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RESEARCH PAPER · Angewandte Chemie International Edition · 2019

Separation of Xe from Kr with Record Selectivity and Productivity in Anion‐Pillared Ultramicroporous Materials by Inverse Size‐Sieving

Qingju Wang, Tian Ke, Lifeng Yang, Zhaoqiang Zhang, Xili Cui, Zongbi Bao, Qilong Ren, Qiwei Yang, Huabin Xing

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Separation of Xe from Kr with Record Selectivity and Productivity in Anion‐Pillared Ultramicroporous Materials by Inverse Size‐SievingOriginalTailoring Pore Aperture and Structural Defects in Zirconium-Based Metal–Organic Frameworks for Krypton/Xenon Separation119Crystal Engineering of Hybrid Coordination Networks: From Form to Function77Two Isostructural Flexible Porous Coordination Polymers Showing Contrasting Single-Component and Mixture Adsorption Properties for Propylene/Propane33Molecular Sieving of C2‐C3 Alkene from Alkyne with Tuned Threshold Pressure in Robust Layered Metal–Organic Frameworks128Molecular Sieving of C2‐C3 Alkene from Alkyne with Tuned Threshold Pressure in Robust Layered Metal–Organic Frameworks15An Ultra‐Microporous Metal–Organic Framework with Exceptional Xe Capacity17Topology Meets Reticular Chemistry for Chemical Separations: MOFs as a Case Study109Boosting Selective Adsorption of Xe over Kr by Double-Accessible Open-Metal Site in Metal–Organic Framework: Experimental and Theoretical Research60Rational design and synthesis of ultramicroporous metal-organic frameworks for gas separation218CoNi Alloy Nanoparticles Embedded in Metal–Organic Framework‐Derived Carbon for the Highly Efficient Separation of Xenon and Krypton via a Charge‐Transfer Effect100CoNi Alloy Nanoparticles Embedded in Metal–Organic Framework‐Derived Carbon for the Highly Efficient Separation of Xenon and Krypton via a Charge‐Transfer Effect26Crystallizing Atomic Xenon in a Flexible MOF to Probe and Understand Its Temperature-Dependent Breathing Behavior and Unusual Gas Adsorption Phenomenon132Docking of Cu I and Ag I in Metal–Organic Frameworks for Adsorption and Separation of Xenon195Docking of CuI and AgI in Metal–Organic Frameworks for Adsorption and Separation of Xenon15Robust metal–organic framework with multiple traps for trace Xe/Kr separation102Pore Size Control via Multiple-Site Alkylation to Homogenize Sub-Nanoporous Covalent Organic Frameworks for Efficient Sieving of Xenon/Krypton45A microporous Ce-based MOF with the octahedron cage for highly selective adsorption towards xenon over krypton19Recent advances in the capture and abatement of toxic gases and vapors by metal–organic frameworks85An Unprecedented Pillar‐Cage Fluorinated Hybrid Porous Framework with Highly Efficient Acetylene Storage and Separation211An Unprecedented Pillar‐Cage Fluorinated Hybrid Porous Framework with Highly Efficient Acetylene Storage and Separation34High‐Silica CHA Zeolite Membrane with Ultra‐High Selectivity and Irradiation Stability for Krypton/Xenon Separation70High‐Silica CHA Zeolite Membrane with Ultra‐High Selectivity and Irradiation Stability for Krypton/Xenon Separation12Construction of an Anion-Pillared MOF Database and the Screening of MOFs Suitable for Xe/Kr Separation99Tuning the Structural Flexibility for Multi-Responsive Gas Sorption in Isonicotinate-Based Metal–Organic Frameworks53A pore-engineered metal-organic framework with mixed ligands enabling highly efficient separation of hexane isomers for gasoline upgrading46Metal-organic frameworks as functional materials for implantable flexible biochemical sensors41Ultramicroporous carbons featuring sub‐Ångstrom tunable apertures for the selective separation of light hydrocarbon46Development of the Assessment to Measure the Critical Thinking Ability of the Blood Circulation Systems for Humans in Bengkulu City1Isoreticular chemistry within metal–organic frameworks for gas storage and separation584Predicting adsorption and separation performance indicators of Xe/Kr in metal-organic frameworks via a precursor-based neural network model14Tailoring Pore Structure and Morphologies in Covalent Organic Frameworks for Xe/Kr Capture and Separation35Geometry control of adsorption sites in sulfonate-pillared hybrid ultramicroporous materials for efficient C4 olefin separations34Efficient Xe/Kr separation on two Metal-Organic frameworks with distinct pore shapes50Efficient separation of C4 olefins using tantalum pentafluor oxide anion-pillared hybrid microporous material19Experimental and computational evaluation of Ag-exchanged ZSM-5 and SSZ-13 for xenon capture14A Review on Anion-Pillared Metal Organic Framework (Apmof) and its Composites with the Balance of Adsorption Capacity and Separation Selectivity for Efficient Gas Separation1Efficient Xe selective separation from Xe/Kr/N 2 mixtures over a microporous CALF-20 framework41Enhanced Xe/Kr separation via the pore size confinement effect of a microporous thorium-based metal–organic framework9Recent advances in metal–organic frameworks for gas adsorption/separation262Recent advances in microporous metal–organic frameworks as promising adsorbents for gas separation83Strong Hydrogen Bond in the Crystal Structure Design of CuNbOF 5·4H 2O0Ultramicroporous hydrogen-bond decorated robust metal–organic framework for high xenon capture performances20Hydrogen‐Bonded Metal–Nucleobase Frameworks for Efficient Separation of Xenon and Krypton18Hydrogen‐Bonded Metal–Nucleobase Frameworks for Efficient Separation of Xenon and Krypton89Shell‐like Xenon Nano‐Traps within Angular Anion‐Pillared Layered Porous Materials for Boosting Xe/Kr Separation15Shell‐like Xenon Nano‐Traps within Angular Anion‐Pillared Layered Porous Materials for Boosting Xe/Kr Separation75Fine pore engineering in a series of isoreticular metal-organic frameworks for efficient C2H2/CO2 separation327Virtual Screening of Nanoporous Materials for Noble Gas Separation16Robust and Radiation-Resistant Hofmann-Type Metal–Organic Frameworks for Record Xenon/Krypton Separation168Balancing uptake and selectivity in a copper-based metal–organic framework for xenon and krypton separation29Efficient organic iodide capture by a mesoporous bimetallic-organic framework35Nanoporous 3D Graphene-like Zeolite-Templated Carbon for High-Affinity Separation of Xenon from Krypton16Dinuclear Nickel–Oxygen Cluster-Based Metal–Organic Frameworks with Octahedral Cages for Efficient Xe/Kr Separation23Efficient Xe/Kr Separation Based on a Lanthanide–Organic Framework with One-Dimensional Local Positively Charged Rhomboid Channels45Microporous Metal–Organic Framework with Cage-within-Cage Structures for Xenon/Krypton Separation16Double-Accessible Open Metal Sites in Metal–Organic Frameworks with Suitable Pore Size for Efficient Xe/Kr Separation29One-step removal of alkynes and propadiene from cracking gases using a multi-functional molecular separator42Utilization of cationic microporous metal-organic framework for efficient Xe/Kr separation56HF Resistant Porous Aromatic Frameworks for Electronic Special Gases Separation36Recent Advances in the Development of Metal–Organic Frameworks for Propylene and Propane Separation49A review on anion-pillared metal–organic frameworks (APMOFs) and their composites with the balance of adsorption capacity and separation selectivity for efficient gas separation102Thermodynamics-Kinetics-Balanced Metal–Organic Framework for In-Depth Radon Removal under Ambient Conditions45Computation-informed optimization of Ni(PyC)2 functionalization for noble gas separations12Microporous carbon granules with narrow pore size distribution and rich oxygen functionalities for Xe/Kr separation19Dense packing of xenon in an ultra-microporous metal–organic framework for benchmark xenon capture and separation33Thiophene-based conjugated ultra-micropore rigid polymers for selective xenon capture21Strong hydrogen bond in the crystal structure design of CuNbOF5·4H2O3Dicopper( ii ) paddle-wheel metal–organic frameworks for high propyne storage under ambient conditions9Porous organic cages for gas separations74Zirconium halide complexes. Synthesis, structure, practical application potential0Strategies, Synthesis, and Applications of Metal-Organic Framework Materials0Zirconium Halide Complexes: Synthesis, Structure, and Practical Applications0Switchable Xe/Kr Selectivity in a Hofmann‐Type Metal–Organic Framework via Temperature‐Responsive Rotational Dynamics34Pore partition in two-dimensional covalent organic frameworks152Shaped layered two-dimensional fluorinated metal-organic frameworks for highly efficient acetylene/ethylene separation12Topology and porosity control on zirconium–fumarate frameworks boosting xenon/krypton separation16Pore environment modulation of metal-organic frameworks enables efficient adsorptive separation of Xe/Kr23Methyl-functionalized flexible ultra-microporous MOF for efficient SF6/N2 mixture separation71High-Throughput, Multiscale Computational Screening of Metal–Organic Frameworks for Xe/Kr Separation with Machine-Learned Parameters17A Microporous Hydrogen‐Bonded Organic Framework Based on Hydrogen‐Bonding Tetramers for Efficient Xe/Kr Separation86A Microporous Hydrogen‐Bonded Organic Framework Based on Hydrogen‐Bonding Tetramers for Efficient Xe/Kr Separation9Metal-organic frameworks for xenon and krypton separation32Efficient C2H2/CO2 and C2H2/C2H4 separations in a novel fluorinated metal–organic framework56Mixed matrix membranes based on NbOF52− anion-pillared porous MOFs for efficient CO2 separation8A novel microporous hydrogen-bonded organic framework with electron-rich alkynyl groups for highly efficient C 2 H 6 /C 2 H 4 separation17Co (II) -doped hybrid Zn (II) tetraborate complexes, [Zn x Co (1− x ) (1,3-dap)B 4 O 7 ] (1,3-dap = 1,3-diaminopropane): BET analysis and N 2 /H 2 O/D 2 O adsorption studies0Contracting pore channels of a magnesium-based metal–organic framework by decorating methyl groups for effective Xe/Kr separation3Flexible Microporous Framework for One-Step Acquisition of Ethylene from Ternary C 2 Hydrocarbons12Biomass-derived ultramicroporous carbon with narrow pore size distribution for record-high radon adsorption17A Robust Al-Based Metal–Organic Framework for Highly Efficient Natural Gas Purification9Adsorptive separation of Xe/Kr mixtures by microporous lanthanide metal-organic frameworks with high thermal stability3Dinuclear Copper Sulfate-Based Square Lattice Topology Network with High Alkyne Selectivity6Effective approaches to boost Xe/Kr separation in Metal-Organic Frameworks: A review52Control of Zeolite Local Polarity toward Efficient Xenon/Krypton Separation57Meso/macropore emerging from MOF granulation for enhancing performance in the Xe/Kr separation9Flexible Properties: Adsorptive Storage and Separation2Adsorption of Xenon, Krypton, and Their Mixture on the Flexible Metal–Organic Framework DUT-8(Ni)9Metal-organic frameworks with optimal pore cages for high Xe adsorption and efficient Xe/Kr separation20Significant Enhancement of Xe Adsorption and Xe/Kr Separation of Metal–Organic Framework Induced by Pore Channel Shaping and Pore Polarity Engineering29Suitable Pore Confinement with Multiple Interactions in a Low-Cost Zeolitic Imidazolate Framework for Efficient Xe Capture and Separation7Pore Chemistry and Architecture Control in Anionic Functional Ultramicroporous Materials for Record Dense Packing of Xenon55Highly Efficient Separation of Intermediate‐Size m ‐Xylene from Xylenes via a Length‐Matched Metal–Organic Framework with Optimal Oxygen Sites Distribution27Highly Efficient Separation of Intermediate‐Size m‐Xylene from Xylenes via a Length‐Matched Metal–Organic Framework with Optimal Oxygen Sites Distribution7The Reinforced Separation of Intractable Gas Mixtures by Using Porous Adsorbents61Recent progress of radionuclides separation by porous materials265A N-heterocyclics induced π-π interaction strategy to synthesis hyper-crosslinked polymers with enhanced porosity for xenon adsorption8A Microporous Hydrogen‐Bonded Organic Framework with Open Pyrene Sites Isolated by Hydrogen‐Bonded Helical Chains for Efficient Separation of Xenon and Krypton34A Microporous Hydrogen‐Bonded Organic Framework with Open Pyrene Sites Isolated by Hydrogen‐Bonded Helical Chains for Efficient Separation of Xenon and Krypton4Fluoro-functionalized metal organic frameworks with two-fold interpenetration for boosting xenon/krypton separation6Construction of synergistic binding sites in a robust MOF for excellent C 2 H 4 purification and C 3 H 6 recovery performance20Record high CH4/N2 adsorption separation selectivity in a scalable metal-organic framework26Metal−Organic Framework with Constrained Flexibility for Benchmark Separation of Hexane Isomers22Metal−Organic Framework with Constrained Flexibility for Benchmark Separation of Hexane Isomers5Bromine functionalized zirconium–fumarate frameworks for enhanced xenon capture and separation9Nonpolar Pore Confinement within Metal–Organic Frameworks for Xe/Kr Separation20Efficient SF6 Separation from a SF6/N2 Gas Mixture Based on Terephthalate Metal–Organic Framework MIL-53(Al)5Smooth pore surface in zeolites for krypton capture under humid conditions1Microporous Na–Nd Heterometallic Organic Frameworks for C2H2/CO2 and C3H4/C3H6 Separation3Simultaneously tuning the pore size and structural softness on flexible metal-organic frameworks for enhanced CO2/C2H2 separation15Confinement-intensified multi-heavy-atom effect in a tetrahedral iodine cage enables unprecedented capture of trace xenon and krypton15Efficient Capture and Separation of Xenon/Krypton from Off‐Gas by a Radiation‐Resistant Metal–Organic Framework10Precise Kinetic Separation of Hexane Isomers via Morphology Engineering of Metal–Organic Frameworks with Diffusion‐Selective Pore Structure3Precise Kinetic Separation of Hexane Isomers via Morphology Engineering of Metal–Organic Frameworks with Diffusion‐Selective Pore Structure8Simultaneous recovery of xenon and krypton with high purity and high productivity enabled by densely distributed nanotraps within an interpenetrated porous material0Biomimetic Hydrophobic‐Polar Metal‐Organic Frameworks for Record‐Breaking Separation and Capture of Xenon and Krypton15Anion‐Shielded Porous Organic Cages for High‐Performance Xenon/Krypton Separation11Highly efficient Xe/Kr separation within a metal-organic framework featuring continuous molecule traps3Elucidating the Sigmoidal Adsorption Behavior of Xenon in Flexible Hofmann‐Type MOFs Through Experiments and Molecular Dynamics with Machine Learning Potentials5Exclusive recognition of CO2 from exhaled anesthetic gas mixtures by a stable ultramicroporous Al-MOF with customized pore cavities1Alkoxy‐Functionalized Three‐Dimensional Microporous Covalent Organic Frameworks for Efficient Xenon/Krypton Separation0Functional Chain Engineering in MOFs: Balancing Pore Size and Affinity for Noble Gas Separation0Selective separation of Kr/Xe via borophene nanochannels under external driving forces: A combined molecular dynamics and neural network study0“Two‐in‐One” Anion Engineering Strategy for One‐Step Ethylene Purification From a Ternary Mixture1Diffusion‐Trap Mechanism‐Mediated Trace Propylene Capture in a Microporous Metal‐Organic Framework Enables Record Ethylene Purification From Cracking Gas1Diffusion‐Trap Mechanism‐Mediated Trace Propylene Capture in a Microporous Metal‐Organic Framework Enables Record Ethylene Purification From Cracking Gas0Hierarchical Microporous Anion Pillared Metal–Organic Frameworks (APMOFs) for Gas Separation2Linker Engineering in Flexible Metal–Organic Frameworks Suppressing Slipping‐Off Effect for Efficient Xe/Kr Separation0

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  44. Hydrogen‐Bonded Metal–Nucleobase Frameworks for Efficient Separation of Xenon and Krypton

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  45. Shell‐like Xenon Nano‐Traps within Angular Anion‐Pillared Layered Porous Materials for Boosting Xe/Kr Separation

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  47. Fine pore engineering in a series of isoreticular metal-organic frameworks for efficient C2H2/CO2 separation

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  48. Virtual Screening of Nanoporous Materials for Noble Gas Separation

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  50. Balancing uptake and selectivity in a copper-based metal–organic framework for xenon and krypton separation

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