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RESEARCH PAPER · Nature Chemistry · 2023

High-throughput phase elucidation of polycrystalline materials using serial rotation electron diffraction

Yi Luo, Bin Wang, Stef Smeets, Junliang Sun, Weimin Yang, Xiaodong Zou

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High-throughput phase elucidation of polycrystalline materials using serial rotation electron diffractionOriginalSCM-25: A Zeolite with Ordered Meso-cavities Interconnected by 12 × 12 × 10-Ring Channels Determined by 3D Electron Diffraction173D electron diffraction for structure determination of small‐molecule nanocrystals: A possible breakthrough for the pharmaceutical industry20Electron crystallography and dedicated electron-diffraction instrumentation27Autonomous MicroED data collection enables compositional analysis8Phase identification and discovery of hidden crystal forms in a polycrystalline pharmaceutical sample using high-throughput 3D electron diffraction1Making the Most of 3D Electron Diffraction: Best Practices to Handle a New Tool43Visualization of topotactic structural transformations of zeolites using 3D electron diffraction4Covalent-coordination driven hierarchical assembly of tubular frameworks0STEM SerialED: achieving high-resolution data for ab initio structure determination of beam-sensitive nanocrystalline materials27Advances and applications of microcrystal electron diffraction (MicroED)8High-Throughput Identification of Crystalline Natural Products from Crude Extracts Enabled by Microarray Technology and microED29Compositional Analysis of Complex Mixtures using Automatic MicroED Data Collection20High-ion-conductive zeolite X with built-in < 1 nm 3D pores achieving superior thermoelectric performance1Current trends and advancements in crystallization and single-crystal structural analysis of small molecules45Hierarchical assembly of tubular frameworks driven by covalent and coordinate bonding25Three-Dimensional Electron Diffraction: A Revolutionary Technique for Structure Analysis of Nano-sized Minerals1MicroED: Unveiling the Structural Chemistry of Plant Biomineralisation1Hierarchy design of zeolite mesocrystals20Atomic-scale insights into topotactic transformations in an extra-large-pore zeolite using time-resolved 3D electron diffraction23Multiscale Structural Analysis of Aggregation-Induced Emission Nanocrystals by Combining Electron and Confocal Microscopy3AutoLEI: An XDS-based Graphical User Interface for Automated Real-time and Offline Batch 3D ED/MicroED Data Processing2Atomic-Level Electron Crystallography of Metal–Organic Frameworks Via Resin-Peeled Ultramicrotomy2Accelerated discovery of stable, extra-large-pore nano zeolites with micro-electron diffraction29Discovery of Stable Extra-large Pore Zeolites Based on Rational Design of Structure-directing Agents30Quantification of enantiomorphs in chiral crystalline powders through three-dimensional electron diffraction5Serial Chemical Crystallography for Autonomous Quantitative Phase Analysis in an Electron Microscope0Spatially Aware Diffraction Mapping Enables Fully Autonomous MicroED4Agentic material science5Probing Site Occupancy of Rare-Earth Elements in Zoned Apatite via Three-Dimensional Electron Diffraction Coupled with Focused Ion Beam Sampling0Sub-Ångström Three-Dimensional Electron Diffraction Reveals Crystal Structures and Phase Transformations in Liquids43DED as a robust technique for decoding phyllosilicate frameworks0Teaching powder diffraction and crystal structure analysis using Rietica: an educational approach0Solvent-Directed Phase Control in Disulfide-Linked Metal–Organic Frameworks Revealed by Microcrystal Electron Diffraction0

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  1. SCM-25: A Zeolite with Ordered Meso-cavities Interconnected by 12 × 12 × 10-Ring Channels Determined by 3D Electron Diffraction

    Inorganic Chemistry · 2022-01-25

    Yi Luo, Wenhua Fu, Bin Wang, Zhiqing Yuan, Junliang Sun, Xiaodong Zou, Weimin Yang

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  2. 3D electron diffraction for structure determination of small‐molecule nanocrystals: A possible breakthrough for the pharmaceutical industry

    Wiley Interdisciplinary Reviews Nanomedicine and Nanobiotechnology · 2022-05-20

    Iryna Andrusenko, Mauro Gemmi

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  3. Electron crystallography and dedicated electron-diffraction instrumentation

    Acta Crystallographica Section E Crystallographic Communications · 2023-04-11

    P. Simoncic, Eva Romeijn, Eric R. Hovestreydt, Gunther Steinfeld, Gustavo Santiso-Quiñones, Johannes Merkelbach

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  4. Autonomous MicroED data collection enables compositional analysis

    Research Square · 2023-05-18

    Johan Unge, Jieye Lin, Sara J. Weaver, Ampon Sae Her, Tamir Gonen

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  5. Phase identification and discovery of hidden crystal forms in a polycrystalline pharmaceutical sample using high-throughput 3D electron diffraction

    ChemRxiv · 2023-05-19

    Molly Lightowler, Shuting Li, Xiao Ou, Jungyoun Cho, Ao Li, Gerhard Höfer, Jiaoyan Xu, Taimin Yang, Xiaodong Zou, Ming Lü, Hongyi Xu

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  6. Making the Most of 3D Electron Diffraction: Best Practices to Handle a New Tool

    Symmetry · 2023-08-08

    Khai‐Nghi Truong, Shô Itô, Jakub M. Wojciechowski, Christian R. Göb, Christian J. Schürmann, Akihito Yamano, Mark Del Campo, Eiji Okunishi, Yoshitaka Aoyama, Tomohiro Mihira, Naoki Hosogi, Jordi Benet‐Buchholz, Eduardo C. Escudero‐Adán, Fraser White, Joseph D. Ferrara, Robert Bücker

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  7. Visualization of topotactic structural transformations of zeolites using 3D electron diffraction

    ChemRxiv · 2023-08-31

    Yi Luo, Hao Xu, Yue Han, Wen Tong, Meichen Jiao, Naihong Wang, Jingang Jiang, Xiaodong Zou, Peng Wu

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  8. Covalent-coordination driven hierarchical assembly of tubular frameworks

    Research Square · 2023-10-20

    Cheng‐Yong Su, Hai‐Sen Xu, Yi Luo, Lin Liang, Runlai Li, Hongfei Wang, Ting Chen, Wen-Na Jiao, Si Yu Huang, Wei-De Zhu, Mathias Nero, Fangzheng Chen, Qiang Gao, Xing Li, Mei Ling Pan, Tom Willhammar, Kian Ping Loh

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  9. STEM SerialED: achieving high-resolution data for ab initio structure determination of beam-sensitive nanocrystalline materials

    IUCrJ · 2023-11-09

    Pascal Hogan-Lamarre, Yi Luo, Robert Bücker, R. J. Dwayne Miller, Xiaodong Zou

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  10. Advances and applications of microcrystal electron diffraction (MicroED)

    Current Opinion in Structural Biology · 2023-12-11

    Alison Haymaker, Brent L. Nannenga

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  11. High-Throughput Identification of Crystalline Natural Products from Crude Extracts Enabled by Microarray Technology and microED

    ACS Central Science · 2023-12-20

    David A. Delgadillo, Jessica E. Burch, Lee Joon Kim, Lygia S. de Moraes, Kanji Niwa, Jason Williams, Melody J. Tang, Vincent Lavallo, Bhuwan Khatri Chhetri, Christopher G. Jones, Isabel Hernandez Rodriguez, Joshua Alexander Signore, Lewis Marquez, Riya Bhanushali, Madison Greene, 우선민, Julia Kubanek, Cassandra Leah Quave, Yi Tang, Hosea M. Nelson

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  12. Compositional Analysis of Complex Mixtures using Automatic MicroED Data Collection

    Advanced Science · 2024-04-22

    Johan Unge, Jieye Lin, Sara J. Weaver, Ampon Sae Her, Tamir Gonen

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  13. High-ion-conductive zeolite X with built-in < 1 nm 3D pores achieving superior thermoelectric performance

    Nano Research · 2024-06-01

    Guilong Pan, Fanshi Wu, Jiale Zhang, Wanjia Zhang, Jiao Li, Xiaoqing Lu, Xiyang Wang, Zhan Shi, Bao‐Hua Xu, Yue Lou

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  14. Current trends and advancements in crystallization and single-crystal structural analysis of small molecules

    Coordination Chemistry Reviews · 2024-06-25

    Yuntian Xiao, Chuanhua Wu, Ling Yi Zhou, Patrick Commins, Liang Li, Pancě Naumov, Qiuxiang Yin

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  15. Hierarchical assembly of tubular frameworks driven by covalent and coordinate bonding

    Nature Synthesis · 2024-08-26

    Hai‐Sen Xu, Yi Luo, Runlai Li, Wen-Na Jiao, Si Huang, Wei-De Zhu, Hongfei Wang, Ting Chen, Mathias Nero, Fangzheng Chen, Qiang Gao, Xing Li, Mei Ling Pan, Tom Willhammar, Kian Ping Loh, Cheng‐Yong Su

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  16. Three-Dimensional Electron Diffraction: A Revolutionary Technique for Structure Analysis of Nano-sized Minerals

    Acta Mineralogica Sinica · 2024-09-30

    Yiping YANG, Xiaoju LIN, Haiyang Xian, Shengdong CHEN, Yuhuan YUAN, Jiaxin XI, Jianxi ZHU, Hongping HE

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  17. MicroED: Unveiling the Structural Chemistry of Plant Biomineralisation

    Molecules · 2024-10-17

    Damian Trzybiński, Marcin Ziemniak, Barbara Olech, Szymon Marcin Sutula, Tomasz K. Goral, Olga Bemowska-Kałabun, Krzysztof Brzost, Małgorzata H. Wierzbicka, Krzysztof Woźniak

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  18. Hierarchy design of zeolite mesocrystals

    Chemical Engineering Journal · 2025-01-05

    Bo‐Jun Zeng, Si‐Ming Wu, Markus Antonietti, Christoph Janiak, Osamu Terasaki, Xiaoyu Yang

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  19. Atomic-scale insights into topotactic transformations in an extra-large-pore zeolite using time-resolved 3D electron diffraction

    Nature Synthesis · 2025-01-10

    Yi Luo, Hao Xu, Yue Han, Wen Tong, Meichen Jiao, Naihong Wang, Jingang Jiang, Wende Hu, Chuanming Wang, Xiaodong Zou, Peng Wu

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  20. Multiscale Structural Analysis of Aggregation-Induced Emission Nanocrystals by Combining Electron and Confocal Microscopy

    Journal of the American Chemical Society · 2025-04-08

    Shitao Wu, Jianyu Zhang, Jianyu Zhang, Jing Zhang, Jing Zhang, Yanhang Ma

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  21. AutoLEI: An XDS-based Graphical User Interface for Automated Real-time and Offline Batch 3D ED/MicroED Data Processing

    bioRxiv (Cold Spring Harbor Laboratory) · 2025-04-12

    Lei Wang, Yinlin Chen, Emma Rose Scaletti, Pål Stenmark, Gerhard Höfer, Hongyi Xu, Xiaodong Zou

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  22. Atomic-Level Electron Crystallography of Metal–Organic Frameworks Via Resin-Peeled Ultramicrotomy

    Journal of the American Chemical Society · 2025-05-12

    Zhiye Zhong, Enci Zhang, Pu Yan, Huaidong Jiang, Yanhang Ma

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  23. Accelerated discovery of stable, extra-large-pore nano zeolites with micro-electron diffraction

    Science · 2025-06-26

    Chao Ma, Zhenghan Zhang, Mengdi Zhang, Xudong Tian, Cong Lin, Lei Han, Guangchao Li, Tsz Woon Benedict Lo, Ka‐Fu Yung, Haitao Song, Wei Shin Lin, Miguel Angel Camblor, Le Xu, Jian Li

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  24. Discovery of Stable Extra-large Pore Zeolites Based on Rational Design of Structure-directing Agents

    Accounts of Chemical Research · 2025-07-25

    Fei‐Jian Chen, Jihong Yu

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  25. Quantification of enantiomorphs in chiral crystalline powders through three-dimensional electron diffraction

    Nature Chemistry · 2025-09-24

    Junyi Hu, Zhuoya Dong, Chaoyang Chu, Yanhang Ma

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  26. Serial Chemical Crystallography for Autonomous Quantitative Phase Analysis in an Electron Microscope

    Small Methods · 2025-10-20

    Taimin Yang, David Geoffrey Waterman, Zheting Chu, James Beilsten‐Edmands, Zhehao Huang, Xiaodong Zou

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  27. Spatially Aware Diffraction Mapping Enables Fully Autonomous MicroED

    Journal of the American Chemical Society · 2025-11-10

    Dmitry B. Eremin, Kunal Kumar Jha, David A. Delgadillo, Hongyu Zhang, Samuel H. Foxman, Samuel N. Johnson, Niko W. Vlahakis, Duilio Cascio, Vincent Lavallo, José A. Rodríguez, Hosea M. Nelson

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  28. Agentic material science

    Journal of Materials Informatics · 2026-01-30

    Chengbo Li, Nian Ran, Jianjun Liu

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  29. Probing Site Occupancy of Rare-Earth Elements in Zoned Apatite via Three-Dimensional Electron Diffraction Coupled with Focused Ion Beam Sampling

    ACS Earth and Space Chemistry · 2026-02-06

    Wenlin Yang, Haiyang Xian, Yiping Yang, Jianxi Zhu, Wenting Huang, Xianghui Zhang

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  30. Sub-Ångström Three-Dimensional Electron Diffraction Reveals Crystal Structures and Phase Transformations in Liquids

    Journal of the American Chemical Society · 2026-04-17

    Huiqiu Wang, Joakim Lajer, Edward T. Broadhurst, Tayyaba Malik, Murat Nulati Yesibolati, Emil C S Jensen, Kristian Speranza Mølhave, Hongyi Xu, Xiaodong Zou

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  31. 3DED as a robust technique for decoding phyllosilicate frameworks

    Applied Clay Science · 2026-04-25

    Yuhuan Yuan, Yiping Yang, Jiaxin Xi, Ke Wen, Haiyang Xian, Jianxi Zhu, Hongping He, Huifang Xu

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  32. Teaching powder diffraction and crystal structure analysis using Rietica: an educational approach

    European Journal of Physics · 2026-06-01

    Vicran Zharvan, Nurul Fachrunnisa, Eko Hadi Sujiono

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  33. Solvent-Directed Phase Control in Disulfide-Linked Metal–Organic Frameworks Revealed by Microcrystal Electron Diffraction

    Precision Chemistry · 2026-07-10

    Patrick F. Strobel, Lucas Laventure, Priyanshu Chandra, Mark Del Campo, Pierre Le Maguerès, Lauren Aheran, Jing Jin, Nathan J. Oldenhuis, David Punihaole, Aylin Aykanat

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