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RESEARCH PAPER · Chemical Science · 2023

Modular, multi-robot integration of laboratories: an autonomous workflow for solid-state chemistry

Amy. M. Lunt, Hatem Fakhruldeen, Gabriella Pizzuto, Louis Longley, Alexander White, Nicola Rankin, Rob Clowes, Ben M. Alston, Lucia Gigli, Graeme Matthew Day, Andrew Ian Cooper, Samantha Yu-ling Chong

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Modular, multi-robot integration of laboratories: an autonomous workflow for solid-state chemistryOriginalAutonomous laboratories for accelerated materials discovery: a community survey and practical insights33Autonomous robotic experimentation system for powder X-ray diffraction19Chemspyd : an open-source python interface for Chemspeed robotic chemistry and materials platforms29Exploration of the polymorphic solid-state landscape of an amide-linked organic cage using computation and automation11Matching ROY crystal structures to high-throughput PXRD1The future of self-driving laboratories: from human in the loop interactive AI to gamification102Challenges in High-Throughput Inorganic Materials Prediction and Autonomous Synthesis114Deep learning of experimental electrochemistry for battery cathodes across diverse compositions49A soft cable loop based gripper for robotic automation of chemistry13Toward Making Polymer Chemistry Autonomous24Current trends and advancements in crystallization and single-crystal structural analysis of small molecules45Integration of artificial intelligence and big data in materials science: New paradigms and scientific discoveries2Accelerating Laboratory Automation Through Robot Skill Learning For Sample Scraping*12Diffusion mechanisms of fast lithium-ion conductors171Mass Spectrometry Advancements and Applications for Biomarker Discovery, Diagnostic Innovations, and Personalized Medicine76Discovery of high-performance dielectric materials with machine-learning-guided search9Reproducibility in automated chemistry laboratories using computer science abstractions28Transforming science labs into automated factories of discovery55Predicting and Accelerating Nanomaterial Synthesis Using Machine Learning Featurization32Calibration free approaches for rapid polymorph discrimination via low frequency (THz) Raman spectroscopy3LucidGrasp: Robotic Framework for Autonomous Manipulation of Laboratory Equipment with Different Degrees of Transparency via 6D Pose Estimation1The amorphous state as a frontier in computational materials design74The Changing Landscape of Materials Discovery0A multi-robot–multi-task scheduling system for autonomous chemistry laboratories32A revolutionary paradigm in chemistry and materials science research: self-driving laboratories8Autonomous laboratories in China: an embodied intelligence-driven platform to accelerate chemical discovery20Autonomy without Oversight: Governance Vacuums in Self-Driving Computational Materials Engineering Systems0Cross-disciplinary perspectives on the potential for artificial intelligence across chemistry51Enabling technology for accelerated discovery of supramolecular materials2Smart coacervate catalysis: robotic optimization of Knoevenagel reaction networks3Transforming microfluidics for single-cell analysis with robotics and artificial intelligence15Reliable and robust robotic handling of microplates via computer vision and touch feedback7Robot‐Assisted Measurement of the Critical Micelle Concentration2A Holistic Data-Driven Approach to Synthesis Predictions of Colloidal Nanocrystal Shapes14Lowering the Entrance Hurdle for Lab Automation: An Artificial Intelligence‐Supported, Interactive Robotic Arm for Automated, Repeated Testing Procedures8A Multiagent-Driven Robotic AI Chemist Enabling Autonomous Chemical Research On Demand167Comparison of Single-Arm and Dual-Arm Collaborative Robots in Precision Assembly15SmartLab: Flexible and interoperable manufacturing laboratory system for remote education and research using a mobile manipulator4Discovery of Crystalline Inorganic Solids in the Digital Age4Revolutionizing clean energy labs: Robotic imitation learning for efficient fabrication AI-powered electrical units assembly platform3Precision, intelligence, and a new paradigm for chemical research4Data-intelligent-driven exploration of robotic chemist systems1Multimodal Behaviour Trees for Robotic Laboratory Task Automation1AI-Robot-Driven Autonomous Synthesis of Functional Inorganic Thin Films0An Adaptive Contoured Soft Gripping Actuator for Chemical Experimental Glassware0Harnessing Machine Learning for the Design of Surface Coatings: Challenges and Opportunities13AI-driven new materials development and data standardization4Autonomous ‘self-driving’ laboratories: a review of technology and policy implications70Connecting metal-organic framework synthesis to applications using multimodal machine learning40Robot Arm Technology in Detection and Manipulation in Smart Pharmacies: A Review4Artificial Intelligence for Materials Discovery, Development, and Optimization171Self-driving laboratories with artificial intelligence: An overview of process systems engineering perspective14An Open-Source Capping Machine Suitable for Confined Spaces0Recent Progress in Autonomous Laboratories for Chemical Synthesis4Accelerated Porosity Screening Using a Multichannel Colorimetric Array3Accelerated Porosity Screening Using a Multichannel Colorimetric Array0Robotic system for chemical experiment automation with dual demonstration of end-effector and jig operations1A quantitative criterion for evidencing predicted compounds in high-throughput powder X-ray diffraction data: Illustration with half-antiperovskite0Accelerating discovery in natural science laboratories with AI and robotics: Perspectives and challenges19Artificial intelligence in chemical kinetics and reactor design0Serial Chemical Crystallography for Autonomous Quantitative Phase Analysis in an Electron Microscope0Perspective on utilizing foundation models for laboratory automation in materials research2Microbial Polyhydroxyalkanoates: Recovery Methods, Biopolymer Processing, Characterization, and Potential Applications4A Visual Dataset for Anomaly Detection in Self-Driving Laboratories4Localization, inspection, and reasoning (LIRA) module for autonomous workflows in self-driving laboratories4Accelerated discovery of multinary chalcogenide quantum dots: combining aqueous chemistry with high-throughput experimentation and machine learning3Toward full automation in synthetic biology: A progressive conceptual framework integrating robotics and intelligent agents2Prospects for the implementation of collaborative robotic systems in laboratory medicine: a review0Computer vision for high-throughput materials synthesis: a tutorial for experimentalists6Machine vision and robotic arm coordination for automated medical object handling—a systematic literature review1MATTERIX: toward a digital twin for robotics-assisted chemistry laboratory automation7A Large-Model-Driven Robotic AI Chemist with the Fusion of Theory and Experiment for Research0A mobile robotic process chemist2AI-driven robotic crystal explorer for rapid polymorph identification6Anomaly Management in Multi-Robot Coordination: Detection and Handling Framework for Self-Driving Laboratories0Autonomous Laboratory Planning Agent for Solid-State Form Selection and Polymorph Screening0Infrared spectroscopy-assisted prediction of impurities in chemicals using machine learning: towards smart self-driving laboratories0Multi-task scheduling of self-driving laboratories under scientific constraints1Navigating the landscape of modular reconfigurable laboratory automation in chemistry1Vision-guided adaptive scooping for powder weighing in autonomous chemistry laboratories0Using Machine Learning for Green Substitution of Industrial Chemicals: Integrating Functionality, Hazard, and Life Cycle Impact17Dara: Automated Multiple-Hypothesis Phase Identification and Refinement from Powder X-ray Diffraction6Risk Mitigation Strategies for Artificial Intelligence-Enabled Self-Driving Laboratories0A Hybrid Navigation Framework for Multi-Robot Path Planning in Dynamic Environments0Benchtop Autonomous Electrochemical Characterization System for Combinatorial Thin-Film Solid Oxide Electrodes2Machine Learning and Autonomous Systems for Accelerated Synthesis1The ADePT framework for assessing autonomous laboratory robotics8Reimagining metal-organic framework discovery: Integrating experiment, computation, and artificial intelligence6Accelerated drug development using a digital formulator and a self-driving tableting data factory6Overcoming Roadblocks for Implementing AI/ML Methods for Materials Advancement3Accelerating Discovery of Organic Molecular Crystals via Materials Informatics and Autonomous Experiments0A hierarchical task-skill autonomous decision-making framework for composite robots in chemical experiment operations0Crystal Polymorph Stability3Scaled containment control for first/second-order multi-agent systems in a noisy environment0AutoLabs: cognitive multi-agent systems with self-correction for autonomous chemical experimentation2Automation in Pharmaceutical Crystallization0Closed-Loop Machine Learning in Materials Discovery: From Predict-Validate-Update Paradigms to Autonomous Ecosystems0Multi-robot coordination for effective anomaly handling in self-driving laboratories0Cobot-based automation in sample preparation0The past, present and future of self-driving laboratories5How can high-throughput experimentation accelerate the rational design of electro-catalysts for sustainable energy conversion?0Robotic safety in self-driving laboratories0Co‐Evolution of Humans, AI, and Robotics in Autonomous Materials Manufacturing0Accelerating solid form discovery through an expert-guided, semi-automated workflow: Modular Multiwell Devices0

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  1. Autonomous laboratories for accelerated materials discovery: a community survey and practical insights

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  2. Autonomous robotic experimentation system for powder X-ray diffraction

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  3. Chemspyd : an open-source python interface for Chemspeed robotic chemistry and materials platforms

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  4. Exploration of the polymorphic solid-state landscape of an amide-linked organic cage using computation and automation

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  5. Matching ROY crystal structures to high-throughput PXRD

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  6. The future of self-driving laboratories: from human in the loop interactive AI to gamification

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  7. Challenges in High-Throughput Inorganic Materials Prediction and Autonomous Synthesis

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  8. Deep learning of experimental electrochemistry for battery cathodes across diverse compositions

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  9. A soft cable loop based gripper for robotic automation of chemistry

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  10. Toward Making Polymer Chemistry Autonomous

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  11. Current trends and advancements in crystallization and single-crystal structural analysis of small molecules

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  12. Integration of artificial intelligence and big data in materials science: New paradigms and scientific discoveries

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  13. Accelerating Laboratory Automation Through Robot Skill Learning For Sample Scraping*

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  14. Diffusion mechanisms of fast lithium-ion conductors

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  15. Mass Spectrometry Advancements and Applications for Biomarker Discovery, Diagnostic Innovations, and Personalized Medicine

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  17. Reproducibility in automated chemistry laboratories using computer science abstractions

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  18. Transforming science labs into automated factories of discovery

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  19. Predicting and Accelerating Nanomaterial Synthesis Using Machine Learning Featurization

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  20. Calibration free approaches for rapid polymorph discrimination via low frequency (THz) Raman spectroscopy

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  21. LucidGrasp: Robotic Framework for Autonomous Manipulation of Laboratory Equipment with Different Degrees of Transparency via 6D Pose Estimation

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  22. The amorphous state as a frontier in computational materials design

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  23. The Changing Landscape of Materials Discovery

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  24. A multi-robot–multi-task scheduling system for autonomous chemistry laboratories

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  27. Autonomy without Oversight: Governance Vacuums in Self-Driving Computational Materials Engineering Systems

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