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RESEARCH PAPER · Angewandte Chemie · 2000

Spectroscopy of the Formation of Microporous Transition Metal Ion Containing Aluminophosphates under Hydrothermal Conditions

Bert Marc Weckhuysen, David Baetens, Robert A. Schoonheydt

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Spectroscopy of the Formation of Microporous Transition Metal Ion Containing Aluminophosphates under Hydrothermal ConditionsOriginalSubstitution of transition metal ions into aluminophosphates and silicoaluminophosphates: characterization and relation to catalysis95Snapshots of a working catalyst: possibilities and limitations of in situ spectroscopy in the field of heterogeneous catalysis313Determining the active site in a catalytic process: Operando spectroscopy is more than a buzzword359Looking on Heterogeneous Catalytic Systems from Different Perspectives: Multitechnique Approaches as a New Challenge for In Situ Studies117Efficient Desymmetrization of “Pseudo”-C2-Symmetric Substrates: Illustration in the Synthesis of a Disubstituted Butenolide from Arabitol16In Situ NMR of SAPO-34 Crystallization120Facial Stereoselectivity in the Diels−Alder Reactions of (Arylethynyl)ethoxycarbenes of Group 6 with 1,2,3,4,5-Pentamethylcyclopenta-1,3-diene and Unusual Rearrangement of Strained Norbornadienyl Fischer Carbene Complexes of Chromium(0)31Solvent effects in the synthesis of CoAPO-5, -11 and -34 molecular sieves22High field ENDOR as a characterization tool for functional sites in microporous materials48Monitoring the coordination of aluminium during microporous oxide crystallisation by in situ soft X-ray absorption spectroscopy30A Combined SAXS/WAXS/XAFS Setup Capable of Observing Concurrent Changes Across the Nano-to-Micrometer Size Range in Inorganic Solid Crystallization Processes113An in situ XAS study on the incorporation of metal ions into AlPO4-5 framework in hydrothermal synthesis process0Understanding the crystallisation processes leading to the formation of microporous aluminophosphates2A Comparative Investigation of Co2+ and Mn2+ Incorporation into Aluminophosphates by in Situ XAS and DFT Computation8Implementation of a combined SAXS/WAXS/QEXAFS set-up for time-resolved in situ experiments26131P and 27Al NMR studies of aqueous (2-hydroxyethyl) trimethylammonium solutions containing aluminum and phosphorus11Chapter 3 Ultraviolet–Visible–Near Infrared Spectroscopy in Catalysis83Molecular engineering of microporous crystals: (I) New insight into the formation process of open-framework aluminophosphates26In Situ UV Raman Spectroscopic Study on the Synthesis Mechanism of AlPO‐584In Situ UV Raman Spectroscopic Study on the Synthesis Mechanism of AlPO‐524Tracking the formation of cobalt substituted ALPO-5 using simultaneous in situ X-ray diffraction and X-ray absorption spectroscopy techniques30UV Raman Spectroscopic Studies on Active Sites and Synthesis Mechanisms of Transition Metal-Containing Microporous and Mesoporous Materials166In situ electron paramagnetic resonance: a unique tool for analyzing structure–reactivity relationships in heterogeneous catalysis146Methods for in situ spectroscopic probing of the synthesis of a zeolite112The role of synchrotron radiation in examining the self-assembly of crystalline nanoporous framework materials: from zeolites and aluminophosphates to metal organic hybrids47Supported mesoporous solid base catalysts for condensation of carboxylic acids64Probing ZnAPO-34 Self-Assembly Using Simultaneous Multiple in Situ Techniques39Electronic Spectroscopy: Ultra Violet‐Visible and near IR Spectroscopies16Techniques Coupling for Catalyst Characterisation827Al and 31P NMR Investigations of Soluble Aluminophosphate Species in Alcohol–Water Mixtures2Molecular engineering of microporous crystals: (VI) Structure-directing effect in the crystallization process of layered aluminophosphates20Application of Operando XAS, XRD, and Raman Spectroscopy for Phase Speciation in Water Gas Shift Reaction Catalysts68Molecular engineering of microporous crystals: (VII) The molar ratio dependence of the structure-directing ability of piperazine in the crystallization of four aluminophosphates with open-frameworks21Time resolved in situ X-ray diffraction study of crystallisation processes of large pore nanoporous aluminophosphate materials6UV Raman Spectroscopic Characterization of Catalysts and Catalytic Active Sites53Single-Crystalline Organic–Inorganic Layered Cobalt Hydroxide Nanofibers: Facile Synthesis, Characterization, and Reversible Water-Induced Structural Conversion37Application of phosphorus-31 and aluminum-27 NMR spectroscopic techniques to study aqueous and methanolic solutions of tetraphenylammonium aluminophosphate2Design characteristics ofin situand operando ultraviolet-visible and vibrational spectroscopic reaction cells for heterogeneous catalysis36Coordination environment evolution of Co( ii ) during dehydration and re-crystallization processes of KCoPO 4 ·H 2 O towards enhanced electrocatalytic oxygen evolution reaction6

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  1. Substitution of transition metal ions into aluminophosphates and silicoaluminophosphates: characterization and relation to catalysis

    Research on Chemical Intermediates · 2002-01-01

    Martin Hartmann, Larry Kevan

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  2. Snapshots of a working catalyst: possibilities and limitations of in situ spectroscopy in the field of heterogeneous catalysis

    Chemical Communications · 2002-01-09

    Bert Marc Weckhuysen

    Read original paper ↗ ·

  3. Determining the active site in a catalytic process: Operando spectroscopy is more than a buzzword

    Physical Chemistry Chemical Physics · 2003-01-01

    Bert Marc Weckhuysen

    Read original paper ↗ ·

  4. Looking on Heterogeneous Catalytic Systems from Different Perspectives: Multitechnique Approaches as a New Challenge for In Situ Studies

    Catalysis Reviews · 2003-01-05

    Angelika Brückner

    Read original paper ↗ ·

  5. Efficient Desymmetrization of “Pseudo”-C2-Symmetric Substrates: Illustration in the Synthesis of a Disubstituted Butenolide from Arabitol

    The Journal of Organic Chemistry · 2003-02-01

    Bruno Linclau, A. James Boydell, Philip J. Clarke, Richard A. J. Horan, Claire Jacquet

    Read original paper ↗ ·

  6. In Situ NMR of SAPO-34 Crystallization

    Chemistry of Materials · 2003-03-29

    Ørnulv B. Vistad, Duncan E. Akporiaye, Françis Taulelle, Karl Petter Lillerud

    Read original paper ↗ ·

  7. Facial Stereoselectivity in the Diels−Alder Reactions of (Arylethynyl)ethoxycarbenes of Group 6 with 1,2,3,4,5-Pentamethylcyclopenta-1,3-diene and Unusual Rearrangement of Strained Norbornadienyl Fischer Carbene Complexes of Chromium(0)

    Organometallics · 2005-06-10

    Miguel Angel Vazquez, Leonor Reyes, René Miranda, Juventino J. Garcı́a, Hugo Alejandro Jiménez-Vázquez, Joaquı́n Tamariz, Francisco Delgado

    Read original paper ↗ ·

  8. Solvent effects in the synthesis of CoAPO-5, -11 and -34 molecular sieves

    Microporous and Mesoporous Materials · 2005-06-25

    Weibin Fan, Ruifeng Li, Tao Dou, Takashi Tatsumi, Bert Marc Weckhuysen

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  9. High field ENDOR as a characterization tool for functional sites in microporous materials

    Physical Chemistry Chemical Physics · 2006-01-01

    Daniella Goldfarb

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  10. Monitoring the coordination of aluminium during microporous oxide crystallisation by in situ soft X-ray absorption spectroscopy

    Chemical Communications · 2006-01-01

    Andrew Michael Beale, Ad M. J. van der Eerden, Didier Grandjean, Andrei V. Petukhov, Andy D. Smith, Bert Marc Weckhuysen

    Read original paper ↗ ·

  11. A Combined SAXS/WAXS/XAFS Setup Capable of Observing Concurrent Changes Across the Nano-to-Micrometer Size Range in Inorganic Solid Crystallization Processes

    Journal of the American Chemical Society · 2006-08-31

    Andrew Michael Beale, Ad M. J. van der Eerden, Simon D. M. Jacques, Olivier Leynaud, Matthew G. O’Brien, Florian Meneau, S. G. Nikitenko, Wim Bras, Bert Marc Weckhuysen

    Read original paper ↗ ·

  12. An in situ XAS study on the incorporation of metal ions into AlPO4-5 framework in hydrothermal synthesis process

    Studies in surface science and catalysis · 2007-01-01

    Mei Dong, Guofu Wang, Zhangfeng Qin, Jianguo Wang, Tao Liu, Yaning Xie, Tiandou Hu

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  13. Understanding the crystallisation processes leading to the formation of microporous aluminophosphates

    Studies in surface science and catalysis · 2007-01-01

    Andrew Michael Beale, Bert Marc Weckhuysen

    Read original paper ↗ ·

  14. A Comparative Investigation of Co2+ and Mn2+ Incorporation into Aluminophosphates by in Situ XAS and DFT Computation

    The Journal of Physical Chemistry A · 2007-02-02

    Mei Dong, Guofu Wang, Zhangfeng Qin, Jianguo Wang, Tao Liu, Shuping Yuan, Haijun Jiao

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  15. Implementation of a combined SAXS/WAXS/QEXAFS set-up for time-resolved in situ experiments

    Journal of Synchrotron Radiation · 2008-10-02

    Sergey Nikitenko, Andrew Michael Beale, Ad M. J. van der Eerden, Simon D. M. Jacques, Olivier Leynaud, Matthew G. O’Brien, Dirk Detollenaere, R. G. Kaptein, Bert Marc Weckhuysen, Wim Bras

    Read original paper ↗ ·

  16. 31P and 27Al NMR studies of aqueous (2-hydroxyethyl) trimethylammonium solutions containing aluminum and phosphorus

    Spectrochimica Acta Part A Molecular and Biomolecular Spectroscopy · 2008-10-22

    Abdolraouf Samadi‐Maybodi, Seyed Karim Hassani Nejad‐Darzi, Hamid Reza Bijanzadeh

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  17. Chapter 3 Ultraviolet–Visible–Near Infrared Spectroscopy in Catalysis

    Advances in catalysis · 2009-01-01

    Friederike C. Jentoft

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  18. Molecular engineering of microporous crystals: (I) New insight into the formation process of open-framework aluminophosphates

    Microporous and Mesoporous Materials · 2009-03-25

    Wenfu Yan, Xiaowei Song, Ruren Xu

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  19. In Situ UV Raman Spectroscopic Study on the Synthesis Mechanism of AlPO‐5

    Angewandte Chemie International Edition · 2009-10-13

    Fengtao Fan, Zhaochi Feng, Keju Sun, Meiling Guo, Qiang Guo, Yu Song, Wei‐Xue Li, Can Li

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  20. In Situ UV Raman Spectroscopic Study on the Synthesis Mechanism of AlPO‐5

    Angewandte Chemie · 2009-10-13

    Fengtao Fan, Zhaochi Feng, Keju Sun, Meiling Guo, Qiang Guo, Yu Song, Wei‐Xue Li, Can Li

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  21. Tracking the formation of cobalt substituted ALPO-5 using simultaneous in situ X-ray diffraction and X-ray absorption spectroscopy techniques

    Physical Chemistry Chemical Physics · 2009-11-13

    Kerry Simmance, Gopinathan Sankar, Robert G. Bell, Carmelo Prestipino, Wouter van Beek

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  22. UV Raman Spectroscopic Studies on Active Sites and Synthesis Mechanisms of Transition Metal-Containing Microporous and Mesoporous Materials

    Accounts of Chemical Research · 2009-12-22

    Fengtao Fan, Zhaochi Feng, Can Li

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  23. In situ electron paramagnetic resonance: a unique tool for analyzing structure–reactivity relationships in heterogeneous catalysis

    Chemical Society Reviews · 2010-01-01

    Angelika Brückner

    Read original paper ↗ ·

  24. Methods for in situ spectroscopic probing of the synthesis of a zeolite

    Chemical Society Reviews · 2010-01-01

    Alexander Aerts, Christine E. A. Kirschhock, Johan A. Martens

    Read original paper ↗ ·

  25. The role of synchrotron radiation in examining the self-assembly of crystalline nanoporous framework materials: from zeolites and aluminophosphates to metal organic hybrids

    Chemical Society Reviews · 2010-01-01

    Matthew G. O’Brien, Andrew Michael Beale, Bert Marc Weckhuysen

    Read original paper ↗ ·

  26. Supported mesoporous solid base catalysts for condensation of carboxylic acids

    Journal of Catalysis · 2011-01-24

    Ambareesh D. Murkute, James E. Jackson, Dennis J. Miller

    Read original paper ↗ ·

  27. Probing ZnAPO-34 Self-Assembly Using Simultaneous Multiple in Situ Techniques

    The Journal of Physical Chemistry C · 2011-03-07

    Andrew Michael Beale, Matthew G. O’Brien, Marta Kasunič, Amalija Golobič, Manuel Sánchez‐Sánchez, Alan J. W. Lobo, Dewi W. Lewis, David Stephen Wragg, Sergey Nikitenko, Wim Bras, Bert Marc Weckhuysen

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  28. Electronic Spectroscopy: Ultra Violet‐Visible and near IR Spectroscopies

    Unknown journal · 2012-04-04

    Friederike C. Jentoft

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  29. Techniques Coupling for Catalyst Characterisation

    Unknown journal · 2012-04-04

    Andrew Michael Beale, Matthew G. O’Brien, Bert Marc Weckhuysen

    Read original paper ↗ ·

  30. 27Al and 31P NMR Investigations of Soluble Aluminophosphate Species in Alcohol–Water Mixtures

    Journal of Solution Chemistry · 2012-05-21

    Abdolraouf Samadi‐Maybodi, Seyed Karim Hassani Nejad‐Darzi, Mohsen Tafazzoli

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  31. Molecular engineering of microporous crystals: (VI) Structure-directing effect in the crystallization process of layered aluminophosphates

    Microporous and Mesoporous Materials · 2012-07-15

    Xiaoqiang Tong, Jun Xu, Liang Xin, Pai Huang, Huiying Lü, Chao Wang, Wenfu Yan, Jihong Yu, Feng Deng, Huai Sun, Ruren Xu

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  32. Application of Operando XAS, XRD, and Raman Spectroscopy for Phase Speciation in Water Gas Shift Reaction Catalysts

    ACS Catalysis · 2012-09-17

    Anitha Patlolla, Emily V. Carino, Steven N. Ehrlich, Eli Stavitski, Anatoly I. Frenkel

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  33. Molecular engineering of microporous crystals: (VII) The molar ratio dependence of the structure-directing ability of piperazine in the crystallization of four aluminophosphates with open-frameworks

    Microporous and Mesoporous Materials · 2013-04-06

    Xiaoqiang Tong, Jun Xu, Xu Li, Yi Li, Wenfu Yan, Jihong Yu, Feng Deng, Huai Sun, Ruren Xu

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  34. Time resolved in situ X-ray diffraction study of crystallisation processes of large pore nanoporous aluminophosphate materials

    Faraday Discussions · 2014-10-22

    Kerry Simmance, Wouter van Beek, Gopinathan Sankar

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  35. UV Raman Spectroscopic Characterization of Catalysts and Catalytic Active Sites

    Catalysis Letters · 2014-11-11

    Shaoqing Jin, Zhaochi Feng, Fengtao Fan, Can Li

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  36. Single-Crystalline Organic–Inorganic Layered Cobalt Hydroxide Nanofibers: Facile Synthesis, Characterization, and Reversible Water-Induced Structural Conversion

    Inorganic Chemistry · 2014-11-26

    Xiaodi Guo, Lianying Wang, Shuang Lin Yue, Dongyang Wang, Yanluo Lu, Yu‐Fei Song, Jing He

    Read original paper ↗ ·

  37. Application of phosphorus-31 and aluminum-27 NMR spectroscopic techniques to study aqueous and methanolic solutions of tetraphenylammonium aluminophosphate

    Journal of Molecular Structure · 2016-09-06

    Nasser Goudarzi, Amir Hossein Amin

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  38. Design characteristics ofin situand operando ultraviolet-visible and vibrational spectroscopic reaction cells for heterogeneous catalysis

    Catalysis Reviews · 2017-09-25

    Juan J. Bravo-Suárez, Priya D. Srinivasan

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  39. Coordination environment evolution of Co( ii ) during dehydration and re-crystallization processes of KCoPO 4 ·H 2 O towards enhanced electrocatalytic oxygen evolution reaction

    RSC Advances · 2020-01-01

    Quande Che, Xiaobin Xie, Qian Ma, Junpeng Wang, Yuanna Zhu, Ruixia Shi, Ping Yang

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