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RESEARCH PAPER · Nano Research · 2023

The reformation of catalyst: From a trial-and-error synthesis to rational design

Ligang Wang, Jiabin Wu, Shunwu Wang, Huan Liu, Yao Wang, Dingsheng S. Wang

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The reformation of catalyst: From a trial-and-error synthesis to rational designOriginalWirkung von Spinosad (Audienz) gegen Erdflöhe (Phyllotreta sp.) an Brokkoli0User-Generated Contentにおける潜在情報抽出手法の提案0Rational Synthesis of Methylsilsesquioxane Aerogels Addressing Thermal Load and Compression Recovery Issues in Li-Ion Batteries11Boosting catalytic activity toward methanol oxidation reaction for platinum via heterostructure engineering48Low-coordination environment design of single Co atoms for efficient CO2 photoreduction26Dipole–Dipole Tuned Electronic Reconfiguration of Defective Carbon Sites for Efficient Oxygen Reduction into H 2 O 235Volume-complementary bipolar layered oxide enables stable symmetric sodium-ion batteries23Advances in the study of HOR reaction mechanisms under alkaline conditions12Atomically dispersed metal cocatalysts for solar energy conversion45Atomically dispersed multi-site catalysts: bifunctional oxygen electrocatalysts boost flexible zinc–air battery performance89Composition regulation of Ni-BDC MOF architecture to enhance electrocatalytic urea oxidation in alkaline solution16Coordination polymer derived Fe–N–C electrocatalysts with high performance for the oxygen reduction reaction in Zn–air batteries9Doping Ru on FeNi LDH/Fe II/III –MOF heterogeneous core–shell structure for efficient oxygen evolution23Enhanced photocatalytic CO 2 reduction to CH 4 via restorable surface plasmon and Pd n –W δ + synergetic sites23Expedient alkyne semi-hydrogenation by using a bimetallic AgCu–C3N4 single atom catalyst12Indium oxide with oxygen vacancies boosts O 2 adsorption and activation for electrocatalytic H 2 O 2 production22Insights into the pH effect on hydrogen electrocatalysis172Microenvironment engineering of covalent organic framework based single/dual-atom catalysts toward sustainable energy conversion and storage86Single‐atom materials: The application in energy conversion87Strong Electronic Coupling between Ni-Based Mof and Ni2p Enables High-Efficiency Oxygen Evolution Reaction for Various Application Scenarios15Sulfur-doped g-C 3 N 4 /V 2 C MXene Schottky junctions for superior photocatalytic H 2 evolution55Thermal control of photothermal implants inspired by polar bear skin for the treatment of infected bone defects14A general and facile calcination method to synthesize single-site catalysts for highly efficient electrochemical CO2 reduction13Self-dispersed bimetallic NiRu nanoparticles on CeO2 for CO2 methanation48Coordination Confined Thermolysis Synthesis of the Ni Single Atom Catalyst on the N-Doped Commercial Carbon for the Production of Syngas2Phosphorus-substituted atomically dispersed Rh-N3P1 sites for efficient promotion in CO2 hydrogenation towards ethanol production34Pd–Mn/NC Dual Single-Atomic Sites with Hollow Mesopores for the Highly Efficient Semihydrogenation of Phenylacetylene127Spatial configuration of Fe–Co dual-sites boosting catalytic intermediates coupling toward oxygen evolution reaction150Ru-Ni alloy nanosheets as tandem catalysts for electrochemical reduction of nitrate to ammonia42Bimetallic Interface of RuCu Hollow Nanostructures Combined with B 4 C for Enhancing Electrocatalysis on Nitrate Reduction24Cascade Dual Sites Modulate Local CO Coverage and Hydrogen-Binding Strength to Boost CO2 Electroreduction to Ethylene197RhCuBi Trimetallenes with Composition Segregation Coupled Crystalline‐Amorphous Heterostructure Toward Ethanol Electrooxidation50Anchoring Ru clusters to highly defective N-doped carbon nanotubes via a thermal-shock strategy for stable industrial hydrogen evolution22Tandem catalysis in electrocatalytic nitrate reduction: Unlocking efficiency and mechanism92BiVO4 as a precatalyst for CO2 electroreduction to formate at large current density18Insights into atom-level local reactions for CO2 photocatalytic production: Reaction pathways and product selectivity at the atomic level3Donor–acceptor covalent organic frameworks-confined ultrafine bimetallic Pt-based nanoclusters for enhanced photocatalytic H2 generation48Heterogeneous Iridium-Catalyzed Carbene N–H Bond Insertion with α-Alkyl Diazo Esters29Remodeling the Electronic Structure of Metallic Nickel and Ruthenium via Alloying in a Molecular Template for Sustainable Hydrogen Evolution10Constructing Highly Efficient ZnO Nanocatalysts with Exposed Extraordinary (110) Facet for CO 2 Electroreduction33Enhanced Fenton-like catalysis through in-situ bismuth defection in Bi/CuBi2O4: Vacancy mechanisms11A method to synthesize specific active Cu sites of single-atom catalysts with high stability for acetylene hydration7Molecular and single-atom catalysts based on earth-abundant transition metals for the electroreduction of CO2 to C18Research progress in electrocatalytic reduction of nitrate to ammonia by copper-based materials7Pt single atoms coupled with Ru nanoclusters enable robust hydrogen oxidation for high-performance anion exchange membrane fuel cells19Atomic Pt Sites Anchored in the Interface between Grains on Vacancy‐Enriched CeO2 Nanosheets: One‐Step Precursor Combustion Synthesis41Ligand effect in surface atomic sites of group VI B transition metals on ultrathin Pt nanowires for enhanced oxygen reduction7Tailoring Oxygen Reduction Reaction Kinetics of Fe−N−C Catalyst via Spin Manipulation for Efficient Zinc–Air Batteries378A review of electroreduction of CO2 to C1 products: Catalysts design, characterizations and performance evaluation19Strain regulation of bond length in single Ru sites via curving support surface for enhanced hydrogen evolution reaction35Unraveling Two Pathways for Electrocatalytic Acetonitrile Reduction25Near-Infrared Luminescent Single-Atom Gold Modified Cadmium Sulfide Quantum Dots for Consuming Trace l -Cysteine5Surface reconstruction and synergistic electrocatalysis of perovskite K-Ni-Zn-F for efficient urea-based energy conversion19Coordination engineering and electronic structure modulation of FeNi dual-single-atoms encapsulated in N, P-codoped 3D hierarchically porous carbon electrocatalyst for synergistically boosting oxygen reduction reaction50Multistep Quenching of a Rust-Derived Catalyst for Enhanced Volatile Organic Compound Catalytic Oxidation23Cobalt-and-Nitrogen-Doped Carbon Nanoparticle Catalysts for Selective Hydrogen Transfer Reactions10Ternary heterojunction of cross-linked benzene Polymer/Bi2MoO6-Graphene oxide catalysts promote efficient adsorption and photocatalytic removal of oxytetracycline19Theoretical calculations and experimental verification of carbon dioxide reduction electrocatalyzed by metalloporphyrin24Heterobimetallic [NiCo] integration in a hydrogenase mimic for boosting light-driven hydrogen evolution in CaTiO36Surface hydroxyl manipulation of BiOCl nanosheets for promoted O2 activation and photocatalytic NO removal11Carbon-based single-atom catalysts derived from biomass: Fabrication and application57Precise Modulation of the Coordination Environment of Single Cu Site Catalysts to Regulate the Peroxymonosulfate Activation Pathway for Water Remediation19Single‐element amorphous metals10Stable hydrogen-bonded organic frameworks and their photo- and electro-responses28Accelerating H* desorption of hollow Mo2C nanoreactor via in-situ grown carbon dots for electrocatalytic hydrogen evolution43A selectivity switch for CO2 electroreduction by continuously tuned semi-coherent interface27Deciphering Cationic and Anionic Overoxidation: Key Insights into the Intrinsic Structural Degradation of Catalysts48Balancing the Binding of Intermediates Enhances Alkaline Hydrogen Oxidation on D-Band Center Modulated Pd Sites9Electronic structure engineering of single atomic sites by plasmon-induced hot electrons for highly efficient and selective photocatalysis20Designing of highly-efficient OER and ORR transition metal-nitrogen active centers with the aid of the revised d electron density19Design of Mg-Ni binary single-atom catalysts for conversion of carbon dioxide to syngas with a wide tunable ratio: Each species doing its own job or working together to win?23Atomic-level precision engineering: Single-atom catalysts with controlled loading density for efficient hydrogen evolution reaction6Designing 3d Transition Metal Cation-Doped MRuO x As Durable Acidic Oxygen Evolution Electrocatalysts for PEM Water Electrolyzers170Enhancing Electrocatalytic CO2-to-CO Conversion by Weakening CO Binding through Nitrogen Integration in the Metallic Fe Catalyst14Regulating the Critical Intermediates of Dual‐Atom Catalysts for CO 2 Electroreduction27Efficient Hydrogen Generation from Ammonia Borane Hydrolysis on a Tandem Ruthenium–Platinum–Titanium Catalyst15Efficient Hydrogen Generation from Ammonia Borane Hydrolysis on a Tandem Ruthenium–Platinum–Titanium Catalyst112Scalable graphene foam with ultrahigh conductivity for stabilizing Pt towards efficient hydrogen evolution5Trace Pd alloyed with Au to boost Au/uncalcined TS-1 catalyzed propane hydro-oxidation to acetone8Upcycling electroplating sludge into bioengineering-enabled highly stable dual-site Fe-Ni2P@C electrocatalysts for efficient oxygen evolution4Application of machine learning in designing and understanding effective catalyst for selective catalytic reduction of nitrogen oxide19Engineering the asymmetric active moiety of Ce-N 3P for efficient selective oxidation of aromatic C–H bonds4In-situ assembled cobalt-free PSFNRu nanocomposites as bi-functional electrodes for direct ammonia symmetric solid oxide fuel cells5Synergistic effects of single atoms and nanoparticles: Emerging opportunities for electrocatalysis13Synergy of Photogenerated Electrons and Holes toward Efficient Photocatalytic Urea Synthesis from CO 2 and N 217Synergy of Photogenerated Electrons and Holes toward Efficient Photocatalytic Urea Synthesis from CO 2 and N 2110Single‐atom catalysts: controlled synthesis and dynamic mechanism in electrochemical oxygen evolution substitution reactions21Improving Generation Performance of 1O2 by Atomic Doping for Efficient Catalytic Advanced Oxidation Processes42One-step electrodeposition synthesis of NiFePS on carbon cloth as self-supported electrodes for electrochemical overall water splitting88Screening of Pd-Co-Ni catalyst arrays by scanning electrochemical microscopy and characterization of the potential catalyst for formic acid oxidation8Efficient industrial-current-density H2O2 production in neutral medium via external-shell boron regulation on single-atom VN4 sites10Engineering the Active Sites of MOF ‐derived Catalysts: From Oxygen Activation to Activate Metal‐Air Batteries†35Sn/SnO2 Nanocomposite Encapsulated on Nitrogen-Doped Carbon as a Highly Efficient Catalyst for the Electrochemical Reduction of CO2 to Formate17Unveiling structural evolution of Fe single atom catalyst in nitrate reduction for enhanced electrocatalytic ammonia synthesis47Oxygen vacancy promoting artificial atom (RuPd) by d-orbital coupling for efficient water dissociation26Efficient Electrochemical Nitrate Reduction to Ammonia Driven by a Few Nanometer-Confined Built-In Electric Field83Revealing the role of electrode potential micro-environments in single Mn atoms for carbon dioxide and oxygen electrolysis41Ultrafast and highly‐selective upcycling of plastic polylactic acid waste driven by ZnInFe ‐mixed metal oxide17Boosting oxygen reduction in acidic media through integration of Pt-Co alloy effect and strong interaction with carbon defects32Highly efficient recycling of polyester wastes to diols using Ru and Mo dual-atom catalyst53Tensile Strain and Interatomic Orbital Hybridization Effects Boost the Electrocatalytic Performance of Intermetallic Pd3Pb Nanowires for Ethanol Electrooxidation†26Atomic-Level Asymmetric Tuning of the Co 1 –N 3 P 1 Catalyst for Highly Efficient N -Alkylation of Amines with Alcohols96Multifunction of MXene in Lithium–Sulfur Batteries: A Review20Hydrogen peroxide electrosynthesis via two-electron oxygen reduction: From pH effect to device engineering10Modulating electronic structure and exposed surface area of Cu-based catalysts by Pd doping for enhanced CO2 hydrogenation to methanol13Oxygen-bridging Fe, Co dual-metal dimers boost reversible oxygen electrocatalysis for rechargeable Zn–air batteries79Poly (heptazine imide) nanocrystal for hydrogen peroxide evolution in the dark by accumulating photo-generated electrons11Carbon-Boosted and Nitrogen-Stabilized Isolated Single-Atom Sites for Direct Dehydrogenation of Lower Alkanes224f–2p–3d Orbital Coupling in Ce–Ni3S2 Enhancing the Urea Oxidation Reaction13Tuning the Local Environment of Pt Species at CNT@MO2–x (M = Sn and Ce) Heterointerfaces for Boosted Alkaline Hydrogen Evolution191Experimental and theoretical investigation of sulfur-doped g-C3N4 nanosheets/FeCo2O4 nanorods S-scheme heterojunction for photocatalytic H2 evolution71Unlocking opportunities: Supported metal catalysts for the chemical upcycling of waste plastics26Maximizing hydrogen evolution via Co–Ni dual atoms and nanoclusters on hierarchically ordered porous carbon framework10High-efficiency crystalline carbon nitride photocatalysts: Status and perspectives39Steering the Site Distance of Atomic Cu−Cu Pairs by First‐Shell Halogen Coordination Boosts CO 2 ‐to‐C 2 Selectivity12Steering the Site Distance of Atomic Cu−Cu Pairs by First‐Shell Halogen Coordination Boosts CO2‐to‐C2 Selectivity170Tailoring microenvironment for efficient CO2 electroreduction through nanoconfinement strategy35Copper Atom Pairs Stabilize *OCCO Dipole Toward Highly Selective CO 2 Electroreduction to C 2 H 4110Copper Atom Pairs Stabilize *OCCO Dipole Toward Highly Selective CO2 Electroreduction to C2H46Advances of W-based catalysts from material to electrocatalysis28Periodic Single‐Metal Site Catalysts: Creating Homogeneous and Ordered Atomic‐Precision Structures32Zinc Assisted Thermal Etching for Rich Edge‐Located Fe‐N4 Active Sites in Defective Carbon Nanofiber for Activity Enhancement of Oxygen Electroreduction33Tailoring the Hydrogen Spillover Effect in Ni-Based Heterostructure Catalysts for Boosting the Alkaline Hydrogen Oxidation Reaction51A General Metal Ion Recognition Strategy to Mediate Dual-Atomic-Site Catalysts123Inducing a Synergistic Effect on Pt δ+ /Electron-Rich Sites via a Platinization Strategy: Generating Hyper-High Current Density in Hydrogen Evolution Reaction26Multi-atomic catalysts: Pioneering applications in the pursuit of carbon neutrality9Application of metal-based catalysts for Fenton reaction: from homogeneous to heterogeneous, from nanocrystals to single atom57Recent progress in electrochemical synthesis of urea through C-N coupling reactions8Controllable selective anchoring of subnanometric Ru clusters or single-atoms/clusters on tungsten nitride for the hydrogen oxidation12Catalytic recycling of plastics into value-added products28Suppressing Metal-Support Interaction Enhances Photothermal CO 2 Methanation on the Ru/CeO 2 Catalysts81Enhanced Fenton-like reactions via interface electron reconstruction in low-crystallinity Fe Co bimetallic metal–organic frameworks: Bidirectional control of Fe (III) and Co (II) sites19Precise synthesis of dual atom sites for electrocatalysis153Recent advances in dual‐atom catalysts for energy catalysis27Advancing Heterogeneous Organic Synthesis With Coordination Chemistry‐Empowered Single‐Atom Catalysts66Electrocatalytic Aromatic Alcohols Splitting to Aldehydes and H2 Gas25Advances in Stability of NiFe‐Based Anodes toward Oxygen Evolution Reaction for Alkaline Water Electrolysis66Atomically Dispersed Palladium Catalyst for Chemoselective Hydrogenation of Quinolines39Iron single atoms and nitrogen vacancies on graphitic carbon nitride synergically shallowing deep electron traps towards efficient photocatalytic ozonation12Anchored Fe3O4/Fe nanoparticles on hollow PPy nanotube@Fe-modified ZIF-8 derivative for enhanced ORR activity in zinc-air batteries12Enhanced Zinc-air battery performance and local electrochemical evaluation of atomically dispersed Co and Ni in S, N-codoped carbon nanofibersvia scanning electrochemical microscopy11Manipulation of d-Orbital Electron Configurations in Nonplanar Fe-Based Electrocatalysts for Efficient Oxygen Reduction20Metal-nitrogen coordinated single atomic photocatalysts for solar energy conversion18Oriented Conversion of HMF to FDCA under Mild Conditions over Lignin-Tailored Co Single-Atom Catalyst with Enhanced Co Loadings73Upcycling of Polyamide Wastes to Tertiary Amines Using Mo Single Atoms and Rh Nanoparticles65Upcycling of Polyamide Wastes to Tertiary Amines Using Mo Single Atoms and Rh Nanoparticles9Integrating few-atom layer metal on high-entropy alloys to catalyze nitrate reduction in tandem132Engineering single-atomic Ni sites stabilized with adjacent spinel nanoparticles to boost CO2 electroreduction12Anion intercalation of NiMn-LDH accelerating urea electrooxidation on trivalent nickel12Pt‐Mo₂N Catalyst Formed by Inverse Sintering for the Reverse Water‐Gas Shift Reaction16

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  1. Wirkung von Spinosad (Audienz) gegen Erdflöhe (Phyllotreta sp.) an Brokkoli

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  4. Boosting catalytic activity toward methanol oxidation reaction for platinum via heterostructure engineering

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  5. Low-coordination environment design of single Co atoms for efficient CO2 photoreduction

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  6. Dipole–Dipole Tuned Electronic Reconfiguration of Defective Carbon Sites for Efficient Oxygen Reduction into H 2 O 2

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  11. Composition regulation of Ni-BDC MOF architecture to enhance electrocatalytic urea oxidation in alkaline solution

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  17. Insights into the pH effect on hydrogen electrocatalysis

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  18. Microenvironment engineering of covalent organic framework based single/dual-atom catalysts toward sustainable energy conversion and storage

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  20. Strong Electronic Coupling between Ni-Based Mof and Ni2p Enables High-Efficiency Oxygen Evolution Reaction for Various Application Scenarios

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  31. Cascade Dual Sites Modulate Local CO Coverage and Hydrogen-Binding Strength to Boost CO2 Electroreduction to Ethylene

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  32. RhCuBi Trimetallenes with Composition Segregation Coupled Crystalline‐Amorphous Heterostructure Toward Ethanol Electrooxidation

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  33. Anchoring Ru clusters to highly defective N-doped carbon nanotubes via a thermal-shock strategy for stable industrial hydrogen evolution

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  34. Tandem catalysis in electrocatalytic nitrate reduction: Unlocking efficiency and mechanism

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  35. BiVO4 as a precatalyst for CO2 electroreduction to formate at large current density

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  36. Insights into atom-level local reactions for CO2 photocatalytic production: Reaction pathways and product selectivity at the atomic level

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  38. Heterogeneous Iridium-Catalyzed Carbene N–H Bond Insertion with α-Alkyl Diazo Esters

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  40. Constructing Highly Efficient ZnO Nanocatalysts with Exposed Extraordinary (110) Facet for CO 2 Electroreduction

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  41. Enhanced Fenton-like catalysis through in-situ bismuth defection in Bi/CuBi2O4: Vacancy mechanisms

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  42. A method to synthesize specific active Cu sites of single-atom catalysts with high stability for acetylene hydration

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  43. Molecular and single-atom catalysts based on earth-abundant transition metals for the electroreduction of CO2 to C1

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  44. Research progress in electrocatalytic reduction of nitrate to ammonia by copper-based materials

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  48. Tailoring Oxygen Reduction Reaction Kinetics of Fe−N−C Catalyst via Spin Manipulation for Efficient Zinc–Air Batteries

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  49. A review of electroreduction of CO2 to C1 products: Catalysts design, characterizations and performance evaluation

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  50. Strain regulation of bond length in single Ru sites via curving support surface for enhanced hydrogen evolution reaction

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