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RESEARCH PAPER · Advanced Materials · 2022

Tuning the C 1 /C 2 Selectivity of Electrochemical CO 2 Reduction on Cu–CeO 2 Nanorods by Oxidation State Control

Seungwon Hong, Hafiz Ghulam Abbas, Kyuseon Jang, Kshirodra Kumar Patra, Beomil Kim, Byeong-Uk Choi, Hakhyeon Song, Kug‐Seung Lee, Pyuck‐Pa Choi, Stefan Ringe, Jihun Oh

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Tuning the C 1 /C 2 Selectivity of Electrochemical CO 2 Reduction on Cu–CeO 2 Nanorods by Oxidation State ControlOriginalCO 2 electrolysis towards large scale operation: rational catalyst and electrolyte design for efficient flow-cell19Copper hydroxide/basic copper salt derived Cu 0 with a clear grain boundary for selective electrocatalytic CO 2 reduction to produce multicarbon products21Copper–barium-decorated carbon-nanotube composite for electrocatalytic CO 2 reduction to C2 products15Metal/metal-oxide interface catalysed thermal and electrochemical CO 2 conversion: a perspective from DFT-based studies16Spatially and temporally understanding dynamic solid–electrolyte interfaces in carbon dioxide electroreduction142In Situ Carbon-Encapsulated Copper-Doped Cerium Oxide Derived from MOFs for Boosting CO 2 -to-CH 4 Electro-Conversion117CO 2 Conversion Toward Real‐World Applications: Electrocatalysis versus CO 2 Batteries63Electronic and Structural Engineering of Atomically Dispersed Isolated Single‐Atom and Alloy Architectures17Intermetallic Compound with CuNi Sites for Enhancing the Selectivity of Electrochemical CO2 Conversion10Sequential *CO management via controlling in situ reconstruction for efficient industrial-current-density CO 2 -to-C 2+ electroreduction39Bifunctional phosphate-modulated Cu2O/CeO2 redox heterojunction: A promising approach for proficient CO2 reduction32Molecular Engineering of Copper Phthalocyanine for CO2 Electroreduction to Methane16Rare‐earth Element‐based Electrocatalysts Designed for CO2 Electro‐reduction28Engineering highly selective CO 2 electroreduction in Cu-based perovskites through A-site cation manipulation10Enhancement of electrocatalytic CO 2 performance by different components of Cu-based bimetallic MOFs0Hydroxylation boosted low-overpotential CO 2 reduction to ethylene for a Cu/PTFE electrode4Progress in Cu-based electrocatalysts for electrochemical CO 2 reduction to C 2+ products26Stabilizing the oxidation state of catalysts for effective electrochemical carbon dioxide conversion105Strong effect-correlated electrochemical CO 2 reduction66Halide precursor reduction strategy to modulate bismuthene with high selectivity and wide potential window for electrochemical CO2 reduction7Structure-induced interfacial activation convoying the CO-relayed conversion of CO2 to dimethyl carbonate11Morphology Evolution of CuO Supported on CeO2 and Its Role in Electrochemical CO2 Reduction3Regulation of CuFeZn catalysts by K3PO4 and its effect on CO2 hydrogenation to C2+ alcohols16Electrochemical C-C coupling mediated by novel Sn-SnO2 supported Cu single atoms: The case of CO2 conversion to ethanol12Electron-rich Cu0-Cu2O heterogeneous interface constructed via controllable electrochemical reconstruction for a single CO2 deep-reduction product ethylene30Copper/Polyaniline Interfaces Confined CO2 Electroreduction for Selective Hydrocarbon Production13Cu single atoms mediated multiple active site reconfiguration to trigger Dual-pathway nonradical peroxymonosulfate activation process29Experimental and Theoretical Investigation of Interfacial Engineering in Fe 2 O 3 /NiFe 2 O 4 Heterostructures toward the Cycloaddition of CO 2 with Styrene Oxide13Strategies for Improving Product Selectivity in Electrocatalytic Carbon Dioxide Reduction Using Copper‐Based Catalysts31High Selectivity in CO2 Reduction to CO Using Metal-Decorated C3N4 Nanotubes6Self‐Reconstruction Induced Electronic Metal‐Support Interaction for Modulated Cu+ Sites on TiO2 Nanofibers in Electrocatalytic Nitrate Conversion24AuAg plasmonic nanoalloys with asymmetric charge distribution on CeO 2 nanorods for selective photocatalytic CO 2 ‐to‐CH 4 conversion32Metal–metal oxide hybrid catalysts for electrocatalytic CO2 reduction reaction9Experimental and Theoretical Insights into Single Atoms, Dual Atoms, and Sub‐Nanocluster Catalysts for Electrochemical CO 2 Reduction (CO 2 RR) to High‐Value Products107Surface modification of copper oxide nanosheets with CeO 2 for enhanced CO 2 reduction to C 2 H 46Rubidium- and Copper-Doped CeO2 Nanorods for the Oxidative Coupling of Anilines4Reaction Pathway Regulation for Gaseous and Liquid Products of Electrocatalytic CO2 Reduction under Adsorbate Interactions3Reaction Pathway Regulation for Gaseous and Liquid Products of Electrocatalytic CO2 Reduction under Adsorbate Interactions28Confinement Effect and Hydrogen Species Modulation toward Enhanced Electrochemical CO 2 Reduction to Ethanol9Identification of catalyst optimization trends for electrocatalytic CO (2) reduction to ethylene2Interfacial synergy between Cu nanoclusters and oxygen vacancies on CeO 2 for enhanced selective photoreduction of CO 2 to C 2 H 48Heteroarchitectural Gas Diffusion Layer Promotes CO 2 Reduction Coupled with Biomass Oxidation at Ampere‐Level Current Density0Heteroarchitectural Gas Diffusion Layer Promotes CO 2 Reduction Coupled with Biomass Oxidation at Ampere‐Level Current Density10Interfacial Metal Oxides Stabilize Cu Oxidation States for Electrocatalytical CO2 Reduction2Boosting CO2 Hydrogenation by Synergistic Incorporation of Pure Silica Silicalite‐1 Zeolite and CeO2 into Cu Catalysts19Boosting CO2 Hydrogenation by Synergistic Incorporation of Pure Silica Silicalite‐1 Zeolite and CeO2 into Cu Catalysts4Switching Methane Selectivity in Carbon Dioxide Electroreduction via Confining Copper(I) Oxide Nanocubes by Polyimine Shells9Degradation Behavior of CeO2-Based Nanoparticles as Oxygen Carriers for the Chemical Looping Process6Enhancing C-C Coupling in CO2 Electroreduction by Engineering Pore Size of Porous Carbon-Supported Cu Catalysts37Manipulating hydrogenation pathways enables economically viable electrocatalytic aldehyde-to-alcohol valorization73Progress in Cu‐Based Catalyst Design for Sustained Electrocatalytic CO 2 to C 2+ Conversion33Stabilizing Oxidation State of Cu via Ce Doping into La 2 CuO 4 for Enhanced Electroreduction of CO 2 to Multicarbon Products12Improved Surface Reaction Kinetics in Red Phosphorus by Oxidation State for Efficient CO2 Photoreduction1Atomically dispersed cerium on copper tailors interfacial water structure for efficient CO-to-acetate electroreduction38Sb-Doped CeO2 Nanospheres for Selective CO2 Electroreduction to Ethanol through Dynamic Redox Cycling of Surface Sb and Ce Sites1Cu‐Based Tandem Architectures for CO2 Electrolysis to Multicarbon Products47Engineering Unsaturated Cu1–O3 Coordination to Boost Oxygen Species Activation for Low-Temperature Catalysis in CO Oxidation6The Chemical Nature of the Oxide Directs the Stability and Reactivity of Copper|Oxide Interfaces in the Electrochemical CO2 Reduction Reaction3Atomic Size Misfit for Electrocatalytic Small Molecule Activation16Selective and Energy Efficient Electrocatalytic CO 2 ‐to‐Ethanol Conversion through Anion Modulation42Selective and Energy Efficient Electrocatalytic CO 2 ‐to‐Ethanol Conversion through Anion Modulation4Dynamic valence engineering of CuOx catalysts for selective and stable CO2 electroreduction to ethylene and ethanol12Ce Single Atom‐Engineered Amorphous/Crystalline Nanosheets for Enhanced Alkaline Water Electrolysis42Cavity-confined Au@Cu2O yolk-shell nanoreactors enable switchable CH4/C2H4 selectivity41Stabilization of oxidized Cu species via CeO x nano-islands for enhanced CO2 reduction to C2+ products29Molecular Engineering of Catalyst–Electrolyte Interfaces With Hydrophobic and CO 2 ‐Capturing Cucurbit[6]uril for Enhanced CO 2 Electroreduction5Model thiophene-decorated nickel porphyrins for tandem CO2 reduction18Understanding Electrochemical CO 2 Reduction Selectivity of Cu Binary Alloys from Electronic Structure Descriptors42Bicarbonate‐Stabilized Cu 2 O/Cu Heterointerfaces Enable Efficient Ethylene Electrosynthesis From Carbon Capture Solutions2Cu─O─Al Interfacial Engineering on Cu Nanowires for Durable CO 2 Electroreduction Into Multi‐Carbon Products1Modulating Electrochemical CO 2 Reduction Pathways via Interfacial Electric Field3Dynamic Surface Reconstruction in Machine-Learning-Predicted Cu 3 MoP Governs Selective CO Electroreduction to C 2 + Products0Facet-Mediated Interfacial Zn–O v –Ce Sites for Enhanced CO 2 Electroreduction3From Electronic Structure to Catalytic Function: Rare Earth–Driven Strategies for CO 2 Electroreduction3Reconstructed Copper Compound by Cerium Leaching for Enhanced Electrochemical CO 2 ‐to‐Ethylene Conversion0Interfacial water dynamics on an inverse Cu–CeO2 catalyst for enhanced electrochemical ammonia production7Highly Selective CO 2 Electroreduction to Ethylene on Stable Cu 0 /Cu + Interfaces by Local Microenvironment Modulation3Differential Chloride Affinity Over Amorphous‐Crystalline Interfaces Drives Asymmetric C─C Coupling for Neutral CO 2 Electroreduction to Ethanol2Deciphering Intricacies in Directional CO 2 Conversion From Electrolysis to CO 2 Batteries1Wavelength-Tailoring Copper Oxidation States for Tunable Photoelectrochemical Syngas Generation5Cu‐Based Catalysts Design Toward Electrochemical CO 2 Reduction to Valuable Multi‐Carbons Products3Peaks and pitfalls of electrocatalytic CO2 reduction descriptor models7Dual regulation of geometry and water activation over coherent interface-rich inverse CeO2/CuO catalysts enabling highly selective CO2 electroreduction from C2H4 to CH42Dimensionality–Driven Electronic Modulation at Metal–Perovskite Interfaces for Electrochemical CO 2 Reduction0Interfacial Electric Field Engineering of High‐Entropy Heterostructures Triggering Self‐Limiting Reconstruction for Industrial‐Scale Electrocatalysis0

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  2. Copper hydroxide/basic copper salt derived Cu 0 with a clear grain boundary for selective electrocatalytic CO 2 reduction to produce multicarbon products

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  4. Metal/metal-oxide interface catalysed thermal and electrochemical CO 2 conversion: a perspective from DFT-based studies

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  6. In Situ Carbon-Encapsulated Copper-Doped Cerium Oxide Derived from MOFs for Boosting CO 2 -to-CH 4 Electro-Conversion

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  7. CO 2 Conversion Toward Real‐World Applications: Electrocatalysis versus CO 2 Batteries

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  19. Strong effect-correlated electrochemical CO 2 reduction

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  20. Halide precursor reduction strategy to modulate bismuthene with high selectivity and wide potential window for electrochemical CO2 reduction

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