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RESEARCH PAPER · Dalton Transactions · 2012

2-Dihydromethylpiperazinediium-M II (M II = Cu II , Fe II , Co II , Zn II ) double sulfates and their catalytic activity in diastereoselective nitroaldol (Henry) reaction

Houcine Naı̈li, Fadhel Hajlaoui, Tahar Mhiri, Tatiana C. O. Mac Leod, Maximilian N. Kopylovich, Kamran T. Mahmudov⧫, Armando J. L. Pombeiro

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2-Dihydromethylpiperazinediium-M II (M II = Cu II , Fe II , Co II , Zn II ) double sulfates and their catalytic activity in diastereoselective nitroaldol (Henry) reactionOriginalAqua complex of iron(III) and 5-chloro-3-(2-(4,4-dimethyl-2,6-dioxocyclohexylidene)hydrazinyl)-2-hydroxybenzenesulfonate: Structure and catalytic activity in Henry reaction54Inorganic–organic hybrid double sulfates as catalysts of the diastereoselective nitroaldol reaction23Zinc(II)-1,3,5-triazapentadienate complex as effective catalyst in Henry reaction53Double piperazinediium and 1,4-diazabicyclo[2.2.2]octanediium MII selenates (MII= CoII, NiII, CuII, ZnII) as effective catalysts for Henry reaction34Synthesis and characterization of robust three-dimensional chiral metal sulfates9Zinc metal–organic frameworks: efficient catalysts for the diastereoselective Henry reaction and transesterification99Synthesis, structure and catalytic applications of amidoterephthalate copper complexes in the diastereoselective Henry reaction in aqueous medium49A new cyclic binuclear Ni(II) complex as a catalyst towards nitroaldol (Henry) reaction27Amide functionalized metal–organic frameworks for diastereoselective nitroaldol (Henry) reaction in aqueous medium49Crystal structure determination, spectroscopic characterization and biological profile of a tailored ionic molecular entity, Sn( iv ) iminodiacetic acid–piperazinediium conjugate: in vitro DNA/RNA binding studies, Topo I inhibition activity, cytotoxic and systemic toxicity studies23Lanthanide derivatives comprising arylhydrazones of β-diketones: cooperative E/Z isomerization and catalytic activity in nitroaldol reaction52Sulfonated Schiff base dinuclear and polymeric copper( ii ) complexes: crystal structures, magnetic properties and catalytic application in Henry reaction62Zinc amidoisophthalate complexes and their catalytic application in the diastereoselective Henry reaction26CoII, NiII and UO2II complexes with β-diketones and their arylhydrazone derivatives: Synthesis, structure and catalytic activity in Henry reaction16Nanoporous lanthanide metal–organic frameworks as efficient heterogeneous catalysts for the Henry reaction46Copper(II) arylhydrazone complexes as catalysts for C H activation in the Henry reaction in water63Metal Azolate/Carboxylate Frameworks as Catalysts in Oxidative and C–C Coupling Reactions231D Zn(II) coordination polymer of arylhydrazone of 5,5-dimethylcyclohexane-1,3-dione as a pre-catalyst for the Henry reaction13Structural characterization and physicochemical features of a new arsenate salt templated by mono and di-protonated 4-aminopyridine cations: (C 5 H 7 N 2 )(C 5 H 8 N 2 )[AsO 4 ]·H 2 O12A porous two-dimensional Zn( ii )-coordination polymer exhibiting SC–SC transmetalation with Cu( ii ): efficient heterogeneous catalysis for the Henry reaction and detection of nitro explosives35Copper(II) coordination polymers of arylhydrazone of 1H-indene-1,3(2H)-dione linked by 4,4′-bipyridineor hexamethylenetetramine: Evaluation of catalytic activity in Henry reaction14Recent Advances and Perspectives on the Zinc‐Catalyzed Nitroaldol (Henry) Reaction41Solvothermal Syntheses, Crystal Structures and Catalytic Properties of Four Chiral Compounds Built from (R)‐4‐(4‐(1‐Carboxyethoxy)penoxy) Benzoic Acids5Nitroaldol reaction catalyzed by arylhydrazone di- and triorganotin(IV) complexes4Elementary and efficient catalyst process for the Knoevenagel condensation of araldehydes with arylmethylidene malononitrile8Cu6S6 Clusters as a Building Block for the Stabilization of Coordination Polymers with NiAs, NaCl, and Related Structures: Synthesis, Structure, and Catalytic Studies12A metalloligand appended with benzimidazole rings: tetranuclear [CoZn 3 ] and [CoCd 3 ] complexes and their catalytic applications19Synthesis and structural characterization of a novel dinuclear Cu( ii ) complex: an efficient and recyclable bifunctional heterogeneous catalyst for the diastereoselective Henry reaction30Synthesis, structural determination and antimicrobial evaluation of two novel CoII and ZnII halogenometallates as efficient catalysts for the acetalization reaction of aldehydes22Crystal packing, vibrational studies, DFT calculations of a new hybrid nickel (II)‐complex and its application in Heck and Sonogashira cross‐ coupling reactions9The Henry reaction catalyzed by NiII and CuII complexes bearing arylhydrazones of acetoacetanilide7Synthesis of Metallomacrocycle and Coordination Polymers with Pyridine‐Based Amidocarboxylate Ligands and Their Catalytic Activities towards the Henry and Knoevenagel Reactions29Synthesis, crystal structure and catalytic properties in the diastereoselective nitroaldol (Henry) reaction of new zinc(II) and cadmium(II) compounds5Synthesis and structures of copper complexes bearing unsymmetric derivatives of (R,R)‐1,2‐diaminocyclohexane: An efficient catalyst for asymmetric Henry reaction7Ni(II)-Aroylhydrazone Complexes as Catalyst Precursors Towards Efficient Solvent-Free Nitroaldol Condensation Reaction16Hybrid nanomaterials for asymmetric purposes: green enantioselective C–C bond formation by chiralization and multi-functionalization approaches20Environmentally benign benzyl alcohol oxidation and C-C coupling catalysed by amide functionalized 3D Co(II) and Zn(II) metal organic frameworks82Lamellar and Supramolecular Feature of New Tutton’s Salts Incorporating 2-Amino-4-Methylpyrimidine: Thermal Stability, Optic Study, Antioxidant and Antimicrobial Activities19A novel sulfate-bridged binuclear copper( ii ) complex: structure, optical, ADMET and in vivo approach in a murine model of bone metastasis44Synthesis, crystal structures, Hirshfeld surface analysis and physico-chemical characterization of two new ZnII and CdII halidometallates11Design, synthesis and physico-chemical studies of a Co(II)/Co(III) mixed-valence complex: An experimental and DFT approach25Single-Crystal-to-Single-Crystal Transformation and Catalytic Properties of New Hybrid Perhalidometallates5Single Nickel sites - easy separation and high-performance catalyst for the production of β-Nitro alcohols10Co(II) and 2-amino-perimidinium based new generation hybrid material promoted facile dimerization of aroyl chloride: A route to α-diketone9Solvent-dependent hypsochromic shift in the imidazole based complex [Cu(µ2-SO4)(Im)4] and ameliorative effects on breast cancer-induced bone metastases associated oxidative injury in rats0Tridentate ONO hydrazone Schiff base complexes in organic transformations: Catalytic and mechanistic studies56Temperature-dependent IR and dielectric properties, and DFT calculations (FMOs and ELF), of 2-amino-3-nitropyridinium hydrogen sulfate monohydrate5New Cobalt and Nickel Sulfates Templated with N,N'-Dimethyletethylenediammonium Cation: Synthesis, Crystal Structures, and Topological Features1Double sulfates with 1-methylpiperazinediium and divalent cations: Synthesis, structures, spectroscopic characterization, thermal stability, and topological features of (C5H14N2)[M(H2O)6](SO4)2∙H2O (M = Mg, Mn, Fe, Co, Ni, Zn, and Cd) and (C5H14N2)(SO4)∙H2O2

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  1. Aqua complex of iron(III) and 5-chloro-3-(2-(4,4-dimethyl-2,6-dioxocyclohexylidene)hydrazinyl)-2-hydroxybenzenesulfonate: Structure and catalytic activity in Henry reaction

    Journal of Molecular Structure · 2013-05-29

    Kamran T. Mahmudov⧫, Maximilian N. Kopylovich, Matti Haukka, Gunay S. Mahmudova, Espandi F. Esmaeila, Famil Musa Chyragov, Armando J. L. Pombeiro

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  2. Inorganic–organic hybrid double sulfates as catalysts of the diastereoselective nitroaldol reaction

    Journal of Organometallic Chemistry · 2013-05-31

    Omar Kammoun, Walid Rekik, Thierry Bataille B, Kamran T. Mahmudov⧫, Maximilian N. Kopylovich, Houcine Naı̈li

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  3. Zinc(II)-1,3,5-triazapentadienate complex as effective catalyst in Henry reaction

    Catalysis Today · 2013-07-24

    Namiq Q. Shikhaliyev, Abel Mammadali Maharramov, Atash V. Gurbanov, Valentine G. Nenajdenko, Vasiliy M. Muzalevskiy, Kamran T. Mahmudov⧫, Maximilian N. Kopylovich

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  4. Double piperazinediium and 1,4-diazabicyclo[2.2.2]octanediium MII selenates (MII= CoII, NiII, CuII, ZnII) as effective catalysts for Henry reaction

    Inorganica Chimica Acta · 2013-12-21

    Nouha Loulou Nkhili, Walid Rekik, Tahar Mhiri, Kamran T. Mahmudov⧫, Maximilian N. Kopylovich, Houcine Naı̈li

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  5. Synthesis and characterization of robust three-dimensional chiral metal sulfates

    RSC Advances · 2014-01-01

    J. N. Behera, Joydeep Bhattacharjee, Satoshi Horike, Subba R. Marri, Prem Prakash Dahiya

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  6. Zinc metal–organic frameworks: efficient catalysts for the diastereoselective Henry reaction and transesterification

    Dalton Transactions · 2014-01-01

    Anirban Karmakar, Maria Fátima C. Guedes da Silva, Armando J. L. Pombeiro

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  7. Synthesis, structure and catalytic applications of amidoterephthalate copper complexes in the diastereoselective Henry reaction in aqueous medium

    New Journal of Chemistry · 2014-07-29

    Anirban Karmakar, Susanta Hazra, Maria Fátima C. Guedes da Silva, Armando J. L. Pombeiro

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  8. A new cyclic binuclear Ni(II) complex as a catalyst towards nitroaldol (Henry) reaction

    Catalysis Communications · 2014-08-19

    Manas Sutradhar, Maria Fátima C. Guedes da Silva, Armando J. L. Pombeiro

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  9. Amide functionalized metal–organic frameworks for diastereoselective nitroaldol (Henry) reaction in aqueous medium

    RSC Advances · 2015-01-01

    Anup Paul, Anirban Karmakar, Maria Fátima C. Guedes da Silva, Armando J. L. Pombeiro

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  10. Crystal structure determination, spectroscopic characterization and biological profile of a tailored ionic molecular entity, Sn( iv ) iminodiacetic acid–piperazinediium conjugate: in vitro DNA/RNA binding studies, Topo I inhibition activity, cytotoxic and systemic toxicity studies

    RSC Advances · 2015-01-01

    Farukh Arjmand, Imtiyaz Yousuf, Yusra Zaidi, L. J. TOUPET

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  11. Lanthanide derivatives comprising arylhydrazones of β-diketones: cooperative E/Z isomerization and catalytic activity in nitroaldol reaction

    Dalton Transactions · 2015-01-01

    Kamran T. Mahmudov⧫, Maria Fátima C. Guedes da Silva, Manas Sutradhar, Maximilian N. Kopylovich, Fatali E. Huseynov, N.T. Shamilov, Anna A. Voronina, Tatyana M. Buslaeva, Armando J. L. Pombeiro

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  12. Sulfonated Schiff base dinuclear and polymeric copper( ii ) complexes: crystal structures, magnetic properties and catalytic application in Henry reaction

    New Journal of Chemistry · 2015-01-01

    Susanta Hazra, Anirban Karmakar, Maria Fátima C. Guedes da Silva, Ľubor Dlháň, Roman Boča, Armando J. L. Pombeiro

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  13. Zinc amidoisophthalate complexes and their catalytic application in the diastereoselective Henry reaction

    New Journal of Chemistry · 2015-01-01

    Anirban Karmakar, Maria Fátima C. Guedes da Silva, Susanta Hazra, Armando J. L. Pombeiro

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  14. CoII, NiII and UO2II complexes with β-diketones and their arylhydrazone derivatives: Synthesis, structure and catalytic activity in Henry reaction

    Polyhedron · 2015-07-26

    Zhen Ma, Manas Sutradhar, Atash V. Gurbanov, Abel Mammadali Maharramov, Rafiga A. Aliyeva, Farqana S. Aliyeva, F. N. Bahmanova, В.И. Марданова, Famil Musa Chyragov, Kamran T. Mahmudov⧫

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  15. Nanoporous lanthanide metal–organic frameworks as efficient heterogeneous catalysts for the Henry reaction

    CrystEngComm · 2016-01-01

    Anirban Karmakar, Susanta Hazra, Maria Fátima C. Guedes da Silva, Anup Paul, Armando J. L. Pombeiro

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  16. Copper(II) arylhydrazone complexes as catalysts for C H activation in the Henry reaction in water

    Journal of Molecular Catalysis A Chemical · 2016-06-05

    Zhen Ma, Atash V. Gurbanov, Abel Mammadali Maharramov, Firudin I. Guseinov, Maximilian N. Kopylovich, Fedor Ivanovich Zubkov, Kamran T. Mahmudov⧫, Armando J. L. Pombeiro

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  17. Metal Azolate/Carboxylate Frameworks as Catalysts in Oxidative and C–C Coupling Reactions

    Inorganic Chemistry · 2016-06-06

    Aurel Tăbăcaru, Nertil Xhaferaj, Luísa M. D. R. S. Martins, Elisabete C. B. A. Alegria, Rogério S. Chay, Carlotta Giacobbe, K.V. Domasevitch, Armando J. L. Pombeiro, Simona Galli, Claudio Pettinari

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  18. 1D Zn(II) coordination polymer of arylhydrazone of 5,5-dimethylcyclohexane-1,3-dione as a pre-catalyst for the Henry reaction

    Catalysis Communications · 2016-09-09

    Nuno M. R. Martins, Kamran T. Mahmudov⧫, Maria Fátima C. Guedes da Silva, Luísa M. D. R. S. Martins, Firudin I. Guseinov, Armando J. L. Pombeiro

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  19. Structural characterization and physicochemical features of a new arsenate salt templated by mono and di-protonated 4-aminopyridine cations: (C 5 H 7 N 2 )(C 5 H 8 N 2 )[AsO 4 ]·H 2 O

    Physica E Low-dimensional Systems and Nanostructures · 2016-11-28

    Noureddine Mhadhbi, Houcine Naı̈li, Khaled Jarraya

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  20. A porous two-dimensional Zn( ii )-coordination polymer exhibiting SC–SC transmetalation with Cu( ii ): efficient heterogeneous catalysis for the Henry reaction and detection of nitro explosives

    Dalton Transactions · 2017-01-01

    Mayank Gupta, Dinesh De, Sanchari Pal, Tapan K. Pal, Kapil Tomar

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  21. Copper(II) coordination polymers of arylhydrazone of 1H-indene-1,3(2H)-dione linked by 4,4′-bipyridineor hexamethylenetetramine: Evaluation of catalytic activity in Henry reaction

    Polyhedron · 2017-05-17

    Gonçalo A. O. Tiago, Kamran T. Mahmudov⧫, Maria Fátima C. Guedes da Silva, Ana P. C. Ribeiro, Fatali E. Huseynov, Luís Cobra Branco, Armando J. L. Pombeiro

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  22. Recent Advances and Perspectives on the Zinc‐Catalyzed Nitroaldol (Henry) Reaction

    Asian Journal of Organic Chemistry · 2017-06-21

    Salim Saranya, Nissy Ann Harry, Sankuviruthiyil M. Ujwaldev, Gopinathan Nair Anilkumar

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  23. Solvothermal Syntheses, Crystal Structures and Catalytic Properties of Four Chiral Compounds Built from (R)‐4‐(4‐(1‐Carboxyethoxy)penoxy) Benzoic Acids

    ChemistrySelect · 2017-08-22

    Xuewei Li, Han‐Zhong Zhang, Guang‐Feng Hou, Xin Fang Xu, Ying‐Hui Yu, Jin‐Sheng Gao

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  24. Nitroaldol reaction catalyzed by arylhydrazone di- and triorganotin(IV) complexes

    Journal of Organometallic Chemistry · 2017-10-04

    Atash V. Gurbanov, Maria Fátima C. Guedes da Silva, Leonid Modestovich Kustov, Firudin I. Guseinov, Kamran T. Mahmudov⧫, Armando J. L. Pombeiro

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  25. Elementary and efficient catalyst process for the Knoevenagel condensation of araldehydes with arylmethylidene malononitrile

    Inorganica Chimica Acta · 2017-10-27

    Raja Jlassi, Ana P. C. Ribeiro, Gonçalo A. O. Tiago, Jiawei Wang, Marta S. Krawczyk, Luísa M. D. R. S. Martins, Houcine Naı̈li, Armando J. L. Pombeiro, Walid Rekik

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  26. Cu6S6 Clusters as a Building Block for the Stabilization of Coordination Polymers with NiAs, NaCl, and Related Structures: Synthesis, Structure, and Catalytic Studies

    European Journal of Inorganic Chemistry · 2017-11-30

    Ajay Kumar Jana, Srinivasan Natarajan

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  27. A metalloligand appended with benzimidazole rings: tetranuclear [CoZn 3 ] and [CoCd 3 ] complexes and their catalytic applications

    New Journal of Chemistry · 2018-01-01

    Saurabh Kumar Pandey, Deepak Bansal, Rajeev Gupta

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  28. Synthesis and structural characterization of a novel dinuclear Cu( ii ) complex: an efficient and recyclable bifunctional heterogeneous catalyst for the diastereoselective Henry reaction

    Dalton Transactions · 2018-01-01

    Datta Markad, Sanjay K. Mandal

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  29. Synthesis, structural determination and antimicrobial evaluation of two novel CoII and ZnII halogenometallates as efficient catalysts for the acetalization reaction of aldehydes

    Chemistry Central Journal · 2018-02-28

    Assila Maâtar Ben Salah, Lilia Belghith‐Fendri, Thierry Bataille B, Raquel P. Herrera, Houcine Naı̈li

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  30. Crystal packing, vibrational studies, DFT calculations of a new hybrid nickel (II)‐complex and its application in Heck and Sonogashira cross‐ coupling reactions

    Applied Organometallic Chemistry · 2018-04-06

    Rim Jaballi, Wassim Maalej, Dhieb Atoui, Habib Feki, Ridha Ben Salem, Zakaria Elaoud

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  31. The Henry reaction catalyzed by NiII and CuII complexes bearing arylhydrazones of acetoacetanilide

    Journal of Organometallic Chemistry · 2018-05-31

    Atash V. Gurbanov, Susanta Hazra, Abel Mammadali Maharramov, Fedor Ivanovich Zubkov, Firudin I. Guseinov, Armando J. L. Pombeiro

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  32. Synthesis of Metallomacrocycle and Coordination Polymers with Pyridine‐Based Amidocarboxylate Ligands and Their Catalytic Activities towards the Henry and Knoevenagel Reactions

    ChemistryOpen · 2018-11-01

    Anirban Karmakar, Guilherme M. D. M. Rúbio, Maria Fátima C. Guedes da Silva, Armando J. L. Pombeiro

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  33. Synthesis, crystal structure and catalytic properties in the diastereoselective nitroaldol (Henry) reaction of new zinc(II) and cadmium(II) compounds

    Polyhedron · 2018-11-03

    Raja Jlassi, Ahmed Khalladi, Houcine Naı̈li, Tobias Rüffer, Heinrich Lang, Walid Rekik

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  34. Synthesis and structures of copper complexes bearing unsymmetric derivatives of (R,R)‐1,2‐diaminocyclohexane: An efficient catalyst for asymmetric Henry reaction

    Applied Organometallic Chemistry · 2019-05-07

    Juhyun Cho, Min Kyung Chun, Saira Nayab, Jong Hwa Jeong

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  35. Ni(II)-Aroylhydrazone Complexes as Catalyst Precursors Towards Efficient Solvent-Free Nitroaldol Condensation Reaction

    Catalysts · 2019-06-20

    Manas Sutradhar, Tannistha Roy Barman, Armando J. L. Pombeiro, Luísa M. D. R. S. Martins

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  36. Hybrid nanomaterials for asymmetric purposes: green enantioselective C–C bond formation by chiralization and multi-functionalization approaches

    Catalysis Science & Technology · 2020-01-01

    Sayed Ali Akbar Razavi, Kayhaneh Berijani, Ali Morsali

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  37. Environmentally benign benzyl alcohol oxidation and C-C coupling catalysed by amide functionalized 3D Co(II) and Zn(II) metal organic frameworks

    Journal of Catalysis · 2020-04-13

    Anup Paul, Luísa M. D. R. S. Martins, Anirban Karmakar, Maxim L. Kuznetsov, Alexander S. Novikov, Maria Fátima C. Guedes da Silva, Armando J. L. Pombeiro

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  38. Lamellar and Supramolecular Feature of New Tutton’s Salts Incorporating 2-Amino-4-Methylpyrimidine: Thermal Stability, Optic Study, Antioxidant and Antimicrobial Activities

    Journal of Inorganic and Organometallic Polymers and Materials · 2020-11-16

    Nabil Hfidhi, Najeh Krayem, Erwann Jeanneau B, Thierry Bataille B, Houcine Naı̈li

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  39. A novel sulfate-bridged binuclear copper( ii ) complex: structure, optical, ADMET and in vivo approach in a murine model of bone metastasis

    New Journal of Chemistry · 2021-01-01

    Khouloud Hchicha, Marcus Korb, Riadh Badraoui, Houcine Naı̈li

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  40. Synthesis, crystal structures, Hirshfeld surface analysis and physico-chemical characterization of two new ZnII and CdII halidometallates

    Journal of Materials Science Materials in Electronics · 2021-03-29

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  41. Design, synthesis and physico-chemical studies of a Co(II)/Co(III) mixed-valence complex: An experimental and DFT approach

    Journal of Molecular Structure · 2021-04-07

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  42. Single-Crystal-to-Single-Crystal Transformation and Catalytic Properties of New Hybrid Perhalidometallates

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  43. Single Nickel sites - easy separation and high-performance catalyst for the production of β-Nitro alcohols

    Separation and Purification Technology · 2022-03-08

    Yu‐Chang Huang, Qiankun Hou, De Ding, Nan Qing Yang, Yin Chen

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  44. Co(II) and 2-amino-perimidinium based new generation hybrid material promoted facile dimerization of aroyl chloride: A route to α-diketone

    Journal of Molecular Structure · 2022-08-24

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  45. Solvent-dependent hypsochromic shift in the imidazole based complex [Cu(µ2-SO4)(Im)4] and ameliorative effects on breast cancer-induced bone metastases associated oxidative injury in rats

    Arabian Journal of Chemistry · 2023-05-18

    Khouloud Hchicha, Elena Cambiotti, Hmed Ben‐Nasr, Daniel Chappard, Matti Haukka, Loredana Latterini, Salem Elkahoui, Arif Jamal Siddiqui, Mejdi Snoussi, Mohd Adnan, Houcine Naı̈li, Riadh Badraoui

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  46. Tridentate ONO hydrazone Schiff base complexes in organic transformations: Catalytic and mechanistic studies

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  47. Temperature-dependent IR and dielectric properties, and DFT calculations (FMOs and ELF), of 2-amino-3-nitropyridinium hydrogen sulfate monohydrate

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  48. New Cobalt and Nickel Sulfates Templated with N,N'-Dimethyletethylenediammonium Cation: Synthesis, Crystal Structures, and Topological Features

    Crystallography Reports · 2025-06-01

    Dmitri O. Charkin, V. E. Kireev, Н. В. Сомов, Dmitri N. Dmitriev, A. M. Banaru, Sergey M. Aksenov

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  49. Double sulfates with 1-methylpiperazinediium and divalent cations: Synthesis, structures, spectroscopic characterization, thermal stability, and topological features of (C5H14N2)[M(H2O)6](SO4)2∙H2O (M = Mg, Mn, Fe, Co, Ni, Zn, and Cd) and (C5H14N2)(SO4)∙H2O

    Polyhedron · 2025-09-05

    Dmitri O. Charkin, Alevtina N. Gosteva, Vadim A. Kireev, A. M. Banaru, Dmitri N. Dmitriev, Dina V. Deyneko, Nikita Sergeyevich Tsvetov, Ivan Gundarovich Tananaev, Sergey M. Aksenov

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