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RESEARCH PAPER · Nature · 2026

Vacuum ultraviolet second-harmonic generation in NH4B4O6F crystal

F F Zhang, Zilong Chen, Chen Cui, Zhihua Yang, Miriding Mutailipu, Fuming M. Li, Xueling Hou, Xifa Long, Shilie Pan

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Vacuum ultraviolet second-harmonic generation in NH4B4O6F crystalOriginal[Al(H 2 O) 6 ](NO 3 )Cl 2 : achieving parallel arrangement of functional units and birefringence enhancement through free halogen-mediated structural regulation0[Rb 4 Cl][Cd 11 In 9 Se 26 ]: a salt inclusion chalcogenide with a diamond-like framework for infrared nonlinear optics0A 2 Sb 2 SO 4 F 6 (A = NH 4 + , Na + ): two sulfate fluoride crystals exhibiting enhanced birefringence driven by stereochemically active antimony( iii )1A mercury-based selenite with wide bandgap and moderate birefringence via cation substitution and partial fluorination1Achieving an optimal performance balance in UV nonlinear optical crystals via hydrogen-bond regulation1Charge-order-induced directional enhancement of non-diagonal second-order nonlinear optical tensor components2Chiral calcium thiocyanate hybrids: amino acid-enabled structural diversity and second-harmonic generation0Design of borate-squarate hybrid crystals with large birefringence by synergistic assembly of planar π-conjugated groups0KGdSiSe 4 and KGdGeSe 4 : two rare earth-based selenides with wide bandgaps and large nonlinear optical responses0KGdSiSe4 and KGdGeSe4: Two Rare Earth Metal-Based Selenides with Wide Bandgaps and Large Nonlinear Optical Responses0Layered perovskite-like nitrates A 2 Ca(NO 3 ) 2 Cl 2 (A = Rb, Cs) as ultraviolet birefringent optical materials3Second-harmonic generation responses in low-dimensional metal bromides functionalized with l -arginine1Series of phosphate nonlinear optical materials containing active metal ions with short cut-off edges0Solving the long-standing hygroscopicity and thermal stability issues of the nonlinear optical crystal α-LiIO 3 via homogeneous cation exchange0Structural engineering of α-BaEuBO 3 F 2 borate oxyfluoride: circumventing concentration quenching for a highly efficient and thermally stable red phosphor0Supramolecular template modulation in chiral lead bromide hybrids toward enhanced second-harmonic generation0Synergistic dual-modification strategy of π-conjugated cations and tetrahedra: rational design of ultraviolet high-birefringence monofluorophosphates0Synthesis and characterization of mixed carbonate and bicarbonate materials as candidates for deep-UV applications1The condensation of π-conjugated units: a new paradigm for designing high-performance optical crystals4Zn 0.7 Hg 0.3 Ga 2 Se 4 : a defect diamond-like selenide with a balanced band gap and nonlinear optical response0Functional Unit Design of Deep‐UV NLO Crystals With Short Phase‐Matching and Large SHG Response22Coordination Geometry-Directed Optical Anisotropy and Phase-Matched Nonlinear Optics in Chiral Metal–Organic Frameworks2High average power single-frequency nanosecond laser tunable from 766 nm to 775 nm and 1535 nm to 1570 nm based on a seeded optical parametric generator1Vacuum Ultraviolet Generation in Improved Nonlinear Photonic Crystal Structure of α-Strontium Tetraborate0An Ultraviolet Transparent Nonlinear Optical Crystal Assembled from a Polarizable Tetrahedral Unit1CdY 2 Si 2 S 8 : A Wide Bandgap IR NLO Material with d 10 Metal-Induced Structure Transformation from CS to NCS1NH 4 B 3 PO 6 (OH) 3 : A Hydroxyborophosphate with Short DUV Cutoff Edge and Large Birefringence2High-repetition nanosecond vacuum ultraviolet laser at 177.3 nm generated in a period-disorder SiO 2 crystal0Cs4Ag9I12Cl: A congruent-melting semiconductor crystal with a photoluminescence fast decay component of 3.3 ns by halogen regulation0Chirality-driven polar lattice engineering for high-performance organic nonlinear optical crystals3Local Conformational Confinement and Dipole Engineering for Phase-Matchable Solar-Blind Ultraviolet Nonlinear Optical Crystals11Minimizing Oscillator Strength: A Strategy for Engineering Deep-Ultraviolet Nonlinear Optical Crystals with Optimized Refractive-Index Dispersion0Recent Progress in Hg-Based Oxysalt Crystals for Nonlinear Optics and Birefringence Applications5K 3 Mg 2 [K 6 MgCl 3 ][Ga 20 S 36 ]: A Diamond-like Framework Based on Mixed-Type Supertetrahedra for Excellent Nonlinear Optical Property1F−/OH− terminal modification of [B3O6] clusters: Constructing deep-ultraviolet hydroxyfluorooxoborates with tunable optical performance0Fluorination modulation theory for vacuum-ultraviolet nonlinear optical crystals (I): foundation and framework9Topological structural chemistry of fluorooxoborates: From fundamental building blocks to macroscopic optical performance regulation0Assembly of Functional Units for Constructing an Ultraviolet-Transparent Nonlinear Optical Mixed Alkaline Metal Borate-Formate1LiMn(IO 3 ) 3 : A Noncentrosymmetric Iodate Synthesized by Polyhedral Volume Ratio Modulation0Deep-Ultraviolet Nonlinear-Optical Crystals K1– x A x Be2BO3F2 (A = NH4, OH3) Realized by A-Site Cationic Solid Solution0Regulating B‐O Arrangement Boosts Anisotropy in a Simple Rubidium Borate, Leading to a High‐Performance UV NLO Crystal0Breaking Layered Limitations via Electrostatic-to-Covalent Conversion toward Three-Dimensional T2-Cluster-Based Chalcogenides7Rb 2 ZnGe 3 Se 8 : A Large-Birefringence Layered Chalcogenide Enabled by Anisotropic Electrons in Tetrahedral Units0A Strategy for Enhancing the Optical Anisotropy of Phosphates via Tetrahedral Unit Modification0Deep-Ultraviolet Transparent Zr/Hf Fluorides with Second-Harmonic Generation Effects Induced by Alkali-Metal Modulation2A 3 Zr 2 (PS 4 )(P 2 S 7 ) 2 (A = K, Rb, Cs) Synthesized by the Metal Oxide-Boron-Chalcogen Routine: A Series of Zirconium-Based Thiophosphate Nonlinear Optical Crystals Featuring PS 4 Tetrahedron and P 2 S 7 Dimer0K 3 Yb 2 (BO 3 ) 3 and Rb 3 Yb 2 (BO 3 ) 3 : Two Rare-Earth Borate Ultraviolet Nonlinear Optical Crystals1Design of deep-ultraviolet nonlinear optical BePNO2 guided by non-π-conjugated NLO-active unit0Toward the vacuum-ultraviolet frontier in nonlinear optical frequency conversion: phase-matching mechanisms across dimensions and architectures2Parallel arrangement of functional building blocks: toward performance synergy in oxalate borate ultraviolet nonlinear optical crystals0Ce(2,2′-bipyridyl)3(SCN)3: Lanthanide Coordination- and Hydrogen-Bond-Directed Binary π-Conjugated Assemblies with Synergistic Large Birefringence and Broad Transparency0A new phase and transformation mechanism in BaGa4Se7 infrared nonlinear optical crystal0Growth of High-Quality CLBO Crystals for High-Power 266 nm DUV Laser0Symmetry Breaking Induced by Hydration-Number Tuning Enables Second-Order Nonlinear Optical Responses in Lanthanum Sulfate Hydrates0Heavy‐Halide Coordination and Lattice‐Confined Molecular Alignment Enable Giant Birefringence in Hybrid Metal Halides0MZnCO3OH: A family of hydroxycarbonate nonlinear optical crystals in the UV and DUV regions0Eu5ZnGa6S15, Eu5Zn3Ga2Sn2S15, and Pb5HgGa6S15: Crystal Chemistry and Nonlinear Optical Properties0Accelerating the Discovery of Deep-Ultraviolet Nonlinear Optical Materials by Combining Machine Learning Interatomic Potentials with First-Principles Calculations: A Case of LiB2O3F0Multidimensional Cation Modulation toward Phase-Matchable Nonlinear Optical Fluorides with Short UV Cutoff Edges0[CN4H8]SiF6: Fluorination-guided design of deep-UV crystal with large birefringence0K3Sr3Li2Ga4B6O20F: A Sr2Be2B2O7-Type Ultraviolet Nonlinear Optical Crystal0Cation-regulated orientational coherence in one-dimensional antimony fluoride selenate chains modulates ultraviolet second-Harmonic generation0AlGaS3: a wide band gap ternary diamond-like infrared nonlinear optical material with high laser-induced damage threshold1Unlocking Hidden Potential via Reprogrammed Mineral Structures: How Anionic Transformation Achieves Ultraviolet Nonlinear Optical Performance0An Excellent Deep‐Ultraviolet Nonlinear Optical Crystal Realized via a Functional Group Based on a Two‐in‐One Strategy0Assembly of dual π-conjugated units toward enhanced birefringence in a 2D organic sulfonate crystal0NaGa2PS6: A Noncentrosymmetric Thiophosphate with Wide Band Gap and High Laser-Induced Damage Threshold0Fluorooxoborate crystal NH4B4O6F: a high-performance candidate for practical vacuum ultraviolet nonlinear optics0Borophosphate-based second-order nonlinear optical materials: Advances in structural diversity and optical performance0Beyond the bandgap bottleneck: structure–property design principles for infrared nonlinear optical phosphides0High‐Performance Large‐Format AlN‐Based Vacuum Ultraviolet Imaging Detector0Growth and morphologies of SrB4O7 crystals0Cation‐Regulated [CH 3 BO 2 F]‐Derived Borates: Synergistic Fluorination and Organic Functionalization for High‐Birefringence UV NLO Materials0

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  2. [Rb 4 Cl][Cd 11 In 9 Se 26 ]: a salt inclusion chalcogenide with a diamond-like framework for infrared nonlinear optics

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  3. A 2 Sb 2 SO 4 F 6 (A = NH 4 + , Na + ): two sulfate fluoride crystals exhibiting enhanced birefringence driven by stereochemically active antimony( iii )

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  4. A mercury-based selenite with wide bandgap and moderate birefringence via cation substitution and partial fluorination

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  8. Design of borate-squarate hybrid crystals with large birefringence by synergistic assembly of planar π-conjugated groups

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  9. KGdSiSe 4 and KGdGeSe 4 : two rare earth-based selenides with wide bandgaps and large nonlinear optical responses

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  16. Supramolecular template modulation in chiral lead bromide hybrids toward enhanced second-harmonic generation

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  17. Synergistic dual-modification strategy of π-conjugated cations and tetrahedra: rational design of ultraviolet high-birefringence monofluorophosphates

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  18. Synthesis and characterization of mixed carbonate and bicarbonate materials as candidates for deep-UV applications

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  19. The condensation of π-conjugated units: a new paradigm for designing high-performance optical crystals

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  21. Functional Unit Design of Deep‐UV NLO Crystals With Short Phase‐Matching and Large SHG Response

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  46. A 3 Zr 2 (PS 4 )(P 2 S 7 ) 2 (A = K, Rb, Cs) Synthesized by the Metal Oxide-Boron-Chalcogen Routine: A Series of Zirconium-Based Thiophosphate Nonlinear Optical Crystals Featuring PS 4 Tetrahedron and P 2 S 7 Dimer

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  50. Parallel arrangement of functional building blocks: toward performance synergy in oxalate borate ultraviolet nonlinear optical crystals

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