One-Pot Reaction to Methylene Butyrolactones: Renewable Monomers for Sustainable Acrylic Polymers with Closed-Loop Recyclability27Chemical recycling to monomers: Industrial Bisphenol‐A‐Polycarbonates to novel aliphatic polycarbonate materials80Closed-Loop Recyclable Aliphatic Poly(ester-amide)s with Tunable Mechanical Properties51Regulating the Thermodynamics and Thermal Properties of Depolymerizable Polycyclooctenes through Substituent Effects14Polythioesters Prepared by Ring‐Opening Polymerization of Cyclic Thioesters and Related Monomers70Resource Cycling: Application of Anaerobic Utilization Methods3Polyolefin Innovations toward Circularity and Sustainable Alternatives96Enabling resource circularity through thermo-catalytic and solvent-based conversion of waste plastics49Recyclable Sulfur-Rich Polymers with Enhanced Thermal, Mechanical, and Optical Performance44Mixed plastics waste valorization through tandem chemical oxidation and biological funneling635A circular polyester platform based on simple gem-disubstituted valerolactones175Strong and Tough Supramolecular Covalent Adaptable Networks with Room‐Temperature Closed‐Loop Recyclability222Depolymerization of Polymethacrylates by Iron ATRP112Recyclable Biomass-Derived Polyethylene-Like Materials as Functional Coatings for Commercial Fabrics: Toward Upcycling of Waste Textiles21Light-accelerated depolymerization catalyzed by Eosin Y108Herbaceous plants-derived hydroxycinnamic units for constructing recyclable and controllable copolyesters24Naphthalene engineering of chemically recyclable polyesters with enhanced thermal and mechanical properties15Techno-economic analysis and life cycle assessment of mixed plastic waste gasification for production of methanol and hydrogen139Advances in the Synthesis of Chemically Recyclable Polymers50Recyclable polythioesters and polydisulfides with near-equilibrium thermodynamics and dynamic covalent bonds29Endowing Polythioester Vitrimer with Intrinsic Crystallinity and Chemical Recyclability28Sustainable Polythioesters via Thio(no)lactones: Monomer Synthesis, Ring‐Opening Polymerization, End‐of‐Life Considerations, and Industrial Perspectives46Chemical upcycling of poly(lactide) plastic waste to lactate ester, lactide and new poly(lactide) under Mg-catalysis condition32Emerging Trends in Closed‐Loop Recycling Polymers: Monomer Design and Catalytic Bulk Depolymerization48Ring-Opening Polymerization for the Goal of Chemically Recyclable Polymers117Converting Non‐strained γ‐Valerolactone and Derivatives into Sustainable Polythioesters via Isomerization‐driven Cationic Ring‐Opening Polymerization of Thionolactone Intermediate52Converting Non‐strained γ‐Valerolactone and Derivatives into Sustainable Polythioesters via Isomerization‐driven Cationic Ring‐Opening Polymerization of Thionolactone Intermediate6Current Challenges and Perspectives in CO2-Based Polymers112Installing Controlled Stereo-Defects Yields Semicrystalline and Biodegradable Poly(3-Hydroxybutyrate) with High Toughness and Optical Clarity69Mechanochemical Degradation and Recycling of Synthetic Polymers23Mechanochemical Degradation and Recycling of Synthetic Polymers167Chemistry that allows plastic recycling7Performance‐Advantaged Stereoregular Recyclable Plastics Enabled by Aluminum‐Catalytic Ring‐Opening Polymerization of Dithiolactone60Performance‐Advantaged Stereoregular Recyclable Plastics Enabled by Aluminum‐Catalytic Ring‐Opening Polymerization of Dithiolactone10Hybrid Monomer Design Synergizing Property Trade‐offs in Developing Polymers for Circularity and Performance63Hybrid Monomer Design Synergizing Property Trade‐offs in Developing Polymers for Circularity and Performance4A Simple, Selective, and General Catalyst for Ring Closing Depolymerization of Polyesters and Polycarbonates for Chemical Recycling111A Simple, Selective, and General Catalyst for Ring Closing Depolymerization of Polyesters and Polycarbonates for Chemical Recycling23Dynamic crosslinking compatibilizes immiscible mixed plastics245Dual Recycling of Depolymerization Catalyst and Biodegradable Polyester that Markedly Outperforms Polyolefins89Dual Recycling of Depolymerization Catalyst and Biodegradable Polyester that Markedly Outperforms Polyolefins8Precision native polysaccharides from living polymerization of anhydrosugars75Kinetic Monte Carlo Convergence Demands for Thermochemical Recycling Kinetics of Vinyl Polymers with Dominant Depropagation10Mono-material product design with bio-based, circular, and biodegradable polymers49Insights into substitution strategy towards thermodynamic and property regulation of chemically recyclable polymers84Synthesis of Sulfur/Selenium-containing Polyester with Recyclability and Controllable Hydrophilicity and Glass Transition Temperature7Chemically recyclable oxygen-protective polymers developed by ring-opening metathesis homopolymerization of cyclohexene derivatives26Living/Controlled Anionic Polymerization of Glycolide in Fluoroalcohols: Toward Sustainable Bioplastics50Regulating cationic polymerization: From structural control to life cycle management51Emerging Trends in the Chemistry of End-to-End Depolymerization69Circular plastics technologies: depolymerization of polymers into parent monomers5One-pot upcycling strategy achieved in Bi-continuous thermal conductive polymer composites8Symbolic semantic design of industrial products based on Big data technology0Current Advances and Challenges in Chemical Recycling of Polymeric Materials5Chemically recyclable polyolefin-like multiblock polymers201PolyID: Artificial Intelligence for Discovering Performance-Advantaged and Sustainable Polymers56Copolymerization Involving Sulfur-Containing Monomers102Optimización de las propiedades de tenacidad e impacto de formulaciones de ácido poliláctico (PLA), mediante mezclas con polímeros flexibles y optimización de los sistemas de compatibilización0High- T g PLA copolymers via base-catalyzed transesterification of PLA with 2,5,7-trioxabicyclo[2.2.2]octan-6-one10Recent advances in polyhydroxyalkanoates degradation and chemical recycling88Advances in catalytic chemical recycling of synthetic textiles43Closed-loop recyclable polymers: from monomer and polymer design to the polymerization–depolymerization cycle106Recyclable, Reprocessable, Anticorrosive, and Hydrolysis-Resistant Long-Chain Aliphatic Polycarbonates as Polyethylene-like Materials15Stereoselective Ring‐opening Polymerization of S‐Carboxyanhydrides Using Salen Aluminum Catalysts: A Route to High‐Isotactic Functionalized Polythioesters1Stereoselective Ring‐opening Polymerization of S‐Carboxyanhydrides Using Salen Aluminum Catalysts: A Route to High‐Isotactic Functionalized Polythioesters14From epoxides and carbon dioxide to polycarbonates: synthesis, properties and applications27Recycled polymer: Green roads for polyester plastics65Chemically Recyclable Unnatural (1→6)-Polysaccharides from Cellulose-Derived Levoglucosenone and Dihydrolevoglucosenone10Self-Immolative Polymers: From Synthesis to Applications31Ring-Opening Polymerization of Lactones to Prepare Closed-Loop Recyclable Polyesters116Redesigned Nylon 6 Variants with Enhanced Recyclability, Ductility, and Transparency3Redesigned Nylon 6 Variants with Enhanced Recyclability, Ductility, and Transparency40Accessing Chemically Recyclable Polyamides with TunableProperties via Geminal Dimethyl Substitution1Accessing chemically recyclable polyamides via geminal dimethyl substitution12Enabling Closed‐Loop Circularity of “Non‐Polymerizable” α, β‐Conjugated Lactone Towards High‐Performance Polyester with the Assistance of Cyclopentadiene23Enabling Closed‐Loop Circularity of “Non‐Polymerizable” α, β‐Conjugated Lactone Towards High‐Performance Polyester with the Assistance of Cyclopentadiene2Recyclable and (Bio)degradable Polyesters in a Circular Plastics Economy400Topology-Accelerated and Selective Cascade Depolymerization of Architecturally Complex Polyesters19Understanding ceiling temperature as a predictive design parameter for circular polymers28Heteroatom Substitution Strategy Modulates Thermodynamics Towards Chemically Recyclable Polyesters and Monomeric Unit Sequence by Temperature Switching3Heteroatom Substitution Strategy Modulates Thermodynamics Towards Chemically Recyclable Polyesters and Monomeric Unit Sequence by Temperature Switching28Chemically Recyclable, High Molar Mass Polyoxazolidinones via Ring-Opening Metathesis Polymerization14Bio-based lactone acrylic plastics with performance and recyclability advantages10Ring‐Opening Copolymerization of Biorenewable δ‐Caprolactone with trans‐Hexahydro ‐(4,5)‐benzofuranone toward Closed‐Loop Recyclable Copolyesters and Their Application as Pressure‐Sensitive Adhesives†9Positioning dynamic polymeric materials within the modern polymer economy: From application to recycling and circularity10Thermally Stable and Chemically Recyclable Poly(ketal-ester)s Regulated by Floor Temperature57Closed‐Loop Recycling of Mixed Plastics of Polyester and CO2‐Based Polycarbonate to a Single Monomer33Closed‐Loop Recycling of Mixed Plastics of Polyester and CO2‐Based Polycarbonate to a Single Monomer3Recent advances in the chemical recycling of polyesters44Chemical closed-loop recycling of polymers realized by monomer design19Chemical Recycling of Poly(butylene terephthalate) into Poly(ethylene brassylate-co-butylene terephthalate) with Tunable Thermal, Mechanical and Biodegradable Properties20Encoding Circularity in Polydiketoenamine Thermoplastics via Oxy-Functionalization1Toward a Circular Bioeconomy: Designing Microbes and Polymers for Biodegradation27Access to bromo-functionalized polyester by ring-opening polymerization of a bridged bicyclic lactone and application for grafted copolymers1Terpenoid-based high-performance polyester with tacticity-independent crystallinity and chemical circularity21Synthesis of long-chain aliphatic poly(β-thioester)s via thiol-Michael polyaddition and their applications in noble metal recovery and information encryption4Ring-Opening Polymerization of α-Diazo Lactones: Access to Diazo-Containing Polyesters and Their Post-Polymerization Modifications7Photochemical [2 + 2] Cycloaddition Enables the Synthesis of Highly Thermally Stable and Acid/Base-Resistant Polyesters from a Nonpolymerizable α,β-Conjugated Valerolactone1Chemical Recycling of Poly(cyclohexene carbonate)s via Synergistic Catalysis7New sustainable polymers with on-demand depolymerization property88High Molecular Weight Semicrystalline Substituted Polycyclohexene From Alternating Copolymerization of Butadiene and Methacrylate and Its Ambient Depolymerization23Unraveling the Mechanism of Catalyzed Melt-Phase Polyester Depolymerization via Studies of Kinetics and Model Reactions17Circular Polyesters Based on Lactones4Tackling the Thermodynamic Stability of Low-Ceiling Temperature Polymers for the Preparation of Tough and Chemically Recyclable Thermoplastic Polyurethane-Urea Elastomers11Closed-Loop Chemical Recycling of a Biobased Poly(oxanorbornene-fused γ-butyrolactone)22Self‐Immolative Polymers Derived from Renewable Resources via Thiol–Ene Chemistry**4Self‐Immolative Polymers Derived from Renewable Resources via Thiol–Ene Chemistry**4Adaptive laboratory evolution and genetic engineering improved terephthalate utilization in Pseudomonas putida KT244030Development of a functionalized polystyrene platform from packaging waste via Friedel-Craft acylation7Solvent‐Free Chemical Recycling of Polyesters and Polycarbonates by Magnesium‐Based Lewis Acid Catalyst36Solvent‐Free Chemical Recycling of Polyesters and Polycarbonates by Magnesium‐Based Lewis Acid Catalyst10A hindered-urea vitrimer: recyclable for circular use and upcyclable for rechargeable batteries12Circular polyester design by gem -heterodisubstitution: valerolactone-based polymers with high ductility and excellent strength4Hydrogenative Depolymerization of Polyesters Catalyzed by a PN3-Ruthenium Complex Using Both H2 and EtOH as Hydrogen Sources0Implementing a sulfur-substitution approach toward a high-performance recyclable polythioester9Synergistic engineering of poly(3-hydroxybutyrate) architecture and stereomicrostructure achieves enhanced material properties4Polymer-based antimicrobial strategies for periodontitis8Screening Green Solvents for Multilayer Plastic Film Recycling Processes15Circularity in polydiketoenamine thermoplastics via control over reactive chain conformation4Circular Polymer Designed by Regulating Entropy: Spiro-Valerolactone-Based Polyesters with High Gas Barriers and Adhesion Strength22Toughening Poly(lactic acid) without Compromise – Statistical Copolymerization with a Bioderived Bicyclic Lactone23Pushing forward kinetic modeling tools for polymer circularity design and recycling15Organocatalytic Ring-Opening (Co)polymerization of Six-Membered Monothiocarbonates for the Synthesis of Recyclable Poly(monothiocarbonate)s6Harnessing Non-Thermal External Stimuli for Polymer Recycling23Visible light–triggered depolymerization of commercial polymethacrylates128Looking into the Quest for Stereoselective Ring-Opening Polymerization of Racemic Lactide with Chiral Organocatalysts12Immortal depolymerization of chemical recycling of CO2-Sourced poly (cyclohexene carbonate) to monomers: An overlooked effect of molecular weight1Mechanistic kinetic Monte Carlo modeling of the synthesis of hyperbranched polyesters1Renewable Fluorescent Liquid Crystal Elastomers for Potential Use in Temperature Indicator During Short-time Vaccine Transportation3Tunable and Degradable Dynamic Thermosets from Compatibilized Polyhydroxyalkanoate Blends10Organocatalyst Catalyzed Ring Opening Polymerization of O(S)‐Carboxyanhydride to Produce High Performance Poly(thio)esters0Organocatalyzed Ring‐Opening Polymerization of Cyclic Esters Toward Degradable Polymers0A General and Mild Two‐Step Strategy Using Bioderived Diols and CO 2 for Chemically Recyclable Polycarbonates and Closed‐Loop CO 2 Fixation16A General and Mild Two‐Step Strategy Using Bioderived Diols and CO 2 for Chemically Recyclable Polycarbonates and Closed‐Loop CO 2 Fixation3Chemically and Mechanically Recyclable Vitrimers from Carbon Dioxide-Based Polycarbonates12Bio‐Sourced 4‐Aryl‐1,2‐Dithiolanes for Recyclable Poly(disulfide)s with High Performance1Bio‐Sourced 4‐Aryl‐1,2‐Dithiolanes for Recyclable Poly(disulfide)s with High Performance12En Route Toward Sustainable Polycarbonates via Large Cyclic Carbonates11Crystallization/Precipitation Driven Nonequilibrium Ring‐Opening Polymerization of Thiovalerolactone Toward Closed‐Loop Recyclable Polythioester with Excellent Barrier Properties2

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  1. Access to high-molecular-weight poly(γ-butyrolactone) by using simple commercial catalysts

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  2. Closed-loop chemical recycling of poly(ε-caprolactone) by tuning reaction parameters

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  3. Depolymerizable semi-fluorinated polymers for sustainable functional materials

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  4. Facile synthesis of eight-membered cyclic(ester-amide)s and their organocatalytic ring-opening polymerizations

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  11. Stereoselective Ring-Opening Polymerization of Lactones with a Fused Ring Leading to Semicrystalline Polyesters

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  12. Zinc-Mediated Allylation-Lactonization One-Pot Reaction to Methylene Butyrolactones: Renewable Monomers for Sustainable Acrylic Polymers with Closed-Loop Recyclability

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  35. Emerging Trends in Closed‐Loop Recycling Polymers: Monomer Design and Catalytic Bulk Depolymerization

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  36. Ring-Opening Polymerization for the Goal of Chemically Recyclable Polymers

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  37. Converting Non‐strained γ‐Valerolactone and Derivatives into Sustainable Polythioesters via Isomerization‐driven Cationic Ring‐Opening Polymerization of Thionolactone Intermediate

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  38. Converting Non‐strained γ‐Valerolactone and Derivatives into Sustainable Polythioesters via Isomerization‐driven Cationic Ring‐Opening Polymerization of Thionolactone Intermediate

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  39. Current Challenges and Perspectives in CO2-Based Polymers

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  40. Installing Controlled Stereo-Defects Yields Semicrystalline and Biodegradable Poly(3-Hydroxybutyrate) with High Toughness and Optical Clarity

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  41. Mechanochemical Degradation and Recycling of Synthetic Polymers

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  42. Mechanochemical Degradation and Recycling of Synthetic Polymers

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  43. Chemistry that allows plastic recycling

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  44. Performance‐Advantaged Stereoregular Recyclable Plastics Enabled by Aluminum‐Catalytic Ring‐Opening Polymerization of Dithiolactone

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  45. Performance‐Advantaged Stereoregular Recyclable Plastics Enabled by Aluminum‐Catalytic Ring‐Opening Polymerization of Dithiolactone

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  46. Hybrid Monomer Design Synergizing Property Trade‐offs in Developing Polymers for Circularity and Performance

    Angewandte Chemie International Edition · 2023-04-18

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  47. Hybrid Monomer Design Synergizing Property Trade‐offs in Developing Polymers for Circularity and Performance

    Angewandte Chemie · 2023-04-19

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  48. A Simple, Selective, and General Catalyst for Ring Closing Depolymerization of Polyesters and Polycarbonates for Chemical Recycling

    Angewandte Chemie International Edition · 2023-04-24

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  49. A Simple, Selective, and General Catalyst for Ring Closing Depolymerization of Polyesters and Polycarbonates for Chemical Recycling

    Angewandte Chemie · 2023-04-24

    Connor F. Gallin, Won‐Woo Lee, Jeffery A. Byers

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  50. Dynamic crosslinking compatibilizes immiscible mixed plastics

    Nature · 2023-04-26

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