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RESEARCH PAPER · Chemistry - A European Journal · 2008

Actinide Polyoxometalates: Incorporation of Uranyl–Peroxo in U‐Shaped 36‐Tungsto‐8‐Phosphate

Sib Sankar Mal, Michael H. Dickman, Ulrich Kortz

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Actinide Polyoxometalates: Incorporation of Uranyl–Peroxo in U‐Shaped 36‐Tungsto‐8‐PhosphateOriginalThe palladium(II)-decorated 22-tungsto-2-bismuthate(III), [Pd3(H2O)9Bi2W22O76]8−24ChemInform Abstract: Actinide Polyoxometalates: Incorporation of Uranyl—Peroxo in U‐Shaped 36‐Tungsto‐8‐phosphate.0Symmetry versus Minimal Pentagonal Adjacencies in Uranium‐Based Polyoxometalate Fullerene Topologies178Symmetry versus Minimal Pentagonal Adjacencies in Uranium‐Based Polyoxometalate Fullerene Topologies34A New Supramolecular Assembly Based on Triple-Dawson-Type Polyoxometalate and 3d-4f Heterometallic Cluster91Heterogeneous Wheel‐Shaped Cu20‐Polyoxotungstate [Cu20Cl(OH)24(H2O)12(P8W48O184)]25− Catalyst for Solvent‐Free Aerobic Oxidation of n‐Hexadecane44A Remarkable Member of the Polyoxometalates: The Eight-Nickel-Capped α-Keggin Polyoxoazonickelate35Syntheses and Crystal Structures of dmso‐Coordinated Tungstoantimonates(III) and ‐bismuthates(III)12Crown and Bowl-Shaped Clusters of Uranyl Polyhedra62A new sandwich-type polyoxometalate constructed from penta-lacunary [HPW7O28]8− units and MnIII ion4Two Heterometallic Aggregates Constructed from the {P2W12}-Based Trimeric Polyoxotungstates and 3d-4f Heterometals73Coordination between [H2P2W12O48]12− and antimony(iii): synthesis and characterization of sandwich complex derived from the new {P2W13O51} fragment26Mixed-valent vanadium substituted polyoxometalates: the wheel shaped [Rb3⊂{VVVIV3O7(H2O)6}2{H6P6W39O147(H2O)3}]15−19Polyoxometalates: Building Blocks for Functional Nanoscale Systems2273Polyoxometallate als Bausteine für funktionelle Nanosysteme385Cobalt, Manganese, Nickel, and Vanadium Derivatives of the Cyclic 48-Tungsto-8-Phosphate [H7P8W48O184]33−87Reactivity of Polyoxoniobates in Acidic Solution: Controllable Assembly and Disassembly Based on Niobium‐Substituted Germanotungstates58On the Origin of the Cation Templated Self-Assembly of Uranyl-Peroxide Nanoclusters109Liquid-Phase Selective Oxidation by Multimetallic Active Sites of Polyoxometalate-Based Molecular Catalysts30Structural peculiarities of actinyl complexation with monolacunary polyoxometalates9Low‐Symmetry Uranyl Pyrophosphate Cage Clusters39Silver(I)−Ethynide Clusters Constructed with Phosphonate-Functionized Polyoxovanadates179A comprehensive comparison of transition-metal and actinyl polyoxometalates332Two wheel-like polytungstates obtained by incorporation of two {Cu4} clusters and two molybdenum centers in the {W48} wheel14Uranyl peroxide pyrophosphate cage clusters with oxalate and nitrate bridges27Uranyl Peroxide Oxalate Cage and Core–Shell Clusters Containing 50 and 120 Uranyl Ions70{W48} Ring Opening: Fe16‐Containing, Ln4‐Stabilized 49‐Tungsto‐8‐Phosphate Open Wheel [Fe16O2(OH)23(H2O)9(P8W49O189)Ln4(H2O)20]11−80Uranyl Heteropolyoxometalate: Synthesis, Structure, and Spectroscopic Properties37Experimental and Computational Study of a New Wheel-Shaped {[W5O21]3[(UVIO2)2(μ-O2)]3}30–Polyoxometalate33Synthesis and Structural Characterization of Heterometallic Thorium Aluminum Polynuclear Molecular Clusters14Clusters of Actinides with Oxide, Peroxide, or Hydroxide Bridges344{Ta12}/{Ta16} Cluster-Containing Polytantalotungstates with Remarkable Photocatalytic H2Evolution Activity181Cage clusters built from uranyl ions bridged through peroxo and 1-hydroxyethane-1,1-diphosphonic acid ligands26Hybrid Uranyl-Carboxyphosphonate Cage Clusters27Synthesis, Structures, and Properties of Uranyl Hybrids Constructed by a Variety of Mono- and Polycarboxylic Acids70MOFs of Uranium and the Actinides95Synthesis, crystal structure and photocatalytic properties of an unprecedented arsenic-disubstituted Lindqvist-type peroxopolyoxoniobate ion: {As 2 Nb 4 (O 2 ) 4 O 14 H 1.5 } 4.5−40A New Nb28Cluster Based on Tungstophosphate, [{Nb4O6(OH)4}{Nb6P2W12O61}4]36–50Hybrid Uranium–Transition-Metal Oxide Cage Clusters28Two new members of the niobium-substituted polytungstophosphate family based on hexalacunary [H 2 P 2 W 12 O 48 ] 12− building blocks37Assembly of tetrameric dimethyltin-functionalized selenotungstates: from nanoclusters to one-dimensional chains28Synthesis and oxidation catalysis of a Ti-substituted phosphotungstate, and identification of the active oxygen species31Unexpected Actinyl Cation-Directed Structural Variation in Neptunyl(VI) A-Type Tri-lacunary Heteropolyoxotungstate Complexes20Structure and Solution Speciation of UIV Linked Phosphomolybdate (MoV) Clusters21Oxo Clusters of 5f Elements24Time-Resolved X-ray Scattering and Raman Spectroscopic Studies of Formation of a Uranium-Vanadium-Phosphorus-Peroxide Cage Cluster24A new ring-shaped Cr-containing tungstophosphate based on [H2P2W12O48]12−4Synthesis and Solid-State Structure of Cyclobutyltellurium(IV)-Containing Dimeric Tungstoarsenates(III)2Recent advances in structural studies of heterometallic uranyl-containing coordination polymers and polynuclear closed species93Discovery of Heteropolytantalate: Synthesis and Structure of Two 6-Peroxotantalo-4-phosphate Clusters40Two Families of Rare-Earth-Substituted Dawson-type Monomeric and Dimeric Phosphotungstates Functionalized by Carboxylic Ligands25Microwave-assisted synthesis of organically functionalized hexa-molybdovanadates12Dimethyltin-functionalized cyclic selenotungstates based on {Se 2 W 12 } units8A new sandwich type transition metal complex based on tungstobismuthates and 1-methylimidazole ligands exhibiting photocatalytic properties1Complexation of tetravalent uranium cations by the As 4 W 40 O 140 cryptand12The homometallic polyoxotungstate archetype {P 4 W 24 }18Speciation of Actinide Complexes, Clusters, and Nanostructures in Solution2Polyoxometalates-based chiral frameworks involving helical motifs generated by spontaneous resolution4Charge Density Influence on Enthalpy of Formation of Uranyl Peroxide Cage Cluster Salts21Uranyl Cation Incorporation in the [P8W48O184]40– Macrocycle Phosphopolytungstate23Peroxo-Cerium(IV)-Containing Polyoxometalates: [CeIV6(O2)9(GeW10O37)3]24–, a Recyclable Homogeneous Oxidation Catalyst25Uranyl Incorporation into the Polyoxometalate Cavity. Synthesis and Characterization of [(UO2)8P8W48O184]24–11Synthèses, caractérisations et cristallochimie de polyoxométallates incorporant des actinides et des lanthanides comme simulants d’actinides0Supramolecular association of metal clusters with cyclodextrins : from interactions in solution to the design of mixed systems clusters-polyoxometalates.0Trends and new directions in the crystal chemistry of actinide oxo-clusters incorporated in polyoxometalates29Advances of transition-metal-modified {P2W12}-based polyoxometalates0An Ultrastable, Small {Ag7}5+ Nanocluster within a Triangular Hollow Polyoxometalate Framework91An Ultrastable, Small {Ag7}5+ Nanocluster within a Triangular Hollow Polyoxometalate Framework23Synthesis and Structural Characterization of Lanthanide‐Containing Polytungsto‐antimonate [{Sb3(µ3‐O)2Ln(H2O)Ln(H2O)2}2(SbW10O37)2(SbW8O31)2]22– Molecules Deriving from the Decomposition of the [Sb8W36O132]24– Macroanion2The potential study of ultra-high density heteropolysate solid free brine as well completion fluid for deep reservoir development18[(UO2)(C10H8N2O2)2][HPW12O40]: The First Case of a Uranyl Coordination Network Containing a Keggin‐Type Polyoxometalate5Peroxouranyl-Containing W48 Wheel: Synthesis, Structure, and Detailed Infrared and Raman Spectroscopy Study21Self-assembly of Keggin-type U( vi )-containing tungstophosphates with a sandwich structure: an efficient catalyst for the synthesis of sulfonyl pyrazoles61Sandwich-Type Uranyl Phosphate–Polyoxometalate Cluster Exhibiting Strong Luminescence34Effect of Na(I)-H2O clusters on self-assembly of sandwich-type U(VI)-containing silicotungstates and the efficient catalytic activity for the synthesis of substituted phenylsulfonyl-1H-pyrazoles25Two Dawson-type U(VI)-containing selenotungstates with sandwich structure and its high‐efficiency catalysis for pyrazoles27Recent advances in uranium-containing polyoxometalates59Synthesis and oxidation catalysis of a difluoride-incorporated polyoxovanadate and isolation of active vanadium alkylperoxo species12Two U(VI)-Containing Silicotungstates with Sandwich Structures: Lewis Acid–Base Synergistic Catalyzed Synthesis of Benzodiazepines and Pyrazoles26Uranyl-silicotungstate-containing hybrid building units {α-SiW 9 } and {γ-SiW 10 } with excellent catalytic activities in the three-component synthesis of dihydropyrimidin-2(1 H )-ones60Hexalacunary [α‐H2P2W12O48]12− Wells‐Dawson Anion: X‐ray Crystal Structural Evidence and Oligomerization to WO(OH2)4+‐Bridged Dimer and Trimers6Electrocatalytic Hydrogen Evolution by a Uranium(VI) Polyoxometalate: an Environmental Toxin for Sustainable Energy Generation11Organoarsonates Enable Single-Site Condensation of Hexalacunary {P2W12} Polyoxotungstates5Peroxo‐Zr/Hf‐Containing Wells‐Dawson Polyoxometalates for H2O2‐based Homogeneous, Heterogeneous, and Biphasic Oxidation Catalysis5Two sandwich‐type uranyl‐containing polytungstates catalyze aerobic synthesis of benzimidazoles41A uranium-bridged dimeric Keggin-type polyoxometalate and its proton conductive properties1Inorganic ligand-protected synthesis and characterization of a {Ag 6 } cluster within an annular polyoxometalate7Structural overview and evolution paths of lacunary polyoxometalates79Overview of Wells-Dawson Polyoxometalates: from structure and functionalization to application48The cyclic 48-tungsto-8-phosphate [H 7 P 8 W 48 O 184 ] 33− Contant–Tézé polyanion and its derivatives [H 6 P 4 W 24 O 94 ] 18− and [H 2 P 2 W 12 O 48 ] 12− : structural aspects and reactivity8Recent Advances in Polyoxometalate‒Metal Nanocluster Hybrids11Highly Shielded Peroxo‐Cerium(IV)‐Containing Polyoxometalate: Synthesis, Structure, and Oxidative Studies3Peroxo-Thorium(IV)-Containing Heteropolytungstates and Their Oxo-Analogues: Synthesis, Structure and Solution Studies1Organorhodium and Iridium-Containing Derivatives of the 48-Tungsto-8-phosphate Wheel: Synthesis, Characterization, and Catalytic Activity1Uranyl-Bridged Polyoxometalate Assembled from Te-Oriented Three-Layered Cage Clusters for Photocatalytic Oxy-Thiocyanation of Alkenes2Peroxo-Containing Heteropolyanions [{XW 3 O 7 (O 2 ) 2 } 2 O] 6– (X = HPO 4 2– , HAsO 4 2– , CH 3 AsO 3 2– ): Synthesis, Structure, and Antibacterial Properties0

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  1. The palladium(II)-decorated 22-tungsto-2-bismuthate(III), [Pd3(H2O)9Bi2W22O76]8−

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  2. ChemInform Abstract: Actinide Polyoxometalates: Incorporation of Uranyl—Peroxo in U‐Shaped 36‐Tungsto‐8‐phosphate.

    ChemInform · 2009-01-15

    Sib Sankar Mal, Michael H. Dickman, Ulrich Kortz

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  3. Symmetry versus Minimal Pentagonal Adjacencies in Uranium‐Based Polyoxometalate Fullerene Topologies

    Angewandte Chemie International Edition · 2009-03-04

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  4. Symmetry versus Minimal Pentagonal Adjacencies in Uranium‐Based Polyoxometalate Fullerene Topologies

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  5. A New Supramolecular Assembly Based on Triple-Dawson-Type Polyoxometalate and 3d-4f Heterometallic Cluster

    Inorganic Chemistry · 2009-06-18

    Yun‐Wu Li, Yangguang Li, Yonghui Wang, Xiao‐Jia Feng, Ying Jie Lu, Enbo Wang

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  6. Heterogeneous Wheel‐Shaped Cu20‐Polyoxotungstate [Cu20Cl(OH)24(H2O)12(P8W48O184)]25− Catalyst for Solvent‐Free Aerobic Oxidation of n‐Hexadecane

    Chemistry - A European Journal · 2009-06-23

    Lifang Chen, Juncheng Hu, Sib Sankar Mal, Ulrich Kortz, Helge Jaensch, Georges M. Mathys, Ryan M. Richards

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  7. A Remarkable Member of the Polyoxometalates: The Eight-Nickel-Capped α-Keggin Polyoxoazonickelate

    Inorganic Chemistry · 2009-07-15

    Lanjun Dong, Rudan Huang, Yongge Wei, Wei Chu

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  8. Syntheses and Crystal Structures of dmso‐Coordinated Tungstoantimonates(III) and ‐bismuthates(III)

    European Journal of Inorganic Chemistry · 2009-10-23

    Li‐Hua Bi, Guang‐Feng Hou, Ya‐Yan Bao, Bao Li, Lixin Wu, Zhong‐Min Gao, Timothy McCormac∥, Sib Sankar Mal, Michael H. Dickman, Ulrich Kortz

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  9. Crown and Bowl-Shaped Clusters of Uranyl Polyhedra

    Inorganic Chemistry · 2009-10-26

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  10. A new sandwich-type polyoxometalate constructed from penta-lacunary [HPW7O28]8− units and MnIII ion

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    Qiong Wu, Yangguang Li, Yonghui Wang, Yong-Hui Wang, Zhiming Zhang, Enbo Wang

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  11. Two Heterometallic Aggregates Constructed from the {P2W12}-Based Trimeric Polyoxotungstates and 3d-4f Heterometals

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    Shuang Yao, Zhiming Zhang, Yangguang Li, Ying Lü, Enbo Wang, Zhong‐Min Su

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  12. Coordination between [H2P2W12O48]12− and antimony(iii): synthesis and characterization of sandwich complex derived from the new {P2W13O51} fragment

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    Chundan Zhang, Shuxia Liu, Feng‐Ji Ma, Rui‐Kang Tan, Wei Zhang, Zhong‐Min Su

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  13. Mixed-valent vanadium substituted polyoxometalates: the wheel shaped [Rb3⊂{VVVIV3O7(H2O)6}2{H6P6W39O147(H2O)3}]15−

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  14. Polyoxometalates: Building Blocks for Functional Nanoscale Systems

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  15. Polyoxometallate als Bausteine für funktionelle Nanosysteme

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  16. Cobalt, Manganese, Nickel, and Vanadium Derivatives of the Cyclic 48-Tungsto-8-Phosphate [H7P8W48O184]33−

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  17. Reactivity of Polyoxoniobates in Acidic Solution: Controllable Assembly and Disassembly Based on Niobium‐Substituted Germanotungstates

    Chemistry - A European Journal · 2010-10-11

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  18. On the Origin of the Cation Templated Self-Assembly of Uranyl-Peroxide Nanoclusters

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  19. Liquid-Phase Selective Oxidation by Multimetallic Active Sites of Polyoxometalate-Based Molecular Catalysts

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  20. Structural peculiarities of actinyl complexation with monolacunary polyoxometalates

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  21. Low‐Symmetry Uranyl Pyrophosphate Cage Clusters

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  22. Silver(I)−Ethynide Clusters Constructed with Phosphonate-Functionized Polyoxovanadates

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  23. A comprehensive comparison of transition-metal and actinyl polyoxometalates

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  24. Two wheel-like polytungstates obtained by incorporation of two {Cu4} clusters and two molybdenum centers in the {W48} wheel

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  25. Uranyl peroxide pyrophosphate cage clusters with oxalate and nitrate bridges

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  26. Uranyl Peroxide Oxalate Cage and Core–Shell Clusters Containing 50 and 120 Uranyl Ions

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  27. {W48} Ring Opening: Fe16‐Containing, Ln4‐Stabilized 49‐Tungsto‐8‐Phosphate Open Wheel [Fe16O2(OH)23(H2O)9(P8W49O189)Ln4(H2O)20]11−

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  28. Uranyl Heteropolyoxometalate: Synthesis, Structure, and Spectroscopic Properties

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  29. Experimental and Computational Study of a New Wheel-Shaped {[W5O21]3[(UVIO2)2(μ-O2)]3}30–Polyoxometalate

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  31. Clusters of Actinides with Oxide, Peroxide, or Hydroxide Bridges

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  32. {Ta12}/{Ta16} Cluster-Containing Polytantalotungstates with Remarkable Photocatalytic H2Evolution Activity

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  33. Cage clusters built from uranyl ions bridged through peroxo and 1-hydroxyethane-1,1-diphosphonic acid ligands

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  34. Hybrid Uranyl-Carboxyphosphonate Cage Clusters

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  35. Synthesis, Structures, and Properties of Uranyl Hybrids Constructed by a Variety of Mono- and Polycarboxylic Acids

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  36. MOFs of Uranium and the Actinides

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  37. Synthesis, crystal structure and photocatalytic properties of an unprecedented arsenic-disubstituted Lindqvist-type peroxopolyoxoniobate ion: {As 2 Nb 4 (O 2 ) 4 O 14 H 1.5 } 4.5−

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  38. A New Nb28Cluster Based on Tungstophosphate, [{Nb4O6(OH)4}{Nb6P2W12O61}4]36–

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  39. Hybrid Uranium–Transition-Metal Oxide Cage Clusters

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  40. Two new members of the niobium-substituted polytungstophosphate family based on hexalacunary [H 2 P 2 W 12 O 48 ] 12− building blocks

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  41. Assembly of tetrameric dimethyltin-functionalized selenotungstates: from nanoclusters to one-dimensional chains

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  42. Synthesis and oxidation catalysis of a Ti-substituted phosphotungstate, and identification of the active oxygen species

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  43. Unexpected Actinyl Cation-Directed Structural Variation in Neptunyl(VI) A-Type Tri-lacunary Heteropolyoxotungstate Complexes

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  44. Structure and Solution Speciation of UIV Linked Phosphomolybdate (MoV) Clusters

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  45. Oxo Clusters of 5f Elements

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  46. Time-Resolved X-ray Scattering and Raman Spectroscopic Studies of Formation of a Uranium-Vanadium-Phosphorus-Peroxide Cage Cluster

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  47. A new ring-shaped Cr-containing tungstophosphate based on [H2P2W12O48]12−

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  48. Synthesis and Solid-State Structure of Cyclobutyltellurium(IV)-Containing Dimeric Tungstoarsenates(III)

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  49. Recent advances in structural studies of heterometallic uranyl-containing coordination polymers and polynuclear closed species

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    P. Thuéry, Jack McB. Harrowfield

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  50. Discovery of Heteropolytantalate: Synthesis and Structure of Two 6-Peroxotantalo-4-phosphate Clusters

    Inorganic Chemistry · 2017-05-03

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