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RESEARCH PAPER · Matter · 2023

Closed-loop optimization of nanoparticle synthesis enabled by robotics and machine learning

Jungwon Park, Young Min Kim, Seonghun Hong, Byungchan Han, Ki Tae Nam, Yousung Jung

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Closed-loop optimization of nanoparticle synthesis enabled by robotics and machine learningOriginal3D-printed microfluidic system for the in situ diagnostics and screening of nanoparticles synthesis parameters16Communicating Supraparticles to Enable Perceptual, Information‐Providing Matter11Artificial Intelligence for Surface‐Enhanced Raman Spectroscopy149Evolutionary Monte Carlo of QM Properties in Chemical Space: Electrolyte Design5Toward Making Polymer Chemistry Autonomous24A mini review on the applications of artificial intelligence (AI) in surface chemistry and catalysis27Two-step machine learning-assisted label-free surface-enhanced Raman spectroscopy for reliable prediction of dissolved furfural in transformer oil3When Metal Nanoclusters Meet Smart Synthesis31Automated synthesis and processing of functional nanomaterials: Advances and perspectives27OCTOPUS: operation control system for task optimization and job parallelization via a user-optimal scheduler12Convergence of Nanotechnology and Machine Learning: The State of the Art, Challenges, and Perspectives61Perspective—Rising Era of Green Semiconductors at Nanoscale: Challenges and Prospects20A data-driven approach to interfacial polymerization exploiting machine learning for predicting thin-film composite membrane formation17Biological Synthesis of Nanomaterials1Decision Authority Frameworks in Autonomous Materials Discovery Systems0Digitalisation of catalytic processes for sustainable production of biobased chemicals and exploration of wider chemical space8From synthesis to properties: expanding the horizons of machine learning in nanomaterials research39Machine learning approach for surface morphology of nanoparticles: Image analysis and data mining techniques1Microfluidic-based nanocarriers for overcoming biological barriers in therapeutic delivery systems12Perspective: From Prediction to Design — A Position on Optimization-Centric Workflows in Materials ML0Electrochemical CO2 reduction to liquid fuels: Mechanistic pathways and surface/interface engineering of catalysts and electrolytes34Magnetic–Plasmonic Core–Shell Nanoparticles: Properties, Synthesis and Applications for Cancer Detection and Treatment9Advancing perovskite photovoltaic technology through machine learning‐driven automation49AI-driven innovations in smart multifunctional nanocarriers for drug and gene delivery: A mini-review75A Control Theory Informed Machine Learning-Based Modeling and Monitoring of Nanoparticle Generation Processes3Reaching new frontiers in nanoelectronics through artificial intelligence4Fabrication of manganese-tin electrodes for sodium-ion battery and supercapacitor applications via laser ablation, laser texturing, and inkjet printing11Recent Advancements in the Field of Nanotechnology Using Artificial Intelligence, Data Science and Machine Learning8Advances in Gasoline Hydrodesulfurization Catalysts: The Role of Structure–Activity Relationships and Machine Learning Approaches13Machine Learning-Based Recommender System for Pulsed Laser Ablation in Liquid: Recommendation of Optimal Processing Parameters for Targeted Nanoparticle Size and Concentration Using Cosine Similarity and KNN Models1Machine Learning for Controlling the Particle Size Distribution of TiO2 Nanoparticles in Optical Nanocomposites1From Spin to Star: Ultrafast Dual‐Gradient Centrifugal Microfluidics for Scalable High‐Throughput and Combinatorial Nanomaterial Synthesis1Quality by digital design for accelerated sustainable nanomedicine development26Advances in stimuli-responsive nanoparticles for cancer therapy: Mechanisms, functional materials, and emerging technologies12Artificial intelligence for nanomedicine15Harnessing Microfluidics for the Effective and Precise Synthesis of Advanced Materials12Biosynthesis, optimization, and characterization of CuNPs using Bacillus licheniformis CPJN13S and their antibacterial activity1Multifunctional bio-nanostructure for cancer therapy: mini review0Precision nanoscience aided by multimodal observations0Nanoparticle-mediated bone regeneration: From molecular mechanisms to clinical translation5Fortalecimiento en la biotecnología a través de la inteligencia artificial generativa: revisión sistemática sobre avances, desafíos y oportunidades para la Amazonia Colombiana0Model based process optimization for nanoparticle precipitation1Artificial intelligence-driven nanomaterial design and applications: advances, challenges, and future directions0Perspective: Autonomous Laboratories and Real-Time ML Feedback Loops — A Position for Closed-Loop Discovery0Pessimistic asynchronous sampling in high-cost Bayesian optimization0Synthesis, Characterization, and Properties of Nanomaterials2Toward a High-Throughput Automated Materials Experimentation Platform: Hybrid-Automata-Inspired Modeling and Equipment Configuration Optimization0Machine Learning for Nanomaterial Discovery and Design16Scaling up plasma-derived metallic nanoalloys: A comprehensive review of production bottlenecks, manufacturing readiness, and AI-driven pathways to viability1From conventional screening to self-driving discovery: Organ-on-Chip platforms as engines for AI-guided nanomedicine5Smart Exploration of Perovskite Photovoltaics: From AI Driven Discovery to Autonomous Laboratories1Artificial intelligence shaping the future of hydrogen technologies6Physics-informed machine learning for tumor microenvironment-responsive nanomedicine: Recent updates3From Discovery to Deliverables: Bridging the Machine Learning, Synthesis, and Characterization Gap in Nanoscale Materials1Integrated Machine Learning and Molecular Dynamics for Functional Nanoparticle Design: Synthesis, Characterization, Force-Field Development, and Property Prediction2Convergence of molecular biology and nanobiotechnology: Advances in precision therapeutics and next-generation diagnostics0Recent progress of green synthesized and multifunctional metal oxide nanoparticles for advanced environmental remediation: A review2Nanomedicine-enabled tumor pyroptosis-immunotherapy: From material design and synergistic mechanisms to clinical perspectives1Green synthesis of nanoparticles: a comprehensive review of biogenic methods and their applications1Data-Driven Engineering of Antimicrobial Nanomaterials for Food Safety and Biomedical Systems8Machine learning-driven surface and interface engineering in perovskite quantum dots for photoluminescence-based and chemical sensing platforms0Autonomous laboratories for sustainable nanomaterials discovery0A Brief Review of Density Functional Theory and Machine Learning Insights into Pristine, Binary, and Ternary CdS-Based Photocatalysts for Efficient Water Splitting0An End-to-End Robotic System for High-Precision Rack Insertion in Automated Laboratories*0Data-driven design of carbon dots: Property prediction, optimization, and prospects for autonomous discovery0Machine learning for cracking the molecular code of room-temperature organic phosphorescent materials: From structure-property relationship to performance prediction0Nanodrug-mediated strategies for targeting the undruggable: Comparative perspectives on targeted protein degradation and stabilization0Explainable machine learning in carbon dot research: From prediction to scientific understanding0From natural-extract variability to reproducible nanomaterials: AI-QbD strategies for green synthesis from agro-food waste0Microfluidic engineering of polymer-based drug delivery systems: From particle synthesis to organ-on-a-chip validation and application0Multivariate synthesis optimization, comprehensive characterization, and surface ligand determination of palladium nanoparticles0Generative artificial intelligence for nanomaterial discovery and nanoengineering: From data-driven design to autonomous laboratories0

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