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RESEARCH PAPER · ACS Nano · 2025

33 Unresolved Questions in Nanoscience and Nanotechnology

Chad Alexander Mirkin, Sarah Hurst Petrosko, Natalie Artzi, Koray Aydın, Austin Biaggne, C. Jeffrey Brinker, Katherine E. Bujold, Y. Charles Cao, Rachel R. Chan, Chaojian Chen, Pengcheng Chen, Xiaodong Chen, Olivier J. G. L. Chevalier, Chung Hang Jonathan Choi, Richard M. Crooks, Vinayak P. Dravid, Jingshan S. Du, Sasha B. Ebrahimi, Hongyou Fan, Omar K. Farha, C. Adrian Figg, Tanner D. Fink, Connor M. Forsyth, Harald Fuchs, Franz M. Geiger, Nathan C. Gianneschi, Kyle J. Gibson, David S. Ginger, Sishi Guo, Justin S. Hanes, Liangliang Hao, Jin Shan Huang, Bryan Michael Hunter, Fengwei Huo, Jeongmin Hwang, Rongchao M. Jin, Shana O. Kelley, Thomas J. Kempa, Youngeun Kim, Sergej Kudruk, Sneha Kumari, Kaitlin M. Landy, Ki‐Bum Lee, Noel J. Leon, Jun Li, Yuanwei Li, Zhiwei Li, Bin Liu, Guoliang Liu, Xiaogang Liu, Luis M. Liz‐Marzán, Jochen H. Lorch, Taokun Luo, Robert J. Macfarlane, Jill E. Millstone, Milan Mrksich, Catherine Jones Murphy, Rajesh R. Naik, André E. Nel, Christopher Oetheimer, Jenny Orbeck, So‐Jung Park, Benjamin E. Partridge, Nicholas A. Peppas, Michelle L. Personick, Arindam Raj, Namrata Ramani, Michael B. Ross, Susan E. Ross, Edward Hartley Sargent, Tanushri Sengupta, George Chappell Schatz, Dwight S. Seferos, Tamar Seideman, Soyoung E. Seo, Bo Shen, Wooyoung Shim, Donghoon Shin, Ulrich Simon, Andrew J. Sinegra, Peter T. Smith, Alexander M. Spokoyny, Peter J. Stang, Alexander H. Stegh, James Fraser Stoddart, Dayne F. Swearer, Weihong Tan, Michelle H. Teplensky, Colby Shad Thaxton, David R. Walt, Mary X. Wang, Zhe Wang, Wei David Wei, Paul S. Weiss, Peter H. Winegar, Younan Xia, Yi Xie, Xiaoyang Xu, Peidong Yang, Yiming Yang

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33 Unresolved Questions in Nanoscience and NanotechnologyOriginalCleavable Hydrophobic Anchors Optimize Immunomodulatory Effects of Oligonucleotides4Enhancing the sensitivity of radiotherapy in non-small cell lung cancer through nanotechnology-mediated reactive oxygen species generation2Positive definiteness of deformation energy as a consistency condition of discrete-to-continuum transition6Engaging the Community to Navigate the Nanoscience Horizon2Review on electrochemical sensors for anticancer drug susceptibility testing3Engineering MOFs for thin-film and nanofilm nanocomposite membranes for CO 2 separation6Divergent Transformation Pathways from a Common Au 25 Intermediate: The Effect of “Positional Isomerism”2Machine learning for nanoparticle-based imaging: From rational design to precision diagnosis4Exploratory feature analysis of baseline ionic currents in MoS 2 nanopores0Modulating oxygen vacancies of ZnMn 2 O 4 nanosheets for high-rate aqueous zinc-ion batteries1Factorised electron-nuclear dynamics with effective complex potential: on-the-fly implementation for H 2 + in a laser field0Dual-Functional Magnesium-Doped Zeolitic Imidazolate Framework-8 Nanoparticles for Rice Blast Control and Restoration of Magnesium-Deficient Photosynthesis12Carbon-Based Functional Nanomaterials: Preparation, Properties and Applications2Detailed impurity profiling of graphene oxide fractions by robust inductively coupled plasma optical emission spectrometry monitoring7Bioinspired Interfacial Hitchhiking: 3D Hierarchical Nanopesticide Aggregates via Heterointerface-Confined Coassembly for Spatiotemporal Foliar Deposition and Translocation In Vivo7Backbone Stiffness‐Dependent Photoluminescence of Pendant Fluorophores in Organic Nanoparticles1Dispersion Technique May Change Structure and Bio-Oxidative Activity of Magnetic MOF Nanoparticles0Ultrasensitive Enzyme-Free Detection of Proteins on Magnetic Beads8A Nano Focus on Interdisciplinary Education: Visualizing Ligand and Biomolecule Volume on Nanoparticle Surfaces0Strong-Field Steering of Photoelectron Emission Dynamics in Diverse Nanospheres0Surface-dictated sorting in colloidal mixtures0Erasure by friction: derivation of the coefficient of friction in two-dimensional van der Waals superlubrication critical conditions1Towards a unified mechanistic understanding of the electrical response of bipolar membrane systems0Phase Engineering of Atomically Precise Nanoclusters (APNCs) of Gold and Beyond1Revealing the Interfacial Evolution of Cr/Bi2Se3 Driven by Cation Enrichment0Nano‐enzyme engineering: Advancing enzyme immobilization for industrial and environmental applications0Programmable Stepwise Heteroepitaxial Growth of Colloidal Crystals With Different Phases1Evaporation-Induced Phase Transitions in Free-Standing Plasmonic Nanoparticle Assemblies0Scalable affinity-driven nanofilm nanocomposite membranes for CO2/N2 separation0Metal–Phenolic Coatings Enable Universal Design of Spherical Nucleic Acids0Metal–Phenolic Coatings Enable Universal Design of Spherical Nucleic Acids0Connecting and Engaging1Unraveling Bone‐Skin Crosstalk Enables miRNA Nanoformulation for Cutaneous Neurovascular Reconstruction in Diabetic Mice0Starch-integrated cathode with linear sulfur and activated iodine catalyst: Synergistically boosting kinetics of aqueous zinc-sulfur batteries1An Electronically Coupled Interfacial Energy Descriptor for Predicting Coulombic Efficiency in Aqueous Zinc Batteries1A Conversation with Prof. Paul S. Weiss, Founding Editor-in-Chief of ACS Nano and Nanoscience Pioneer0Intelligent theranostic nanoplatforms in next-generation precision oncology1The Fierce Morphological Battle of Silver Nanoparticles: How Irregularities, Vacancies and Defects Tip the Crossing Sizes0Mechanistic Insights into Magnesium Pyrophosphate Formation in the Presence of Gold Nanoclusters Enable Genetic Analysis via Co-Aggregation-Induced Fluorescence Enhancement0Challenges and Design Strategies Toward Aqueous Zinc‐Ion Batteries Beyond Laboratory0Synthesis of Metal–Quantum Dot Core–Satellite Nanoparticles and Plasmonic Cavity-Induced Recovery of Quantum Yield for High External Quantum Efficiency0Reticular framework architectures for coagulation-flocculation and colloidal separation: Mechanistic insights, structure-performance correlation, and AI-guided discovery0Bridging Catalytic Worlds: A Coassembly Platform for Unified Chemoenzymatic Cascades0Polymers on Metal Nanoparticles: Emerging Chemistry, Self-Assembly, and Their Biomedical Applications0Fluorinated Self‐Assembled Monolayers for Highly Reversible Anode‐Free Zinc Batteries0Fluorinated Self‐Assembled Monolayers for Highly Reversible Anode‐Free Zinc Batteries0FastNano Liquid: An Automated Platform for Small‐Angle X‐ray Scattering‐Based Materials Discovery0Engineering Metal Nanomaterials for Precision Genetic Medicine0Sustainable functional nanomaterials for environmental, cultural heritage, and biomedical applications: Advances in chemical technologies0Omnidirectional bending sensor with three-fold structural symmetry enables decoupling of bending angle and direction0Extreme‐Fast‐Charging Li‐Ion Batteries via Activation‐Energy Regulation With a Li 3 PO 4 ‐Li 2 SO 4 ‐Rich Solid Electrolyte Interphase0Artificial Intelligence‐Driven Inverse Design of Singlet Fission Candidates in the Acene family1Ni-induced reconfiguration of the bonding network enables high-rate and stable MnFe Prussian blue analogue for sodium-ion batteries0A Wurster-type branched polymer design breaks the voltage-capacity trade-off in p-type organic cathodes0Conductometric process analytical technology for real-time endpoint control of graphene oxide dialysis purification1Edge-Dependent Capacitive Response and Geometry-Tunable Metallization Field in Same-Lattice Graphene/Graphane/Graphene Nanoribbon Nanocapacitors0Plasmon Decay Pathways in Magic-Sized Nanoclusters: Hot-Carrier Dynamics for Photocatalyst Design0Solvent-Dipole Deshielding of Hydrated Aluminum Lewis Acids for Enhanced 5-Hydroxymethylfurfural Production from Biomass0

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  2. Enhancing the sensitivity of radiotherapy in non-small cell lung cancer through nanotechnology-mediated reactive oxygen species generation

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  3. Positive definiteness of deformation energy as a consistency condition of discrete-to-continuum transition

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  4. Engaging the Community to Navigate the Nanoscience Horizon

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  5. Review on electrochemical sensors for anticancer drug susceptibility testing

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  6. Engineering MOFs for thin-film and nanofilm nanocomposite membranes for CO 2 separation

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  7. Divergent Transformation Pathways from a Common Au 25 Intermediate: The Effect of “Positional Isomerism”

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  8. Machine learning for nanoparticle-based imaging: From rational design to precision diagnosis

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  9. Exploratory feature analysis of baseline ionic currents in MoS 2 nanopores

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  10. Modulating oxygen vacancies of ZnMn 2 O 4 nanosheets for high-rate aqueous zinc-ion batteries

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  11. Factorised electron-nuclear dynamics with effective complex potential: on-the-fly implementation for H 2 + in a laser field

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  12. Dual-Functional Magnesium-Doped Zeolitic Imidazolate Framework-8 Nanoparticles for Rice Blast Control and Restoration of Magnesium-Deficient Photosynthesis

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  13. Carbon-Based Functional Nanomaterials: Preparation, Properties and Applications

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  14. Detailed impurity profiling of graphene oxide fractions by robust inductively coupled plasma optical emission spectrometry monitoring

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  15. Bioinspired Interfacial Hitchhiking: 3D Hierarchical Nanopesticide Aggregates via Heterointerface-Confined Coassembly for Spatiotemporal Foliar Deposition and Translocation In Vivo

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  16. Backbone Stiffness‐Dependent Photoluminescence of Pendant Fluorophores in Organic Nanoparticles

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  17. Dispersion Technique May Change Structure and Bio-Oxidative Activity of Magnetic MOF Nanoparticles

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  18. Ultrasensitive Enzyme-Free Detection of Proteins on Magnetic Beads

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  19. A Nano Focus on Interdisciplinary Education: Visualizing Ligand and Biomolecule Volume on Nanoparticle Surfaces

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  20. Strong-Field Steering of Photoelectron Emission Dynamics in Diverse Nanospheres

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  23. Towards a unified mechanistic understanding of the electrical response of bipolar membrane systems

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  25. Revealing the Interfacial Evolution of Cr/Bi2Se3 Driven by Cation Enrichment

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  35. An Electronically Coupled Interfacial Energy Descriptor for Predicting Coulombic Efficiency in Aqueous Zinc Batteries

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  36. A Conversation with Prof. Paul S. Weiss, Founding Editor-in-Chief of ACS Nano and Nanoscience Pioneer

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  45. Fluorinated Self‐Assembled Monolayers for Highly Reversible Anode‐Free Zinc Batteries

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  47. FastNano Liquid: An Automated Platform for Small‐Angle X‐ray Scattering‐Based Materials Discovery

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  49. Sustainable functional nanomaterials for environmental, cultural heritage, and biomedical applications: Advances in chemical technologies

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  50. Omnidirectional bending sensor with three-fold structural symmetry enables decoupling of bending angle and direction

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