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RESEARCH PAPER · Journal of the American Chemical Society · 2023

Diverse Alkyl–Silyl Cross-Coupling via Homolysis of Unactivated C(sp 3 )–O Bonds with the Cooperation of Gold Nanoparticles and Amphoteric Zirconium Oxides

Hiroki Miura, Masafumi Doi, Yuki Yasui, Yosuke Masaki, Hidenori Nishio, Tetsuya Shishido

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Diverse Alkyl–Silyl Cross-Coupling via Homolysis of Unactivated C(sp 3 )–O Bonds with the Cooperation of Gold Nanoparticles and Amphoteric Zirconium OxidesOriginalPalladium-catalyzed C(sp 3 )–Si cross-coupling silylation of benzyl halides with hydrosilanes11Deoxygenative Silylation of C(sp3)–O Bonds with Hydrosilane by Cooperative Catalysis of Gold Nanoparticles and Solid Acids24Silylation of Alkyl Esters and Ethers Catalyzed by Gold Nanoparticles on Zirconium Oxides0Harnessing Supported Gold Nanoparticle as a Single‐Electron Transfer Catalyst for Decarboxylative Cross‐Coupling14Nickel-catalyzed cross-electrophile C-Ge coupling of benzyl pivalates and chlorogermanes26Partially Thiolated Au n ( n = 25, 102) Clusters on Layered Double Hydroxides Anchored by Electrostatic Interactions: Size Effect on 5-Hydroxymethylfurfural Oxidation Catalysis35Preparation of Nickel-Immobilized-Sio2-Tio2 Fine Particles in the Presence of Cetyltrimethylammonium Bromide as a Catalyst for Ultrasound-Assisted-Kumada Cross Coupling Reaction0Synthesis of colloidal Pd nanoparticles immobilised on poly( N -vinylacetamide): characterisation and application in catalysis0Directing-Group-Assisted Non-Strained Ether C–O Bond Homolysis Mediated by Low-Valent Titanium4Borylation of Stable C(sp3)–O Bonds of Alkyl Esters over Supported Au Catalysts10Pt(II) complexes bearing P,N-donor ligands as catalysts in chemoselective hydrosilylation, hydrogermylation, and hydroboration of terminal alkenes15Synthesis of goldene comprising single-atom layer gold155Axial Ligand Enables Synthesis of Allenylsilane through Dirhodium(II) Catalysis1Axial Ligand Enables Synthesis of Allenylsilane through Dirhodium(II) Catalysis15Organophotocatalyzed Cross Coupling of C- and Si-Radical to Access Dibenzylic Silanes from para-Quinone Methides and Silanecarboxylic Acids6Novel nickel-immobilized-SiO2-TiO2 fine particles in the presence of cetyltrimethylammonium bromide as a catalyst for ultrasound-assisted-Kumada cross-coupling reaction1Optimization of Metal–Support Cooperation for Boosting the Performance of Supported Gold Catalysts for the Borylation of C–O and C–N Bonds9Synthesis of organoboron compounds via heterogeneous C–H and C–X borylation4Unsaturated organosilanes: synthesis, transformations and applications3Substrate-Dependent Role of a Pd Dopant in PdAu12 Catalysts in the Oxidation of p-Substituted Benzyl Alcohols: Promotion of Hydride Abstraction and Reductive Activation of O217Low-Temperature Borylation of C(sp 3 )–O Bonds of Alkyl Ethers by Gold–Metal Oxide Cooperative Catalysis8Reaction mechanism of silylation of C–O bonds in alkyl ethers over supported gold catalysts: experimental and theoretical investigations0Conversion of Polypropylene to Light Olefins by HMFI Catalysts below Pyrolytic Temperature: Catalytic, Spectroscopic, and Theoretical Studies3Formal Transesterification Reaction of But-3-enyl Esters Enabled by a Synergistic Nickel/Zinc Relay1Hydrosilylation or dehydrogenative silylation pathways via the Au-catalyzed activation of hydrosilanes6Synthesis of Colloidal DMF-Protected Cobalt Nanoparticles for Alkene Hydrosilylation Catalyst: Effect of Cobalt Precursors and Recycling Process6Perspectives on noble metallenes: from synthesis to application8One-Pot Sequential Alcohol Activation and Nickel-Catalyzed Cross-Electrophile Coupling with Chlorosilanes14Rhodium/Indium Heterobimetallic Alloy as an Effective Catalyst for Reductive C(sp 3 )─O Silylation of Ethers with Chlorosilanes0Rhodium/Indium Heterobimetallic Alloy as an Effective Catalyst for Reductive C(sp 3 )─O Silylation of Ethers with Chlorosilanes2Electrochemical synthesis of allenyl silanes and allenyl boronic esters7Dynamics of Cooperative Palladium/Copper Catalysis for Aerobic Oxidative Difunctionalization of 1,3-Dienes with Aniline and Disilane6Harnessing Electrochemistry for Direct Deoxygenative Silylation of Alcohols and Ketones17Harnessing Electrochemistry for Direct Deoxygenative Silylation of Alcohols and Ketones3Upcycling C–O Bond Polymers into Value‐Added Chemicals with Air as the Sole Oxidant2Reductive Cross‐Coupling of Alcohol Derivatives with Chlorosilanes via Pyridines‐Promoted Si─Cl Activation2Reductive Cross‐Coupling of Alcohol Derivatives with Chlorosilanes via Pyridines‐Promoted Si─Cl Activation6Regioselective Carbosilylation of Allenes by Supported Au Catalysts2Microwave-Assisted Construction of Acid–Base Cooperative Layered Heterogeneous Catalysts for Dehydrogenative Coupling of Silanes with Alcohols1Electronic and optical properties of two-dimensional monolayer noble metals: A first-principles approach1Cobalt-catalysed deoxygenative silylation of oxo-compounds0Electrochemical deoxygenation: a green tool for functional molecule diversification – challenges and opportunities6Photo-catalyzed hydroxylation and disulfidation of vinyl arenes with tetrasulfides, oxygen and water0General synthesis of ordered mesoporous gallate spinels with ultrathin frameworks for gas sensing and catalytic applications2Auene‐Supported Transition‐Metal Single‐Atom Catalysts for Promising Electrocatalytic Nitrogen Reduction0Cleavage of Si–O–Si bonds with alcohols catalyzed by p -toluenesulfonic acid: synthesis of monoalkoxysilanes and computational mechanistic study1Functions Containing at Least One Metalloid (Si, Ge, or B) and no Halogen, Chalcogen, or Group 15 Element; Also Functions Containing Two Metals0Deoxygenative functionalization of alcohols, ethers, and carbonyl compounds by chromium catalysis0

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  2. Deoxygenative Silylation of C(sp3)–O Bonds with Hydrosilane by Cooperative Catalysis of Gold Nanoparticles and Solid Acids

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  4. Harnessing Supported Gold Nanoparticle as a Single‐Electron Transfer Catalyst for Decarboxylative Cross‐Coupling

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  7. Preparation of Nickel-Immobilized-Sio2-Tio2 Fine Particles in the Presence of Cetyltrimethylammonium Bromide as a Catalyst for Ultrasound-Assisted-Kumada Cross Coupling Reaction

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  10. Borylation of Stable C(sp3)–O Bonds of Alkyl Esters over Supported Au Catalysts

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  11. Pt(II) complexes bearing P,N-donor ligands as catalysts in chemoselective hydrosilylation, hydrogermylation, and hydroboration of terminal alkenes

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  22. Reaction mechanism of silylation of C–O bonds in alkyl ethers over supported gold catalysts: experimental and theoretical investigations

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