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RESEARCH PAPER · Journal of the American Chemical Society · 2024

Experimental Evidence for Zerovalent Pd(NHC) as a Competent Catalyst in C–N Cross-Coupling (NHC = DiMeIHeptCl)

Volodymyr Semeniuchenko, Sepideh Sharif, Neha Rana, Nalin Chandrasoma, Wilfried M. Braje, R. Tom Baker, Jeffrey M. Manthorpe, William J. Pietro, Michael G. Organ

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Experimental Evidence for Zerovalent Pd(NHC) as a Competent Catalyst in C–N Cross-Coupling (NHC = DiMeIHeptCl)OriginalEnhancing activity and selectivity of palladium catalysts in ketone α-arylation by tailoring the imine chelate of pyridinium amidate (PYA) ligands7Ligand Substitution, Catalyst Activation, and Oxidative Addition Studies of a Stable Dialkyl Palladium Precatalyst8C2-Selective Palladium-Catalyzed C–S Cross-Coupling of 2,4-Dihalopyrimidines10On-Demand Access to Palladium Oxidative Addition Complexes (OACs) from a Stable Organopalladate Salt10Metal–N-Heterocyclic Carbene Complexes in Buchwald–Hartwig Amination Reactions61NHC/Phosphite Nickel(II) Precatalysts for the C–N Cross-Coupling of (Hetero)Aryl Chlorides under Mild Conditions5Initiation of Palladium Precatalysts: Efficiency and Product Selectivity as a Function of Ligand, Substrate, and Reaction Conditions4Imidazolium-based covalent organic cages: from construction to functions3Unexpected Deactivation of PdCl(cinnamyl)(NHC Cl ) Precatalysts Mediated by Alkylamines3Mapping the Relationship of the Dynamic Active Site and the Activation Barrier for Cross-Coupling Reactions on Geminal-Cu Catalyst2Modulating Electronic Properties of N‐Heterocyclic Carbene Ligands: Effects on the Pd‐Catalyzed Buchwald–Hartwig Amination0Room-temperature Suzuki–Miyaura polycondensation of aryl dichloride monomers enabled by “large-but-flexible” Pd-NHC precatalysts1Achieving (quasi)-monocoordination in metal complexes with an exceptionally bulky carbene ligand1Research Progress on the Buchwald-Hartwig Amination Reactions Catalyzed by N-Heterocyclic Carbene Palladium Complexes1Selectivity for Exhaustive Cross-Coupling of Dihaloarenes Is Affected by the Interplay between the Halide Byproduct, Solvent, and Ligand1High color-rendering index WLEDs based on red-emission quaternary alloyed quantum dots cooperating with highly efficient green-emission NHC-Cu(I) complexes0Palladium-NHC Catalysed Biaryl Ether Formation0What is the real catalyst in M/NHC systems? From molecular complexes to cocktail-type catalysis0Two‐Coordinate 13‐Electron Pd I Complexes Stabilized by the Bulky DIMeIHept Cl NHC Ligand0

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  1. Enhancing activity and selectivity of palladium catalysts in ketone α-arylation by tailoring the imine chelate of pyridinium amidate (PYA) ligands

    Catalysis Science & Technology · 2024-12-18

    Esaïe Reusser, Michael Aeschlimann, Martin Albrecht

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  2. Ligand Substitution, Catalyst Activation, and Oxidative Addition Studies of a Stable Dialkyl Palladium Precatalyst

    Organometallics · 2025-01-06

    Ian C. Chagunda, Antonia Kropp, David C. Leitch, J. Scott McIndoe

    Read original paper ↗ ·

  3. C2-Selective Palladium-Catalyzed C–S Cross-Coupling of 2,4-Dihalopyrimidines

    Journal of the American Chemical Society · 2025-01-20

    Oliver D. Jackson, Albert Reyes, Collin D. Stein, Nathaniel G. Larson, Calvin T. Andrews, Sharon R. Neufeldt

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  4. On-Demand Access to Palladium Oxidative Addition Complexes (OACs) from a Stable Organopalladate Salt

    Organometallics · 2025-02-28

    Aidan P. Looby, Lalu Venigalla, Wenjun Hou, Mengyuan Xiao, Yongqing Yang, Hao Chen, Brad P. Carrow

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  5. Metal–N-Heterocyclic Carbene Complexes in Buchwald–Hartwig Amination Reactions

    Chemical Reviews · 2025-06-06

    Sourav Sekhar Bera, Greta Utecht‐Jarzyńska, Shiyi Yang, Steven P. Nolan, Michal Szostak

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  6. NHC/Phosphite Nickel(II) Precatalysts for the C–N Cross-Coupling of (Hetero)Aryl Chlorides under Mild Conditions

    Organic Letters · 2025-09-09

    Nutan Rajendra Darandale, Morgan E. John, Stephen A. Moggach, Dinesh Nanaji Sawant, George A. Koutsantonis, Reto Dorta, Scott G. Stewart

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  7. Initiation of Palladium Precatalysts: Efficiency and Product Selectivity as a Function of Ligand, Substrate, and Reaction Conditions

    ACS Catalysis · 2025-10-29

    Robert M. Wolesensky, María T. Morales-Colón, Melanie Sarah Sanford

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  8. Imidazolium-based covalent organic cages: from construction to functions

    Chemistry Letters · 2025-10-30

    Wenyu Zhang, Meiyu Zhang, Qiang Liu, Qing Guo He

    Read original paper ↗ ·

  9. Unexpected Deactivation of PdCl(cinnamyl)(NHC Cl ) Precatalysts Mediated by Alkylamines

    Organometallics · 2025-11-03

    Volodymyr Semeniuchenko, Sepideh Sharif, Neha Rana, Nalin Chandrasoma, Wilfried M. Braje, R. Tom Baker, Jeffrey M. Manthorpe, William J. Pietro, Michael G. Organ

    Read original paper ↗ ·

  10. Mapping the Relationship of the Dynamic Active Site and the Activation Barrier for Cross-Coupling Reactions on Geminal-Cu Catalyst

    The Journal of Physical Chemistry Letters · 2025-11-07

    Wanxiang Yang, Yi Li, Yongfan Zhang, Wei Lin

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  11. Modulating Electronic Properties of N‐Heterocyclic Carbene Ligands: Effects on the Pd‐Catalyzed Buchwald–Hartwig Amination

    European Journal of Inorganic Chemistry · 2025-11-28

    Meilin Q. Lim, Cassandra DeFrancesco, Kasandra J. Brick, Sterling Renzoni, Eric Fortin Constant, Alexander A. Glover, Casey A. Lenart, Jesse H. Leblanc, Charley N. Garrard, Eric C. Keske

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  12. Room-temperature Suzuki–Miyaura polycondensation of aryl dichloride monomers enabled by “large-but-flexible” Pd-NHC precatalysts

    Polymer Chemistry · 2025-12-30

    Juan-Juan Feng, Yuman Guo, Qian Song, Ze-Cheng Guo, Feng‐Shou Liu

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  13. Achieving (quasi)-monocoordination in metal complexes with an exceptionally bulky carbene ligand

    Chemical Science · 2026-01-01

    Ludwig Zapf, Eric Rivard

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  14. Research Progress on the Buchwald-Hartwig Amination Reactions Catalyzed by N-Heterocyclic Carbene Palladium Complexes

    化学学报 · 2026-01-01

    Yanze Xu, Nannan Han, Xiaoqiong Diao, Jinwei Yuan, Yongmei Xiao, 杨亮茹, Lingbo Qu

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  15. Selectivity for Exhaustive Cross-Coupling of Dihaloarenes Is Affected by the Interplay between the Halide Byproduct, Solvent, and Ligand

    Organometallics · 2026-02-20

    Nathaniel G. Larson, Matthew Sandin, Sharon R. Neufeldt

    Read original paper ↗ ·

  16. High color-rendering index WLEDs based on red-emission quaternary alloyed quantum dots cooperating with highly efficient green-emission NHC-Cu(I) complexes

    Journal of Luminescence · 2026-04-03

    Fei He, Feng Li, Yun Zhang, Yan Huang, Feng Zhao

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  17. Palladium-NHC Catalysed Biaryl Ether Formation

    Journal of Polytechnic · 2026-07-02

    Emine Özge Karaca, Mitat Akkoç, Nevın Gürbüz, İsmaıl Özdemır

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  18. What is the real catalyst in M/NHC systems? From molecular complexes to cocktail-type catalysis

    Catalysis Reviews · 2026-07-23

    Valentine P. Ananikov, Victor M. Chernyshev, Darya Olegovna Prima, Konstantin Evgen'evich Shepelenko

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  19. Two‐Coordinate 13‐Electron Pd I Complexes Stabilized by the Bulky DIMeIHept Cl NHC Ligand

    Chemistry - A European Journal · 2026-09-04

    Volodymyr Semeniuchenko, Sepideh Sharif, Neha Rana, Nalin Chandrasoma, Wilfried M. Braje, R. Tom Baker, Jeffrey M. Manthorpe, William J. Pietro, Michael G. Organ

    Read original paper ↗ ·
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