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RESEARCH PAPER · Journal of Materials Chemistry A · 2020

Scalable upcycling of thermoplastic polyolefins into vitrimers through transesterification

Goutam Prasanna Kar, Mohand O. Saed, Eugene Michael Terentjev

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Scalable upcycling of thermoplastic polyolefins into vitrimers through transesterificationOriginalRecyclable, reprocessable, self-adhered and repairable carbon fiber reinforced polymers using full biobased matrices from camphoric acid and epoxidized soybean oil117Dually Crosslinked Polymer Networks Incorporating Dynamic Covalent Bonds161Strategic Approach Towards Plastic Waste Valorization: Challenges and Promising Chemical Upcycling Possibilities174Upcycling and catalytic degradation of plastic wastes332Dynamic Semicrystalline Networks of Polypropylene with Thiol-Anhydride Exchangeable Crosslinks69Performance modifying techniques for recycled thermoplastics105Polybutadiene Vitrimers with Tunable Epoxy Ratios: Preparation and Properties29Progress in Utilizing Dynamic Bonds to Fabricate Structurally Adaptive Self‐Healing, Shape Memory, and Liquid Crystal Polymers44Dynamic covalent exchange induced cyclization in poly(methacrylic anhydride)8On-demand catalyst-regulated distinctive topological transformations in a dynamic covalent network18Simple upcycling of virgin and waste polyethylene into covalent adaptable networks: catalyst-free, radical-based reactive processing with dialkylamino disulfide bonds87Shape memory poly (ether ether ketone)s with tunable chain stiffness, mechanical strength and high transition temperatures38Enhanced, hydrophobic, initial-shape programmable shape-memory composites with a bio-based nano-framework via gradient metal-ligand cross-linking13Fused Filament Fabrication of a Dynamically Crosslinked Network Derived from Commodity Thermoplastics30Biodegradable-Renewable Vitrimer Fabrication by Epoxidized Natural Rubber and Oxidized Starch with Robust Ductility and Elastic Recovery65Regulating the Dynamic Behaviors of Transcarbamoylation-Based Vitrimers via Mono-Variation in Density of Exchangeable Hydroxyl52Atomic Oxygen Resistance Vitrimers with High Strength, Recyclability, and Thermal Stability10Innovations Toward the Valorization of Plastics Waste65Diffusion-limited hydrolysis in polymeric materials24Polymerization, Stimuli‐induced Depolymerization, and Precipitation‐driven Macrocyclization in a Nitroaldol Reaction System**7Microscopic Dynamics and Viscoelasticity of Vitrimers71Exploring of the property of epoxy resins based on diselenide and disulfide dynamic linkers6Enabling resource circularity through thermo-catalytic and solvent-based conversion of waste plastics49Rheology of vitrimers150Organic-inorganic composite polyurethane vitrimers with high toughness, self-healing ability and recyclability27Effect of cross‐linking on the mechanical properties, degree of crystallinity and thermal stability of polyethylene vitrimers74Plastic Waste Upcycling: A Sustainable Solution for Waste Management, Product Development, and Circular Economy117Polyolefins Vitrimers: Design Principles and Applications108Thermal/Near‐Infrared Light Dual‐Responsive Reconfigurable and Recyclable Polythiourethane/CNT Composite with Simultaneously Enhanced Strength and Toughness7Reprocessable and Chemically Recyclable Hard Vitrimers Based on Liquid‐Crystalline Epoxides82Circularity in polymers: addressing performance and sustainability challenges using dynamic covalent chemistries112Novel covalent adaptable networks (CANs) of ethylene/1-octene copolymers (EOCs) made by free-radical processing: comparison of structure–property relationships of EOC CANs with EOC thermosets27Recycled Polymer Bio-based Composites: A Review of Compatibility and Performance Issues6Synthesis and characterization of polyolefin thermoplastic elastomers: A review85Scalable micropatterned epoxy vitrimer films by thermo-triggered bond exchange for repairable and recyclable triboelectric nanogenerators13Mechanical characterizations, recyclability of thermoplastics through melt grafting a dynamic covalent network onto polyethylene20Self‐Healable, Regenerable, and Degradable Dynamic Covalent Nitroalcohol Organogels5Polyester-based epoxy vitrimer integrating spent coffee ground as a natural filler15Self-healing and recyclable elastomer based on epoxidized natural rubber and carboxylated-chitosan28Experimental study on the mode Ι interlaminar properties of self-healable vitrimeric CFRP with various interfaces39Linear viscoelasticity, nonlinear rheology and applications of polyethylene terephthalate vitrimers15Polymeric Dynamic Crosslinker for Upcycling of Fragile Low-Molecular-Weight Polypropylene39Retrieving back plastic wastes for conversion to value added petrochemicals: opportunities, challenges and outlooks86Reprocessable, malleable and intrinsically fire-safe epoxy resin with catalyst-free mixed carboxylate/phosphonate transesterification27Dynamic covalent exchange in methacrylic anhydride copolymers5Sustainable developments in polyolefin chemistry: Progress, challenges, and outlook204Carbon Fiber-Reinforced Dynamic Covalent Polymer Networks Containing Acylsemicarbazide Bonds: Toward High-Performance Composites with Excellent Self-Healing and Upcycling Performance29One-step and Scalable Synthesis of EAA-based Reprocessable Vitrimer with Superior Mechanical Properties5Facile Approach for the Preparation of Robust and Thermally Stable Silyl Ether Cross-Linked Poly(ethylene-vinyl acetate) Vitrimers32Recyclable and Self-Healing Natural Rubber Vitrimers from Anhydride-Epoxy Exchangeable Covalent Bonds35Clarifying the Role of Epoxy Molecules and Base Catalysts for Vitrimer Transformation from Linear Polyesters11Design of Copolymer‐Based Blend Compatibilizers for Mixed Plastic Recycling38Does the Varying Reactivity in the Transient Polymer Network through Dynamic Exchange Regulate the Closed-Loop Circularity in Polyolefin Vitrimers?20Covalent adaptable networks and thermosets of multi-block ethylene/1-octene copolymers made by free-radical processing: Effects of melt flow index and crystallinity on thermomechanical properties and reprocessability17Effect of addition of aluminum phosphinate as fire retardant in a PBT vitrimer12C–H Functionalization of Polyolefins to Access Reprocessable Polyolefin Thermosets105Transformation of Styrene into Biodegradable Polymer through In Situ Epoxidation-Copolymerization Using Tandem Polymeric Catalysts8Tek Proseste Kompaund Elde Edebilen Tandem Bir Sistemle Yapılan Termoplastik Geri Dönüşümünün Çevreye ve Dünyaya Faydaları0Challenges in the mechanical recycling and upcycling of mixed postconsumer recovered plastics (PCR): A review42Durable and recyclable biomimetic glycol lignin/polyolefin compounds for a circular economy10Polypropylene-based transesterification covalent adaptable networks with internal catalysis41Effect of cross-link density on the performance of polyimine/epoxy vitrimers10Vulcanization of polypropylene7A review on value-addition to plastic waste towards achieving a circular economy76Experimental investigation on the self-healing properties of ester-exchanged vitrimeric CFRP laminate with microchannels8Dual reconfigurable network from a semi-crystalline functional polyolefin10Covalent Adaptable Networks Made by Reactive Processing of Highly Entangled Polymer: Synthesis-Structure-Thermomechanical Property-Reprocessing Relationship in Covalent Adaptable Networks35Microstructure, Viscoelasticity, and Extensional Rheology of Ethylene–Propylene Copolymer Vitrimers28Network homogeneity on linear and nonlinear viscoelasticity of polyethylene terephthalate vitrimers13Maleic Anhydride, Maleic Acid, and Fumaric Acid0Recyclable and Biobased Vitrimers for Carbon Fibre-Reinforced Composites—A Review24A continuous melt extrusion approach toward polyethylene‐based vitrimers with improved crosslinking and performance15Effect of processing conditions on the properties of vitrimerized polybutylene terephthalate prepared by reactive extrusion12New Advances in Covalent Network Polymers via Dynamic Covalent Chemistry372Synthesis of polyethylene-based covalent adaptable networks including 1,2,3-triazolium or imine dynamic cross-links by reactive processing9A comprehensive review on fiber-reinforced polymer composites: Raw materials to applications, recycling, and waste management237One-pot synthesis of robust silyl ether-based HDPE vitrimers with enhanced performance and recyclability12A Curing Agent for Facile Fabrication of Intrinsically Flame-Retardant Epoxy Vitrimers with Catalyst-Free Mixed Carboxylate/Phosphonate Transesterification17Design and Continuous (Re)Processing of Thermally Resilient Poly(Styrene-co-Maleic Maleate)-Based Covalent Adaptable Networks18A Study on the Impact of Chemical Structure on the Evolution of Aggregate Structure in Fiber-shaped High Density Polyethylene Vitrimer8Polypropylene Blends with Durable Hydrophobicity and Enhanced Mechanical Properties Based on POSS and Alkane Modified Polypentafluorophenyl Methacrylate2Closed-loop circular economy in ‘upcycled’ acrylonitrile–butadiene–styrene vitrimer10Cross-Linked Polyolefins: Opportunities for Fostering Circularity Throughout the Materials Lifecycle28Upcycling Post-Consumer Recycled Polypropylene Using a “Tailor-Made” Dynamic Cross-Linker with Controlled “Cross-Link Distribution”15Synthesis of Cross-Linkable Norbornenyl Copolymers via ROMP for Fabricating Cyclic Olefin Vitrimers7Upcycling of polyethylene waste to biodegradable adhesive and coating via Baeyer-Villiger reaction: A new view on oxidation-fracture mechanism and structure-function relationship10Functionalization and Repurposing of Polypropylene to a Thermoset Polyurethane13Click Chemistry in Designing Vitrimers: A New Class of Potential Sustainable Materials0Plastic recycling: Challenges and opportunities88Extrudable and Highly Creep-Resistant Covalent Adaptable Networks Made from Polyethylene and Ethylene/1-Octene Copolymers by Reactive Processing with Aromatic Disulfide Cross-Links21Comparative Study of Polyethylene, Polypropylene, and Polyolefins Silyl Ether-Based Vitrimers9Disulfide Exchange Reactions: The Bridge Between Processability, Performance, and High‐Throughput Recyclability in Crosslinked Elastomers8The conformational preference of dynamic crosslinker modulates the ‘closed-loop’ circular economy in polypropylene vitrimer11‘Vitrimer nanocomposites’ derived from graphene oxide and post-consumer recycled polypropylene12Can mixed plastics be recycled and upcycled without separation?11Composition–structure–property relationships of polyethylene vitrimers crosslinked by 8-arm polyhedral oligomeric silsesquioxane7Impact of nanofillers on vitrimerization and recycling strategies: a review20Scalable solution for high dispersibility and low heterogeneity of nuclear-shielding high inorganic filler/polymer composites: a vitrimer via reactive extrusion & mechanochemical intercalation0Robust, Reprocessable and Scalable Ethylene Acrylic Acid Copolymer (EAA) Derived Vitrimer Based on Dual Cross-linked Networks2Chitosan-Enhanced Vitrimerization of Thermoset Epoxy Resins: Multiple-Dynamic Networks for Sustainable Approaches, Improved Mechanical Properties, and Rapid Stress Relaxation5Enhanced healability and weldability properties of vitrimers: Review article10Reactive Processing of Polyethylene with Azidotriazine: From Modified Thermoplastics to Injection Moldable Covalent Adaptable Networks7Self‐healing and shape memory functions in elastomers: Recent advances and future prospectives3Synthesis of Cross-Linked Polyolefin Elastomers with High Performance Yet Good Reprocessability11Repurposing Post‐Consumer Polyethylene to Access Cross‐Linked Polyethylene with Reprocessability, Recyclability, and Tunable Properties18Repurposing Post‐Consumer Polyethylene to Access Cross‐Linked Polyethylene with Reprocessability, Recyclability, and Tunable Properties2Dynamic crosslinking of thermoplastics via perfluorophenyl nitrene C–H insertion to form recyclable thermosets24Polypropylene Covalent Adaptable Networks with Full Cross-Link Density Recovery after Reprocessing: Development by Free-Radical Reactive Processing with Resonance-Stabilized, Aromatic Disulfide Cross-Linkers25Dynamic Cross-Linker Facilitates a Closed-Loop Circular Economy in Upcycled Acrylonitrile-Butadiene-Styrene5Recycling reinvented: Converting PET bottle waste into 3D printable PCR polypropylene vitrimers for a sustainable future20Extrudable Thermosets Based on Dynamic Covalent Polymers4Reprocessable Polypropylene Covalent Adaptable Networks via Free-Radical Reactive Processing with Vinyl Aromatic Additives15Functionalized Glass Fibers in Reversible Networks─A Cross-Road to Dimensional Stability and Facile Recycling of Cross-Linked Elastomers3Toward Circular Polymer Materials and Manufacturing: Dynamic Bonding Strategies for Upcycling Thermoplastics and Thermosets12Robust cyclic olefin thermoplastic elastomer with excellent mechanical and thermal performance3Recyclable Cross-Linked Polyethylene from Self-Condensing Telechelic Polyethylene by Combining Olefin Metathesis, Hydrogenation, and Transesterification4Transparent Siloxane-Based Polyolefin Vitrimer and Its Use As an Encapsulant for Recyclable Photovoltaic Modules3Enhancing vitrimer applications: development of E-GMA/EMAZn vitrimeric filaments for advanced 3D/4D printing3Fully Recyclable and Remarkably Robust Cross-Linked Polyethylene Networks via Direct Free-Radical Copolymerization with Disulfide Dynamic Covalent Bonds19Enhancing Mechanical Properties and Crystallization Kinetics of Isotactic Polypropylene by Boronic Acid-Cross-Linked Additives3Understanding Non-isothermal Crystallization Behaviors of Polyethylene-Derived Vitrimers11A Circular Thermoplastic Vulcanizate (TPV) Comprising Biobased EPDM and Recycled Polypropylene: Introducing Vitrimer Chemistry10Scaling up vitrimers: developing thermoplastic-based dynamic networks via epoxy–anhydride reactions2From ocean to opportunity: Upcycling fishing net waste into high-performance, reprocessable nylons4Upcycling Waste Polypropylene into Multifunctional Homogeneous Additives for Simultaneously Enhanced Mechanical Performance and Processability6Reactive extrusion of vitrimers: A short review8Mechanically robust, fast self-healing epoxy vitrimers based on TBD catalyzed dynamic imine and siloxane exchanges4Reprocessing and degradation capability of biobased epoxy vitrimer composites0Efficient Compatibilization and Toughening of Polyethylene and Polypropylene Blends through Dynamic Cross-Linking: A Sustainable Approach to Polyolefin Recycling8Pioneering a circular economy: Sustainable co-upcycling of polyethylene and polypropylene waste via dynamic vitrimer networks12Catalyst-Free Ethylene Vinyl Acetate Copolymer (EVA) Vitrimer Based on Titanate Exchange through a One-Step, Green, and Scalable Reactive Blending Approach3Catalyst Influence on the Crystallization Behaviors and Mechanical Properties of Polyethylene Vitrimers10“Catfish Effect”‐Inspired Hybrid Dynamic Polymer Networks with Fast Liquid‐Like Dynamics and Scalable Processability for Sustainable Electronics1Disulfide‐Initiated Addition–Fragmentation Chain Transfer in Allyl Sulfide‐Based Vitrimers11Disulfide‐Initiated Addition–Fragmentation Chain Transfer in Allyl Sulfide‐Based Vitrimers1Recent advances in plastic upcycling enabled by dynamic covalent cross-linking strategies0One Molecule, Two Roles: Vitrimer‐Enabled Polypropylene for High‐Performance, Recyclable MWCNT Nanocomposites5Cure Kinetics and Chemorheological Modeling of a Transesterification‐Based Epoxy/Anhydride Vitrimer3Enhancing the robustness of thiol–thioester covalent adaptable networks through reversible thiol–Michael masking1Creep-resistant, extrudable, and recyclable polyolefin covalent adaptable networks incorporating azine cross-links via reactive processing3Photocurable vitrimer resins combining elastic behavior, low hysteresis and self-healing for sustainable additive manufacturing0Strong Carbon Nanotube Fiber-Vitrimer Interfaces Yield Closed-Loop Recyclable High-Performance Composites0Vitrimers: bridging the recycling gap between thermosets and thermoplastics0Impact of Network Architecture and Cross-Link Aggregation on the Crystallization Behavior of a Polypropylene-Based Thermoset Polyurethane2Revisiting Properties of Vitrimers: Special Rheological and Chemical Characteristics and Reconsidered Concepts6Covalent Adaptable Networks: Reprocessable Cross-Linked Polymers63Reactive Melt Extrusion for Polymer Deconstruction and Upcycling4Dynamic epoxy–anhydride compatibilization of EVA/HDPE blends for mechanically robust, reprocessable, and self-healing hot-melt adhesives1Sustainable BHMF-based polyester vitrimers with tunable dynamics and mechanical recyclability0Carbamate‐Containing Decrosslinkers for Reactive Melt Extrusion Deconstruction of Crosslinked Polyurethane Composites0

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