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RESEARCH PAPER · Journal of the American Chemical Society · 2016

Circumventing Diffusion in Kinetically Controlled Solid-State Metathesis Reactions

Andrew J. Martinolich, Joshua A. Kurzman, James Richmond Neilson

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Circumventing Diffusion in Kinetically Controlled Solid-State Metathesis ReactionsOriginalThe thermodynamic scale of inorganic crystalline metastability961Paracrystalline Disorder from Phosphate Ion Orientation and Substitution in Synthetic Bone Mineral23Toward Reaction-by-Design: Achieving Kinetic Control of Solid State Chemistry with Metathesis112Rapid microwave-assisted preparation of binary and ternary transition metal sulfide compounds17Synthesis, crystal structure and optical absorption of NaInS2-Se11Topochemical Deintercalation of Al from MoAlB: Stepwise Etching Pathway, Layered Intergrowth Structures, and Two-Dimensional MBene388Combined computational and experimental investigation of the La 2 CuO 4– x S x (0 ≤ x ≤ 4) quaternary system9Rapid Phase Screening via Hydride Route: A Discovery of K8–xZn18+3xSb1626The development of strategies for nanoparticle synthesis: Considerations for deepening understanding of inherently complex systems20Selective Formation of Yttrium Manganese Oxides through Kinetically Competent Assisted Metathesis Reactions57Kinetically Controlled Low-Temperature Solid-State Metathesis of Manganese Nitride Mn3N227Protocols for High Temperature Assisted-Microwave Preparation of Inorganic Compounds62Yttrium Manganese Oxide Phase Stability and Selectivity Using Lithium Carbonate Assisted Metathesis Reactions17Catalytic behavior of hexaphenyldisiloxane in the synthesis of pyrite FeS 22Selective metathesis synthesis of MgCr 2 S 4 by control of thermodynamic driving forces44Ion Exchange of Layered Alkali Titanates (Na2Ti3O7, K2Ti4O9, and Cs2Ti5O11) with Alkali Halides by the Solid-State Reactions at Room Temperature36Pushing the Limits of Metastability in Semiconducting Perovskite Oxides for Visible-Light-Driven Water Oxidation33Sequential pairwise reactions dictate phase evolution in the solid-state synthesis of multicomponent ceramics0Mechanistic insight of KBiQ 2 (Q = S, Se) using panoramic synthesis towards synthesis-by-design27Mechanochemical methods for the transfer of electrons and exchange of ions: inorganic reactivity from nanoparticles to organometallics65Selective kinetic growth and role of local coordination in forming Al 2 TiO 5 -based coatings at lower temperatures8Observing and Modeling the Sequential Pairwise Reactions that Drive Solid‐State Ceramic Synthesis89Kinetically Stabilized Cation Arrangement in Li 3 YCl 6 Superionic Conductor during Solid‐State Reaction57Panoramic (in beam) studies of materials synthesis1Metathesis routes to materials7Rapid and Energetic Solid-State Metathesis Reactions for Iron, Cobalt, and Nickel Boride Formation and Their Investigation as Bifunctional Water Splitting Electrocatalysts29Fluorine-Free Fabrication of MXene via Photo-Fenton Approach for Advanced Lithium–Sulfur Batteries128Circumventing Thermodynamic Constraints in Nucleation-Controlled Crystallization of Al2TiO5-Based Chemical Vapor Deposition Coatings4Relative Kinetics of Solid-State Reactions: The Role of Architecture in Controlling Reactivity29Thin-Film Paradigm to Probe Interfacial Diffusion during Solid-State Metathesis Reactions4Spontaneous Seed Formation during Electrodeposition Drives Epitaxial Growth of Metastable Bismuth Selenide Microcrystals13Thermochemical reaction strategies for the rapid formation of inorganic solid-state materials3Metastability and Photoelectrochemical Properties of Cu 2 SnO 3 and Cu 2– x Li x TiO 3 : Two Cu(I)-Based Oxides with Delafossite Structures12Phase-field modeling of solid-state metathesis reactions with the charge neutrality constraint3Role of Oxygen in Vacancy-Induced Phase Formation and Crystallization of Al2TiO5-Based Chemical Vapor-Deposited Coatings9In situ high temperature powder x-ray diffraction technique using a sapphire single-crystal flat cell12Stability and Metastability of Li3YCl6 and Li3HoCl613Soft Chemistry of Hard Materials: Low-Temperature Pathways to Bulk and Nanostructured Layered Metal Borides17Considerations for quantitative in situ X-ray powder diffraction studies of solid-state reactions2Resolving Fast Relative Kinetics in Inorganic Solid-State Synthesis15Low-temperature synthesis of cation-ordered bulk Zn 3 WN 4 semiconductor via heterovalent solid-state metathesis6Mechanistically Guided Materials Chemistry: Synthesis of Ternary Nitrides, CaZrN 2 and CaHfN 222Ultrafast Carbothermal Shock Synthesis of Wadsley–Roth Phase Niobium‐Based Oxides for Fast‐Charging Lithium‐Ion Batteries27Simple to Quadruple Perovskite Transformation by Coordination Switching upon Solid-State Ion Exchange of NaNbO33Kinetic and Thermodynamic Pathways Via Ion Exchange Metathesis of Cobalt Thiophosphate0Electrode materials for calcium batteries: Future directions and perspectives13Reaction pathways for the formation of complex fluorides revealed by in situ synchrotron X-ray diffraction1Efficient Exploratory Synthesis of Quaternary Cesium Chlorides Guided by In Silico Predictions5Development of a compact near-infrared lamp furnace for synchrotron powder diffraction and its application for in situ high-temperature observation of ferrite magnets1Synergistic effect of an oxygen-defective TiNb 2 O 7 anode and lithiated polyacrylic acid for high-power lithium-ion storage12Chemical weathering of molecular single crystals to monoliths of quantum dots3Room temperature, solid-state Ca ion-exchange in Na0.67Mn0.72Mg0.28O21All-single-crystal mullite nanowire aerogels for thermal protection at 1700°C0Catalytic function of Y2O3-based catalyst in chemical looping synthesis of C2H2 from inorganic C and H2O at moderate temperatures0Exploring magnesium- and calcium-based compounds via solid-state metathesis reactions0

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  2. Paracrystalline Disorder from Phosphate Ion Orientation and Substitution in Synthetic Bone Mineral

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  4. Rapid microwave-assisted preparation of binary and ternary transition metal sulfide compounds

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  6. Topochemical Deintercalation of Al from MoAlB: Stepwise Etching Pathway, Layered Intergrowth Structures, and Two-Dimensional MBene

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  7. Combined computational and experimental investigation of the La 2 CuO 4– x S x (0 ≤ x ≤ 4) quaternary system

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  8. Rapid Phase Screening via Hydride Route: A Discovery of K8–xZn18+3xSb16

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  10. Selective Formation of Yttrium Manganese Oxides through Kinetically Competent Assisted Metathesis Reactions

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  14. Catalytic behavior of hexaphenyldisiloxane in the synthesis of pyrite FeS 2

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  15. Selective metathesis synthesis of MgCr 2 S 4 by control of thermodynamic driving forces

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  16. Ion Exchange of Layered Alkali Titanates (Na2Ti3O7, K2Ti4O9, and Cs2Ti5O11) with Alkali Halides by the Solid-State Reactions at Room Temperature

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  17. Pushing the Limits of Metastability in Semiconducting Perovskite Oxides for Visible-Light-Driven Water Oxidation

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  18. Sequential pairwise reactions dictate phase evolution in the solid-state synthesis of multicomponent ceramics

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  19. Mechanistic insight of KBiQ 2 (Q = S, Se) using panoramic synthesis towards synthesis-by-design

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  23. Kinetically Stabilized Cation Arrangement in Li 3 YCl 6 Superionic Conductor during Solid‐State Reaction

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