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RESEARCH PAPER · Green Chemistry · 2024

Synthesis of α-methylene-δ-valerolactone and its selective polymerization from a product mixture for concurrent separation and polymer production

Alexander A. Khechfe, Francesca D. Eckstrom, Eswara Rao Chokkapu, Lucas A. Baston, Bowei Liu, Eugene Y.‐X. Chen, Yuriy Román‐Leshkov

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Synthesis of α-methylene-δ-valerolactone and its selective polymerization from a product mixture for concurrent separation and polymer productionOriginalSolution and precipitation based radical polymerization of renewable vinyl lactones in renewable solvents1Green preparation of ultra-high molecular weight narrow-distribution polystyrene by enzymatic synthesis2Triacetic acid lactone conversion to methylene-δ-caprolactone: a renewable monomer for bio-based circular polymer synthesis1Selective Synthesis and Polymerization of Methyl-1,4-dioxan-2-one toward Closed-Loop Recyclable Poly(ether- alt -ester) from Methyl Glycolate and Propylene Oxide2Phenol-rich bio-oil production from Choerospondias axillaris endocarps via microwave pyrolysis coupled with ex-situ catalytic upgrading1α‐Methylene‐δ‐Valerolactone as a Bioderived Comonomer for RAFT and PhotoATRP0

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  1. Solution and precipitation based radical polymerization of renewable vinyl lactones in renewable solvents

    RSC Advances · 2025-01-01

    Dimitrios Apostolidis, William E. Dyer, Clemens A. Dransfeld, Barış Kumru

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  2. Green preparation of ultra-high molecular weight narrow-distribution polystyrene by enzymatic synthesis

    European Polymer Journal · 2025-12-07

    Xuanyu Zhang, Zongjiang Yu, Jihua Ma, Yü Liu, Huibin Zou, Chao Xu, Mo Xian

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  3. Triacetic acid lactone conversion to methylene-δ-caprolactone: a renewable monomer for bio-based circular polymer synthesis

    Green Chemistry · 2026-01-01

    Camilo A. Ortega-Vega, Bowei Liu, Francesca D. Eckstrom, Eswara Rao Chokkapu, Eugene Y.‐X. Chen, Yuriy Román‐Leshkov, Yomaira J. Pagán‐Torres

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  4. Selective Synthesis and Polymerization of Methyl-1,4-dioxan-2-one toward Closed-Loop Recyclable Poly(ether- alt -ester) from Methyl Glycolate and Propylene Oxide

    Biomacromolecules · 2026-02-18

    Dongfang Zhao, Tianqi Li, Lihang Jiang, Zheng Li, Zhibo Li

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  5. Phenol-rich bio-oil production from Choerospondias axillaris endocarps via microwave pyrolysis coupled with ex-situ catalytic upgrading

    Industrial Crops and Products · 2026-06-12

    Chuangxin Xu, Yuan Zeng, Dong Shu, Jiahui Zhang (3163929), Anqi Dai, Hao Zeng, Qiuhao Wu, Leilei Dai, Roger R. Ruan, Yunpu Wang

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  6. α‐Methylene‐δ‐Valerolactone as a Bioderived Comonomer for RAFT and PhotoATRP

    Journal of Polymer Science · 2026-08-31

    Elliott H. Denton, Banruo Huang, Mizhi Xu, Anaita Mistry, Parker T. Morris, Craig J. Hawker

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