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RESEARCH PAPER · The Journal of Physical Chemistry C · 2020

Controlling Particle Size and Phase Purity of “Single-Crystal” LiNi0.5Mn1.5O4 in Molten-Salt-Assisted Synthesis

Weina Wang, Dechao Meng, Guannan Qian, Sijie Xie, Yanbin Shen, Liwei Chen, Xiaomin Li, Qunli Rao, Haiying Che, Jiabing Liu, Yu‐Shi He, Zi‐Feng Ma, Linsen Li

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Controlling Particle Size and Phase Purity of “Single-Crystal” LiNi0.5Mn1.5O4 in Molten-Salt-Assisted SynthesisOriginalVisualization of Structural Heterogeneities in Particles of Lithium Nickel Manganese Oxide Cathode Materials by Ptychographic X-ray Absorption Fine Structure21Effect of Thin Film to Boost the Electrochemical Properties of LiMn1.5Ni0.5O419Identifying Element-Modulated Reactivity and Stability of the High-Voltage Spinel Cathode Materials via In Situ Time-Resolved X-Ray Diffraction2Single‐Crystalline Cathodes for Advanced Li‐Ion Batteries: Progress and Challenges111Submicron single‐crystalline LiNi 0.5 Mn 1.5 O 4 cathode with modulated Mn 3+ content enabling high capacity and fast lithium‐ion kinetics31Role of carbon nanotube on preparation of spinel LiNi0.5Mn1.5O4 cathode5Tuning the structural disordering in hierarchical LiNi0.5Mn1.5O4 microrods for stable high-rate electrode performance25On the Composition of LiNi 0.5 Mn 1.5 O 4 Cathode Active Materials96Controlled crystal growth and electrode formation of single crystalline Li(Ni,Mn)2O4 spinel cathodes4The influence of different drying methods on the properties of LiNi0.5Mn1.5O4 material0Molten Salt Synthesis of Multifaceted Pure-Phase Spinel LiNi 0.5 Mn 1.5 O 4 Platelets12Correlative Raman imaging and scanning electron microscopy for advanced functional materials characterization41Effect of washing on nickel-rich NCMs: methodology to quantify the lithium/proton-exchange kinetics, the inserted protons, and the structural changes17High‐Voltage Spinel Cathode Materials: Navigating the Structural Evolution for Lithium‐Ion Batteries119Synthesis of Monodisperse and Discrete Ultra-High Nickel LiNi0.97Co0.02Mn0.01O2 Octahedral Single Crystals via Single Crystal Intermediates for Li-Ion Batteries8Controllable preparation of chamfered LiNi0.5Mn1.5O4 monocrystal cathode materials by trace Ti atoms replacing Mn and electrochemical properties3Towards High‐Performance Li‐Rich Cathode Materials: from Morphology Design to Electronic Structure Modulation15Single-crystal Ni-rich-doped LiNi 0.59 Co 0.3 Ti 0.1 Al 0.01 O 2 (NCTA) cathode materials: effect of annealing temperature on the structure, morphology, and electrochemical performance1Strategies toward high-energy-density Co-free lithium nickel manganese oxide: from crystal structure control to flexible configuration design22KOH-Assisted Molten Salt Route to High-Performance LiNi0.5Mn1.5O4 Cathode Materials0Breaking the Cycle of Heterogeneous Degradation: Surface-Targeted Protection for Ni-Rich Cathodes in Practical High-Energy Batteries21Molten salt synthesis of a single-crystal LiNi0.5Mn1.5O4 cathode with an in situ constructed stable interface for 4.8 V-class all-solid-state batteries5Titania-based organometallic super-hydrophobic finishing of cellulose fabric for potential organic/aqueous phase separation application1Mg Substitution Improves the Surface Stability of High‐Voltage Spinel Cathodes under Accelerated Aging Conditions2Mitigating the Rock‐Salt Phase Transformation in Disordered LNMO Through Synergetic Solid‐State AlF 3 /LiF Modifications1Harnessing Metastable Byproducts: A Dual-Regulation Strategy for Intrinsically Stable High-Voltage Spinel Cathodes0

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  1. Visualization of Structural Heterogeneities in Particles of Lithium Nickel Manganese Oxide Cathode Materials by Ptychographic X-ray Absorption Fine Structure

    The Journal of Physical Chemistry Letters · 2021-06-17

    Hideshi Uematsu, Nozomu Ishiguro, Masaki Abe, Shuntaro Takazawa, Jungmin Kang, Eiji Hosono, Duong‐Nguyen Nguyen, Hieu‐Chi Dam, Masashi Okubo, Yukio Takahashi

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  2. Effect of Thin Film to Boost the Electrochemical Properties of LiMn1.5Ni0.5O4

    Energy & Fuels · 2021-08-25

    Wenbin Luo, Zi‐Sheng Chao, Shuangxing Lu, Yanhui Liu, Jincheng Fan

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  3. Identifying Element-Modulated Reactivity and Stability of the High-Voltage Spinel Cathode Materials via In Situ Time-Resolved X-Ray Diffraction

    ACS Applied Materials & Interfaces · 2021-12-06

    Ying Min Luo, Yong Wang, Linsen Li, Yingjie Du, Liqin Yan, Tianrang Yang, Wen Wen, Liheng Zhang, Rui Guo, Cheng Yang, Jingying Xie

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  4. Single‐Crystalline Cathodes for Advanced Li‐Ion Batteries: Progress and Challenges

    Small · 2022-03-01

    Yongkang Han, Yike Lei, Jie Ni, Yingchuan Zhang, Zhen Geng, Pingwen Ming, Cunman Zhang, Xiaorui Tian, Ji‐Lei Shi, Yu‐Guo Guo, Qiangfeng Xiao

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  5. Submicron single‐crystalline LiNi 0.5 Mn 1.5 O 4 cathode with modulated Mn 3+ content enabling high capacity and fast lithium‐ion kinetics

    Rare Metals · 2022-03-14

    Zhao Fang, Xingliang Zhang, Xueyang Hou, Wenlong Huang, Linbo Li

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  6. Role of carbon nanotube on preparation of spinel LiNi0.5Mn1.5O4 cathode

    Journal of Materials Science · 2022-07-30

    Hao Ding, Ningshuang Zhang, Peng Wang, Hong Dong, Runrun Li, Shiyou Li

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  7. Tuning the structural disordering in hierarchical LiNi0.5Mn1.5O4 microrods for stable high-rate electrode performance

    Journal of Alloys and Compounds · 2022-12-19

    Zhuoya Tong, Qingquan Ye, Yimei Deng, Qin She, Aoyu Huang, Jun Xu, Xiaobo Zhu

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  8. On the Composition of LiNi 0.5 Mn 1.5 O 4 Cathode Active Materials

    Advanced Energy Materials · 2023-01-20

    Pirmin Stüble, Valeriu Mereacre, Holger Geßwein, Joachim R. Binder

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  9. Controlled crystal growth and electrode formation of single crystalline Li(Ni,Mn)2O4 spinel cathodes

    Journal of Alloys and Compounds · 2023-06-21

    Si Jin Seong, Minseuk Kim, Jeong‐Min Kim, Changil Park, Semin Ko, Ja Yeon Kim, Mihye Wu, Young‐Chul Song, Si‐Young Choi, Sungho Choi

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  10. The influence of different drying methods on the properties of LiNi0.5Mn1.5O4 material

    International Journal of Modern Physics B · 2023-06-21

    Yunxiu Li, Yu Zhang, Shihang Dai, Xianxian Qin, Xuetian Li, Zhongcai Shao, Zhijiang Liu

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  11. Molten Salt Synthesis of Multifaceted Pure-Phase Spinel LiNi 0.5 Mn 1.5 O 4 Platelets

    ACS Applied Energy Materials · 2023-07-28

    Gozde Oney, Jacob Olchowka, Arnaud Demortière, François Weill, Laurence Croguennec

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  12. Correlative Raman imaging and scanning electron microscopy for advanced functional materials characterization

    Cell Reports Physical Science · 2023-10-01

    Fuxi Liu, Xu Zou, Nailin Yue, Wei Zhang, Wei Zhang

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  13. Effect of washing on nickel-rich NCMs: methodology to quantify the lithium/proton-exchange kinetics, the inserted protons, and the structural changes

    Journal of Materials Chemistry A · 2024-01-01

    Stefan Oswald, Rebecca Wilhelm, Tim Kratky, László Szentmiklósi, Boglárka Maróti, Ildikó Harsányi, Sebastian A. Hallweger, Gregor Kieslich, Sebastian Günther, Hubert Andreas Gasteiger

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  14. High‐Voltage Spinel Cathode Materials: Navigating the Structural Evolution for Lithium‐Ion Batteries

    Advanced Materials · 2024-05-09

    Xiaobo Zhu, Aoyu Huang, Isaac Martens, Nikita Vostrov, Yongqi Sun, Marie‐Ingrid Richard, Tobias Urs Schülli, Lianzhou Wang

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  15. Synthesis of Monodisperse and Discrete Ultra-High Nickel LiNi0.97Co0.02Mn0.01O2 Octahedral Single Crystals via Single Crystal Intermediates for Li-Ion Batteries

    ACS Applied Materials & Interfaces · 2024-10-29

    Seung Hyun Choi, Soon-Kie Hong, Byunghyun Yun, Junho Jung, Chanhyun Baik, Kanghyeon Kim, Kyu Tae Lee

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  16. Controllable preparation of chamfered LiNi0.5Mn1.5O4 monocrystal cathode materials by trace Ti atoms replacing Mn and electrochemical properties

    Ionics · 2024-12-13

    Mengwen Wang, Jianwen Yang, Shengxian Li, Danfeng Zhang, Yuhang Wang, Zongsheng Qiu, Bin Huang, Quanqi Chen, Qing Zhu, Qiming Li

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  17. Towards High‐Performance Li‐Rich Cathode Materials: from Morphology Design to Electronic Structure Modulation

    Small · 2024-12-15

    Jing‐Zhe Wan, Chao Ma, Jie‐Sheng Chen, Kai‐Xue Wang

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  18. Single-crystal Ni-rich-doped LiNi 0.59 Co 0.3 Ti 0.1 Al 0.01 O 2 (NCTA) cathode materials: effect of annealing temperature on the structure, morphology, and electrochemical performance

    Physical Chemistry Chemical Physics · 2025-01-01

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  19. Strategies toward high-energy-density Co-free lithium nickel manganese oxide: from crystal structure control to flexible configuration design

    Energy & Environmental Science · 2025-01-01

    Jiguo Tu, Yan Li, Bokun Zhang, Xiaoyun Wang, Ramachandran Vasant Kumar, Libo Chen, Shuqiang Jiao

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  20. KOH-Assisted Molten Salt Route to High-Performance LiNi0.5Mn1.5O4 Cathode Materials

    Molecules · 2025-02-09

    Feng Pang, Fushan Feng, Shuyu Zhang, Na Feng, Changkun Cai, Shengli An

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  21. Breaking the Cycle of Heterogeneous Degradation: Surface-Targeted Protection for Ni-Rich Cathodes in Practical High-Energy Batteries

    ACS Energy Letters · 2025-02-28

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  22. Molten salt synthesis of a single-crystal LiNi0.5Mn1.5O4 cathode with an in situ constructed stable interface for 4.8 V-class all-solid-state batteries

    Science China Materials · 2025-05-07

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  23. Titania-based organometallic super-hydrophobic finishing of cellulose fabric for potential organic/aqueous phase separation application

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  24. Mg Substitution Improves the Surface Stability of High‐Voltage Spinel Cathodes under Accelerated Aging Conditions

    Advanced Functional Materials · 2025-11-01

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  25. Mitigating the Rock‐Salt Phase Transformation in Disordered LNMO Through Synergetic Solid‐State AlF 3 /LiF Modifications

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  26. Harnessing Metastable Byproducts: A Dual-Regulation Strategy for Intrinsically Stable High-Voltage Spinel Cathodes

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