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RESEARCH PAPER · EES Catalysis · 2025

The dark side of metal exsolution: a combined in situ surface spectroscopic and electrochemical study on perovskite-type cathodes for high-temperature CO 2 electrolysis

Christian Melcher, Andreas Nenning, Florian Schrenk, Kirsten Rath, Christoph Rameshan, Alexander Karl Opitz

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The dark side of metal exsolution: a combined in situ surface spectroscopic and electrochemical study on perovskite-type cathodes for high-temperature CO 2 electrolysisOriginalUHV-based analytics with electrochemical oxygen activity control3Activation of bifunctional perovskite oxides through exsolution in symmetrical solid oxide cells: Recent advances, challenges, and outlook4Reversible rhenium exsolution in SrFe1-xRexO3-δ for redox-stable symmetrical oxide fuel cells2Composition-Tuned Ni Exsolution from Ruddlesden-Popper Oxides for Durable CO2 Dry Reforming of Methane0Visualising redox-driven metal–oxide interface dynamics in Ni/GDC electrodes via in situ Auger–Meitner electron microscopy0In Situ Characterization of Strontium Titanium Ferrite Perovskites for Application as Electrodes of Solid Oxide Cells1Theoretical insights into the LSCM-based fuel electrodes for efficient CO2 electrolysis in SOEC0Fermi-Level Compression in Zn-Cu Alloys through ZnO/CuO Ratio Control for Selective CO 2 Reduction0Phase-tunable exsolution approaches to energy-functional nanostructured metal-based hybrid materials: synthesis, application, and perspective3Interfacial design principles in mixed-dimensional perovskite heterostructures: Bridging nanostructure chemistry and device functionality0Chemical layering during CO/H2 reduction of iron oxides revealed by APXPS and multiscale characterization0High-Temperature CO2 Reduction: Operando Analysis and Reaction Dynamics0Perovskites for CO 2 Conversion: Active‐Phase Identity, Reconstruction, and the Evidence Behind Mechanistic Claims0

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  1. UHV-based analytics with electrochemical oxygen activity control

    Journal of Materials Chemistry A · 2025-01-01

    Andreas Nenning, Stanislaus Breitwieser, Christian Melcher, Jürgen Fleig

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  2. Activation of bifunctional perovskite oxides through exsolution in symmetrical solid oxide cells: Recent advances, challenges, and outlook

    Matter · 2025-10-01

    Roelf Maring, Vasileios Kyriakou

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  3. Reversible rhenium exsolution in SrFe1-xRexO3-δ for redox-stable symmetrical oxide fuel cells

    Chemical Engineering Journal · 2025-12-26

    Abraham Sánchez-Caballero, Javier Zamudio‐García, Miguel A. García-Plaza, Lucía dos Santos‐Gómez, Jesús Canales‐Vázquez, Jose Manuel Porras-Vázquez, Marrero‐Lopez David

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  4. Composition-Tuned Ni Exsolution from Ruddlesden-Popper Oxides for Durable CO2 Dry Reforming of Methane

    SSRN Electronic Journal · 2026-01-01

    Mona Bahout, Haoran Yu, Vincent Dorcet, Elodie Quenard, Jules Galipaud, Ilan Brouard, Thomas C. Hansen, Haiqian Wang

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  5. Visualising redox-driven metal–oxide interface dynamics in Ni/GDC electrodes via in situ Auger–Meitner electron microscopy

    Journal of Materials Chemistry A · 2026-01-01

    Christian Melcher, Andreas Nenning, Stanislaus Breitwieser, Kirsten Rath, Luca Balice, Jonathan Rollenitz, Martin Bram, Christoph Rameshan, Alexander Karl Opitz

    Read original paper ↗ ·

  6. In Situ Characterization of Strontium Titanium Ferrite Perovskites for Application as Electrodes of Solid Oxide Cells

    ACS Applied Energy Materials · 2026-01-23

    Maria Carmenza Dìaz Lacharme, Martina Marasi, Virginia Pérez Dieste, Belèn Ballesteros, Alessandro Donazzi

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  7. Theoretical insights into the LSCM-based fuel electrodes for efficient CO2 electrolysis in SOEC

    Journal of environmental chemical engineering · 2026-04-19

    Aamir Ullah Shah, Azeem Mustafa, Shiru Le, Zhijiang Wang, Yong Shuai, Kazindutsi Jean Damascene

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  8. Fermi-Level Compression in Zn-Cu Alloys through ZnO/CuO Ratio Control for Selective CO 2 Reduction

    Journal of The Electrochemical Society · 2026-04-23

    Haibing Shu, Yu Sun, Guangcai Zhao, Guopu Cai, Muhammad Arif Khan, Zhonghong Xia, Daixin Ye, Hongbin Zhao

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  9. Phase-tunable exsolution approaches to energy-functional nanostructured metal-based hybrid materials: synthesis, application, and perspective

    EnergyChem · 2026-05-22

    Taehoon Kim, Yeon Hu Park, Jinyoung Lee, Ajayan Vinu, Seong‐Ju Hwang

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  10. Interfacial design principles in mixed-dimensional perovskite heterostructures: Bridging nanostructure chemistry and device functionality

    Progress in Quantum Electronics · 2026-06-18

    Dohun Baek, Doyun Kim, Dongwook Lee, Yejin Whang, Suyeong Jo, Chaewon Lee, Yeongju Chun, Min Kim

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  11. Chemical layering during CO/H2 reduction of iron oxides revealed by APXPS and multiscale characterization

    Scripta Materialia · 2026-08-08

    Yuzhao Wang, Manoj Kumar Ghosalya, Saeid Khesali Azadi, Ahmadreza Mohammadian Soodmand, Rafael Fillus Chuproski, Esko Kokkonen, Alexander Yu. Klyushin, Aidin Heidari, Marko Huttula, Timo Matti Juhani Fabritius, Samuli Urpelainen

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  12. High-Temperature CO2 Reduction: Operando Analysis and Reaction Dynamics

    ACS Catalysis · 2026-08-17

    Aamir Ejaz, Waleed Yaseen, Yanqiang Xu, Rentang Pan, Jiahui Lu, Tonglin Liu, Youkun Tao, Jing Shao

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  13. Perovskites for CO 2 Conversion: Active‐Phase Identity, Reconstruction, and the Evidence Behind Mechanistic Claims

    The Chemical Record · 2026-09-09

    Darpan Vijaykumar Bhuse, Ankush G. Thate, Shubham Deshmukh, Suresh Selvaraj, Ganesh L. Agawane, Chandan Patel, Suraj Jadhav

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