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RESEARCH PAPER · The Journal of Physical Chemistry B · 2000

An in Situ Energy-Dispersive X-ray Diffraction Study of the Hydrothermal Crystallization of Zeolite A. 1. Influence of Reaction Conditions and Transformation into Sodalite

Richard I. Walton, Franck Millange, Dermot O’Hare, Andrew T. Davies, Gopinathan Sankar, C. Richard A. Catlow

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An in Situ Energy-Dispersive X-ray Diffraction Study of the Hydrothermal Crystallization of Zeolite A. 1. Influence of Reaction Conditions and Transformation into SodaliteOriginalAn X-ray absorption fine structure study of amorphous precursors of a gallium silicate zeolite19Identification of a Key Precursor Phase for Synthesis of SAPO-34 and Kinetics of Formation Investigated by in Situ X-ray Diffraction73Anomalous wide angle X-ray scattering (AWAXS) and heterogeneous catalysts50In‐Situtime‐resolved X‐ray diffraction: The current state of the art11Mechanism of the Transformation of Silica Precursor Solutions into Si-MFI Zeolite127Following the formation of nanometer-sized clusters by time-resolved SAXS and EXAFS techniques22An in situ study of crystallisation gradients during the hydrothermal/autoclave synthesis of zeolites8Nanosized Molecular Sieves26Modeling Nucleation and Growth in Zeolites4In situ waxs-saxs synchrotron study of the kinetics of nucleation and growth in linde type-a zeolite (LTA)3SYNTHESIS AND KINETIC STUDY OF ZEOLITE FROM LOPBURI PERLITE8Observation and Reactivity of the Chainlike Species ([Al(PO4)2]3-)n during the X-ray Diffraction Investigation of the Hydrothermal Synthesis of the Super-sodalite Sodium Aluminophosphate MIL-74 (Na2Al7(PO4)12·4trenH3·Na(H2O)16)42In situ diagnostics of zeolite crystallization by ultrasonic monitoring22Trivalent Atom Contribution on Solid−Solid Transformation of Ga13 Polycation Intercalated Clay into Sodalite Investigated by X-ray Absorption Spectroscopy6Do Geopolymers Actually Contain Nanocrystalline Zeolites? A Reexamination of Existing Results818Effects of step-change of synthesis temperature on synthesis of zeolite 4A from coal fly ash118On the mechanism of zeolite growing: Crystallization by seeding with delayered zeolites48In-situ XRD as a tool to understanding zeolite crystallization105Enhanced Resonator Sensitivity with Nanostructured Porous Silica Coatings7Direct measurement of the kinetics of geopolymerisation by in-situ energy dispersive X-ray diffractometry60In situ studies of the crystallisation of microporous materials using synchrotron radiation based X-ray techniques0In-situ ultrasonic methods for monitoring the hydrothermal synthesis of LTA-type zeolite from colloidal solutions9In Situ SAXS/WAXS of Zeolite Microwave Synthesis: NaY, NaA, and Beta Zeolites39Monitoring of crystallization processes during synthesis of zeolite A by in situ 27Al NMR spectroscopy29Structure Determination: Experimental Techniques1Effect of Organic Templates on the Kinetics and Crystallization of Microporous Metal-Substituted Aluminophosphates24Structural Effects of Solvents on the Breathing of Metal–Organic Frameworks: An In Situ Diffraction Study210Structural Effects of Solvents on the Breathing of Metal–Organic Frameworks: An In Situ Diffraction Study47Synthesis of Nanometer-Sized Sodalite Without Adding Organic Additives78Viscosity sensing in heated alkaline zeolite synthesis media24Kinetic analysis of experimental intensity curves obtained during zeolite a synthesis using in situ 27Al NMR spectroscopy4Time and position resolved in situ X-ray diffraction study of the hydrothermal conversion of gypsum monoliths to hydroxyapatite11Role of Germanium on the Nucleation and Growth of Zeolite A from Clear Solutions As Studied by in Situ Small-Angle X-ray Scattering, Wide-Angle X-ray Scattering, and Dynamic Light Scattering17The polymorphs and solvates of phenylbutazone and their phase transition behaviour0Early Stage Reversed Crystal Growth of Zeolite A and Its Phase Transformation to Sodalite150In Situ XAS and XRPD Parametric Rietveld Refinement To Understand Dealumination of Y Zeolite Catalyst205Time‐Resolved In Situ Diffraction Study of the Solvothermal Crystallization of Some Prototypical Metal–Organic Frameworks220Time‐Resolved In Situ Diffraction Study of the Solvothermal Crystallization of Some Prototypical Metal–Organic Frameworks51Methods for in situ spectroscopic probing of the synthesis of a zeolite112The role of synchrotron radiation in examining the self-assembly of crystalline nanoporous framework materials: from zeolites and aluminophosphates to metal organic hybrids47Effect of curing temperature on the development of hard structure of metakaolin-based geopolymer1020Genesis of bismuth molybdenum oxide catalyst followed by in-situ techniques and its use in catalytic dense membrane reactor0Time-resolved in situ studies of apatite formation in aqueous solutions41A time-resolved diffraction study of a window of stability in the synthesis of a copper carboxylate metal–organic framework154Oberflächenchemie Metall‐organischer Gerüste an der Flüssig‐fest‐Grenzfläche43Surface Chemistry of Metal–Organic Frameworks at the Liquid–Solid Interface318Role of ethanol in sodalite crystallization in an ethanol–Na2O–Al2O3–SiO2–H2O system31The application of statistical methodology to the analysis of time-resolved X-ray diffraction data12Zeolites X and A crystallization compared by simultaneous UV/VIS-Raman and X-ray diffraction51In‐Situ Monitoring of the Formation of Crystalline Solids251In‐situ‐Verfolgung der Bildung kristalliner Feststoffe69Hollow sodalite spheres synthesized in a first-closed then-open system from the synthesis gels aged under ultrahigh pressures10Zeolite metastability as a function of the composition of the surrounding solution: The case of faujasite and zeolite omega14High‐Throughput and Time‐Resolved Energy‐Dispersive X‐Ray Diffraction (EDXRD) Study of the Formation of CAU‐1‐(OH) 2 : Microwave and Conventional Heating94Uptake of Liquid Alcohols by the Flexible Fe III Metal–Organic Framework MIL‐53 Observed by Time‐Resolved In Situ X‐ray Diffraction47An investigation of the mechanisms of goethite, hematite and magnetite-seeded Al(OH)3 precipitation from synthetic Bayer liquor20High-Throughput and in Situ Energy Dispersive X-ray Diffraction Investigation on the Formation of the New Metal Organogermanate Cu(OOCC2H4Ge)2O319Formate modulated solvothermal synthesis of ZIF-8 investigated using time-resolved in situ X-ray diffraction and scanning electron microscopy368Synthesis of isoreticular CAU-1 compounds: effects of linker and heating methods on the kinetics of the synthesis45Convenient Hydrothermal Synthesis of Zeolite a from Potassium-Extracted Residue of Potassium Feldspar7NaA zeolite cubic crystal formation and deformation: cubes with crystalline core, simultaneous growth of surface and core crystals, and layer-by-layer destruction34Synthesis, Structure, and Crystallization Study of a Layered Lithium Thiophene-Dicarboxylate39High-throughput and in situ EDXRD investigation on the formation of two new metal aminoethylphosphonates – Ca(O3PC2H4NH2) and Ca(OH)(O3PC2H4NH3)·2H2O21Effects of organic additives on crystallization process and the adsorption performances of zeolite A15In situ ultrasonic monitoring of zeolite A crystallization from coal fly ash63On the Complexity of Crystallization of Thioantimonates: In‐situ Energy Dispersive X‐ray Diffraction (EDXRD) Studies of the Solvothermal Formation of the Isostructural Thioantimonates [TM(tren)Sb4S7] (TM = Fe, Zn)16Applications of in situ synchrotron XRD in hydrometallurgy: Literature review and investigation of chalcopyrite dissolution45A two-phase segmented microfluidic technique for one-step continuous versatile preparation of zeolites43Nucleation and growth process of sodalite and cancrinite from kaolinite-rich clay under low-temperature hydrothermal conditions110In situ ultrasonic diagnostic of zeolite X crystallization with novel (hierarchical) morphology from coal fly ash26Crystallisation Kinetics of Metal Organic Frameworks From in situ Time-Resolved X-ray Diffraction59Recent Trends in Operando and In Situ Characterization: Techniques for Rational Design of Catalysts6In-situ ultrasound study of the kinetics of formation of zeolites Na–A and Na–X from coal fly ash12Determination of the electronic and structural configuration of coordination compounds by synchrotron-radiation techniques109In Situ Powder Diffraction Study of the Hydrothermal Synthesis of ZnO Nanoparticles49In situ 27Al NMR kinetic investigation of zeolite A crystallization24New Stories of Zeolite Structures: Their Descriptions, Determinations, Predictions, and Evaluations600Understanding Solvothermal Crystallization of Mesoporous Anatase Beads by In Situ Synchrotron PXRD and SAXS40Synthesis of ZIF-8 from recycled mother liquors79Microwave synthesis of LTN framework zeolite with no organic structure directing agents14An investigation of the crystallization kinetics of zeotype SAPO-34 crystals synthesized by hydrothermal and sonochemical methods32Hydrothermal synthesis of zeolite A from K-feldspar and its crystallization mechanism93Assembly and Evolution of Amorphous Precursors in Zeolite L Crystallization94Synthesis and strength optimization of one-part geopolymer based on red mud363The First 20 Hours of Geopolymerization: An in Situ WAXS Study of Flyash-Based Geopolymers14In Situ Time-Resolved Observation of the Development of Intracrystalline Mesoporosity in USY Zeolite41Synthesis and characterization of iodosodalite49Continuous Hydrothermal Synthesis of Inorganic Nanoparticles: Applications and Future Directions614Phase Formation and Evolution in Mg(OH)2–Zeolite Cements16Simple approach in understanding interzeolite transformations using ring building units25Highly Photoluminescent Sulfide Clusters Confined in Zeolites16Monitoring the Hydrothermal Growth of Cobalt Spinel Water Oxidation Catalysts: From Preparative History to Catalytic Activity20Diverse Physical States of Amorphous Precursors in Zeolite Synthesis74Development of LTA zeolite membrane from clay by sonication assisted method at room temperature for H2-CO2 and CO2-CH4 separation59Lepidocrocite-Type Titanate Formation from Isostructural Prestructures under Hydrothermal Reactions: Observation by Synchrotron X-ray Total Scattering Analyses51Influence of Synthesis Method on LTA Time-Dependent Stability21Solid-State NMR Studies of Zeolites and Zeotype Materials Synthesis0Exploratory Synthesis of Low-Silica Nanozeolites through Geopolymer Chemistry18A kinetic and mechanistic study into the transformation of calcium sulfate hemihydrate to dihydrate40Recent advances in zeolite-encapsulated metal catalysts: A suitable catalyst design for catalytic biomass conversion65The effect of boron on zeolite-4A immobilization of iodine waste forms with a novel preparation method33Microwave synthesis of NaA zeolite membranes on coarse macroporous α-Al2O3 tubes for desalination38Effect of H2O Activity on Zeolite Formation3In situ energy-dispersive X-ray diffraction of local phase dynamics during solvothermal growth of Cu4O32Hydrothermal interconversion of FAU-type zeolite in the presence of sodium and tetramethylammonium ions11In situ scattering studies of material formation during wet-chemical syntheses1Panoramic (in beam) studies of materials synthesis1Study of the Relationship between Synthesis Descriptors and the Type of Zeolite Phase Formed in ZSM‐43 Synthesis by Using Machine Learning6Comparison of lunar and Martian regolith simulant-based geopolymer cements formed by alkali-activation for in-situ resource utilization80Geopolymeric nanomaterials3Autocatalysis and Oriented Attachment Direct the Synthesis of a Metal–Organic Framework35Solvothermal synthesis of zirconia nanomaterials: Latest developments and future45Parameter optimization, characterization, and crystallization mechanisms underlying the synthesis of zeolite A using liquid crystal display waste glass and sandblasting waste as alternative raw materials19A green process for zeolite synthesis: low-temperature vapor phase treatment of natural bauxites15Simultaneous scavenging of As(V) and safranin O dye by Mg/Al LDH-zeolite heterocoagulated materials: The effect of adsorbent synthesis approach on its efficiency in static and dynamic system17Solvothermal and hydrothermal methods for preparative solid-state chemistry5Process Elucidation and Hazard Analysis of the Metal–Organic Framework Scale-Up Synthesis: A Case Study of ZIF-815Zeolite Synthesis and Steam: Preliminary data Using coal fly ash as raw Material6Mapping the Complete Reaction Energy Landscape of a Metal–Organic Framework Phase Transformation11In situ hydrothermal growth of Zeolite-A membrane on polysulfone hollow fibers5Synthesis of zeolites from volcanic ash (Tajogaite, Spain) for the remediation of waters contaminated by fluoride1The Current Understanding of Mechanistic Pathways in Zeolite Crystallization192Exploiting in situ NMR spectroscopy to understand non-traditional methods for zeolite synthesis7Split Syntheses: Introducing Bottom-Up Control over Aluminum in SSZ-13 and ZSM-5 Zeolites16Mechanical activation of kaolinite for sodalite synthesis under mild conditions7Minute-scale synthesis of hierarchical and nanosized ZSM-5 zeolites with high space-time yields3Understanding the Mechanism of Nontraditional Zeolite Synthesis Using In Situ Nuclear Magnetic Resonance Spectroscopy and X-ray Diffraction2Conversion of Waste Red Mud into LTA Zeolite Adsorbent for Highly Selective Cs+/Sr2+ Removal: Governing Effects of Inorganic Acid Type and Hydrothermal Temperature on Zeolite Phase Evolution0Electrochemical acceleration of bulk-phase LTA zeolite crystallization0A kinetic study of the crystallization of LTA-type zeolite from colloidal solutions by in-situ ultrasonic attenuation measurements0

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  1. An X-ray absorption fine structure study of amorphous precursors of a gallium silicate zeolite

    Journal of Physics and Chemistry of Solids · 2001-08-01

    Richard I. Walton, Dermot M. O'Hare

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  2. Identification of a Key Precursor Phase for Synthesis of SAPO-34 and Kinetics of Formation Investigated by in Situ X-ray Diffraction

    The Journal of Physical Chemistry B · 2001-11-22

    Ørnulv B. Vistad, Duncan E. Akporiaye, Karl Petter Lillerud

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  3. Anomalous wide angle X-ray scattering (AWAXS) and heterogeneous catalysts

    Applied Catalysis A General · 2002-03-28

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  4. In‐Situtime‐resolved X‐ray diffraction: The current state of the art

    Synchrotron Radiation News · 2002-07-01

    Ann E. Terry, G. Vaughan, Åke Kvick, Richard I. Walton, Alexander J. Norquist, Dermot M. O'Hare

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  5. Mechanism of the Transformation of Silica Precursor Solutions into Si-MFI Zeolite

    Angewandte Chemie International Edition · 2002-07-15

    Svetlana Mintova, Norman H. Olson, Jürgen Senker, Thomas Bein

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  6. Following the formation of nanometer-sized clusters by time-resolved SAXS and EXAFS techniques

    Faraday Discussions · 2002-10-08

    Florian Meneau, Gopinathan Sankar, Norberto Morgante, Rudolf Winter, C. Richard A. Catlow, G. Neville Greaves, John Meurig Thomas

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  7. An in situ study of crystallisation gradients during the hydrothermal/autoclave synthesis of zeolites

    Physical Chemistry Chemical Physics · 2003-01-01

    David Hooper, Paul Barnes, Jeremy K. Cockcroft, Andrew C. Jupe, Simon D. M. Jacques, Stephen P. Bailey, Fabio Lupo, Martin J. Vickers, Michael Hanfland

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  8. Nanosized Molecular Sieves

    Collection of Czechoslovak Chemical Communications · 2003-01-01

    Svetlana Mintova

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  9. Modeling Nucleation and Growth in Zeolites

    CRC Press eBooks · 2003-07-31

    C. Richard A. Catlow, David S. Coombes, Dewi W. Lewis, J Carlos G. Pereira, Ben Slater

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  10. In situ waxs-saxs synchrotron study of the kinetics of nucleation and growth in linde type-a zeolite (LTA)

    Studies in surface science and catalysis · 2004-01-01

    R. Grizzetti, Gilberto Artioli, Mauro Gemmi, F. Carsughi, Pietro Riello

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  11. SYNTHESIS AND KINETIC STUDY OF ZEOLITE FROM LOPBURI PERLITE

    Unknown journal · 2004-01-01

    Sudaporn Tangkawanit, Kunwadee Rangsriwatananon

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  12. Observation and Reactivity of the Chainlike Species ([Al(PO4)2]3-)n during the X-ray Diffraction Investigation of the Hydrothermal Synthesis of the Super-sodalite Sodium Aluminophosphate MIL-74 (Na2Al7(PO4)12·4trenH3·Na(H2O)16)

    The Journal of Physical Chemistry B · 2004-11-24

    Thierry Loiseau, L. Beitone, Franck Millange, Françis Taulelle, Dermot M. O'Hare, Gérard Férey

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  13. In situ diagnostics of zeolite crystallization by ultrasonic monitoring

    Microporous and Mesoporous Materials · 2005-01-13

    Ralph Herrmann, Wilhelm Schwieger, O. Scharf, Ch. Stenzel, H. Toufar, M. Schmachtl, B. Ziberi, Wolfgang Grill

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  14. Trivalent Atom Contribution on Solid−Solid Transformation of Ga13 Polycation Intercalated Clay into Sodalite Investigated by X-ray Absorption Spectroscopy

    The Journal of Physical Chemistry B · 2005-04-16

    Sung‐Reol Lee, Man Park, Yang‐Su Han, Sung-Ho Hwang, Jin‐Ho Choy

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  15. Do Geopolymers Actually Contain Nanocrystalline Zeolites? A Reexamination of Existing Results

    Chemistry of Materials · 2005-05-11

    John L. Provis, Grant C. Lukey, Jannie S. J. van Deventer

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  16. Effects of step-change of synthesis temperature on synthesis of zeolite 4A from coal fly ash

    Microporous and Mesoporous Materials · 2005-11-03

    Kwan San Hui, Christopher Y.H. Chao

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  17. On the mechanism of zeolite growing: Crystallization by seeding with delayered zeolites

    Microporous and Mesoporous Materials · 2005-11-17

    Urbano Díaz, Vicente Fornés, Avelino Corma

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  18. In-situ XRD as a tool to understanding zeolite crystallization

    Current Opinion in Colloid & Interface Science · 2006-01-28

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  19. Enhanced Resonator Sensitivity with Nanostructured Porous Silica Coatings

    Langmuir · 2006-06-17

    Shilpa H. Bhansali, J. M. Jarvis, I. A. Aksay, Jeffrey D. Carbeck

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  20. Direct measurement of the kinetics of geopolymerisation by in-situ energy dispersive X-ray diffractometry

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  21. In situ studies of the crystallisation of microporous materials using synchrotron radiation based X-ray techniques

    Studies in surface science and catalysis · 2007-01-01

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  22. In-situ ultrasonic methods for monitoring the hydrothermal synthesis of LTA-type zeolite from colloidal solutions

    Studies in surface science and catalysis · 2007-01-01

    Hasan Baser, T. Selvam, Jimmy Ofili, Ralph Herrmann, Wilhelm Schwieger

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  23. In Situ SAXS/WAXS of Zeolite Microwave Synthesis: NaY, NaA, and Beta Zeolites

    ChemPhysChem · 2007-01-25

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  24. Monitoring of crystallization processes during synthesis of zeolite A by in situ 27Al NMR spectroscopy

    Materials Chemistry and Physics · 2007-03-27

    Zoran P. Miladinović, Joanna Zakrzewska, Branimir Kovacevic, Goran Bačić

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  25. Structure Determination: Experimental Techniques

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  26. Effect of Organic Templates on the Kinetics and Crystallization of Microporous Metal-Substituted Aluminophosphates

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  27. Structural Effects of Solvents on the Breathing of Metal–Organic Frameworks: An In Situ Diffraction Study

    Angewandte Chemie International Edition · 2008-04-18

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  28. Structural Effects of Solvents on the Breathing of Metal–Organic Frameworks: An In Situ Diffraction Study

    Angewandte Chemie · 2008-04-18

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  29. Synthesis of Nanometer-Sized Sodalite Without Adding Organic Additives

    Langmuir · 2008-05-29

    Wei Fan, Kazumasa Morozumi, Riichiro Kimura, Toshiyuki Yokoi, Tatsuya Okubo

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  30. Viscosity sensing in heated alkaline zeolite synthesis media

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  31. Kinetic analysis of experimental intensity curves obtained during zeolite a synthesis using in situ 27Al NMR spectroscopy

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  32. Time and position resolved in situ X-ray diffraction study of the hydrothermal conversion of gypsum monoliths to hydroxyapatite

    Dalton Transactions · 2009-01-01

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  33. Role of Germanium on the Nucleation and Growth of Zeolite A from Clear Solutions As Studied by in Situ Small-Angle X-ray Scattering, Wide-Angle X-ray Scattering, and Dynamic Light Scattering

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  34. The polymorphs and solvates of phenylbutazone and their phase transition behaviour

    UCL Discovery (University College London) · 2009-11-01

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  35. Early Stage Reversed Crystal Growth of Zeolite A and Its Phase Transformation to Sodalite

    Journal of the American Chemical Society · 2009-11-17

    Heather F. Greer, Paul S. Wheatley, Sharon Elizabeth Ashbrook, Russell E. Morris, Wuzong Zhou

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  36. In Situ XAS and XRPD Parametric Rietveld Refinement To Understand Dealumination of Y Zeolite Catalyst

    Journal of the American Chemical Society · 2009-12-15

    Giovanni Agostini, Carlo Lamberti, Luca Palin, Marco Milanesio, Nadiya Danilina, Bin Xu, M. Janousch, Jeroen A. van Bokhoven

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  37. Time‐Resolved In Situ Diffraction Study of the Solvothermal Crystallization of Some Prototypical Metal–Organic Frameworks

    Angewandte Chemie International Edition · 2009-12-16

    Franck Millange, Manuela E. Medina, Nathalie Guillou, Gérard Férey, Kathryn M. Golden, Richard I. Walton

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  38. Time‐Resolved In Situ Diffraction Study of the Solvothermal Crystallization of Some Prototypical Metal–Organic Frameworks

    Angewandte Chemie · 2009-12-16

    Franck Millange, Manuela E. Medina, Nathalie Guillou, Gérard Férey, Kathryn M. Golden, Richard I. Walton

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  39. Methods for in situ spectroscopic probing of the synthesis of a zeolite

    Chemical Society Reviews · 2010-01-01

    Alexander Aerts, Christine E. A. Kirschhock, Johan A. Martens

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  40. The role of synchrotron radiation in examining the self-assembly of crystalline nanoporous framework materials: from zeolites and aluminophosphates to metal organic hybrids

    Chemical Society Reviews · 2010-01-01

    Matthew G. O’Brien, Andrew Michael Beale, Bert Marc Weckhuysen

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  41. Effect of curing temperature on the development of hard structure of metakaolin-based geopolymer

    Construction and Building Materials · 2010-01-16

    Pavel Rovnanı́k

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  42. Genesis of bismuth molybdenum oxide catalyst followed by in-situ techniques and its use in catalytic dense membrane reactor

    Unknown journal · 2010-05-07

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  43. Time-resolved in situ studies of apatite formation in aqueous solutions

    American Mineralogist · 2010-08-01

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  44. A time-resolved diffraction study of a window of stability in the synthesis of a copper carboxylate metal–organic framework

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  45. Oberflächenchemie Metall‐organischer Gerüste an der Flüssig‐fest‐Grenzfläche

    Angewandte Chemie · 2010-12-28

    Denise Zacher, Rochus Schmid, Christof Wöll, Roland A. Fischer

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  46. Surface Chemistry of Metal–Organic Frameworks at the Liquid–Solid Interface

    Angewandte Chemie International Edition · 2010-12-28

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  47. Role of ethanol in sodalite crystallization in an ethanol–Na2O–Al2O3–SiO2–H2O system

    CrystEngComm · 2011-01-01

    Yi Huang, Jianfeng Yao, Xueyi Zhang, Chunhua Kong, Huiyong Chen, Dongxia Liu, Michael Tsapatsis B, Matthew R. Hill, Anita J. Hill, Huanting Wang

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  48. The application of statistical methodology to the analysis of time-resolved X-ray diffraction data

    Analytical Methods · 2011-01-01

    J. Burley, Dermot M. O'Hare, Gareth R. Williams

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  49. Zeolites X and A crystallization compared by simultaneous UV/VIS-Raman and X-ray diffraction

    Physical Chemistry Chemical Physics · 2011-01-01

    Anouschka Depla, Elke Verheyen, An Veyfeyken, Elena Gobechiya, Thomas Hartmann, Reinhold Schaefer, Johan A. Martens, Christine E. A. Kirschhock

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  50. In‐Situ Monitoring of the Formation of Crystalline Solids

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