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RESEARCH PAPER · Angewandte Chemie International Edition · 2022

Topochemical Synthesis of Ca3CrN3H Involving a Rotational Structural Transformation for Catalytic Ammonia Synthesis

Yu Cao, Maria A. Kirsanova, Masayuki Ochi, Walid Al Maksoud, Tong Zhu, Rohit Kumar Rai, Shenghan Gao, Tatsuya Tsumori, Shintaro Kobayashi, Shogo Kawaguchi, Edy Abou‐Hamad, Kazuhiko Kuroki, Cédric Tassel, Artem M. Abakumov, Yoji Kobayashi, Hiroshi Kageyama

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Topochemical Synthesis of Ca3CrN3H Involving a Rotational Structural Transformation for Catalytic Ammonia SynthesisOriginalElectronic Structure Manipulation of the Mott Insulator RuCl3 via Single‐Crystal to Single‐Crystal Topotactic Transformation14Electronic Structure Manipulation of the Mott Insulator RuCl3 via Single‐Crystal to Single‐Crystal Topotactic Transformation1Ammonia Synthesis via an Associative Mechanism on Alkaline Earth Metal Sites of Ca3CrN3H13Pressure-Induced Anion Order–Disorder Transition in Layered Perovskite Sr2LiHOCl28Photochemical Acceleration of Ammonia Production by Pt1-Ptn-TiN Reduction and N2 Activation65Ammonia Synthesis on Ternary LaSi‐based Electrides: Tuning the Catalytic Mechanism by the Third Metal11Magnetic quasi-atomic electrons driven reversible structural and magnetic transitions between electride and its hydrides16Revisiting group 4–7 transition metals for heterogeneous ammonia synthesis11Recent progress of thermocatalytic ammonia synthesis via an associative mechanism15Cr5.7Si2.3P8N24—A Chromium(+IV) Nitridosilicate Phosphate with Amphibole‐Type Structure0Cr5.7Si2.3P8N24—A Chromium(+IV) Nitridosilicate Phosphate with Amphibole‐Type Structure0Promoting Effect of Bulk Cs+ over Cs0.68Ti1.83O4 for Ammonia Synthesis8Introduction of Synchrotron X-ray Powder Diffraction System and Demonstration of In-Situ Observation System0Topochemical Synthesis and Formation Mechanism of Garnet Multimetal Fluorides2Configuration and Dynamics of Hydride Ions in the Nitride-Hydride Catalyst Ca3CrN3H3Insight into the role of tunable nitrogen vacancies in transition metal nitrides for ammonia synthesis6Progress of metal hydrides, amides and imides for ammonia synthesis and decomposition6Spin Chains with Highly Quantum Character through Strong Covalency in Ca3CrN33Polymorphic YTiGe Intermetallic Electride Created by Hydrogenation and Dehydrogenation1Anion-Controlled Inorganic Materials as Catalysts for Small-Molecule Conversion Reactions8Oxyhydride Synthesis through Facile Water Dissociation on the Electride Intermetallic LaScSi2Design principles of metastable nanomaterials: A comprehensive review0Hydrides for Dinitrogen Conversion7Ultrastable One‐Dimensional Ti 2 S Electride Support for an Efficient and Durable Bifunctional Electrocatalyst2Simultaneous Formation of Arsenic Nitride Chalcogenides As 3 NS 3 and As 3 NSe 3 and Arsenic–Chalcogen Zintl Anions by Ammonothermal Reactions0Size-driven enhancement of coercivity in tetragonal FeCo nanocrystals2Atomically Dispersed Mn Synergized With LiBaH 3 on MgO Enables Efficient Ammonia Synthesis via an H − Assisted N 2 Dissociation Mechanism1Reactive hydrogen in KH or KOH for catalytic NH3 synthesis1Electride Formation of (Ca 1– x Sr x ) 3 CrN 3 Induced by Negative Chemical Pressure0Flexible hybridization of interstitial electrons with a transition metal center0Pressure-Induced Phase Transitions in Cr-Based Nitride Electrides0

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  1. Electronic Structure Manipulation of the Mott Insulator RuCl3 via Single‐Crystal to Single‐Crystal Topotactic Transformation

    Angewandte Chemie International Edition · 2023-03-02

    Weiqun Lu, Hyungseok Lee, Joonil Cha, Jian Zhang, In Jae Chung

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  2. Electronic Structure Manipulation of the Mott Insulator RuCl3 via Single‐Crystal to Single‐Crystal Topotactic Transformation

    Angewandte Chemie · 2023-03-02

    Weiqun Lu, Hyungseok Lee, Joonil Cha, Jian Zhang, In Jae Chung

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  3. Ammonia Synthesis via an Associative Mechanism on Alkaline Earth Metal Sites of Ca3CrN3H

    ChemSusChem · 2023-04-28

    Yu Cao, Ekaterina Toshcheva, Walid Al Maksoud, Rafia Ahmad, Tatsuya Tsumori, Rohit Kumar Rai, Ya Nan Tang, Luigi Cavallo, Hiroshi Kageyama, Yoji Kobayashi

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  4. Pressure-Induced Anion Order–Disorder Transition in Layered Perovskite Sr2LiHOCl2

    Inorganic Chemistry · 2023-05-09

    Zefeng Wei, Hiroki Ubukata, Chengchao Zhong, Cédric Tassel, Hiroshi Kageyama

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  5. Photochemical Acceleration of Ammonia Production by Pt1-Ptn-TiN Reduction and N2 Activation

    Journal of the American Chemical Society · 2023-06-06

    Chengliang Mao, Jiaxian Wang, Yunjie Zou, Yanbiao Shi, Camilo Javier Viasus, Joel Y. Y. Loh, Meikun Xia, Shufang Ji, Meiqi Li, Huan Shang, Mireille Ghoussoub, Yangfan Xu, Jessica Ye, Zhilin Li, Nazir P. Kherani, Lirong Zheng, Yanjiang Liu, Lizhi Zhang, Geoffrey A. Ozin

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  6. Ammonia Synthesis on Ternary LaSi‐based Electrides: Tuning the Catalytic Mechanism by the Third Metal

    ChemSusChem · 2023-08-16

    Hongchen Li, Yutong Gong, Hongliang Yang, Xiao Ming Yang, Ke Li, Junjie Wang, Hideo Hosono

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  7. Magnetic quasi-atomic electrons driven reversible structural and magnetic transitions between electride and its hydrides

    Nature Communications · 2023-09-06

    Seung Yong Lee, Dong Cheol Lim, Md Salman Khan, Jeong Yun Hwang, Hyungsub Kim, Kyu Hyoung Lee, Sung Wng Kim

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  8. Revisiting group 4–7 transition metals for heterogeneous ammonia synthesis

    EES Catalysis · 2024-01-01

    Wenbo Gao, Yawei Wang, Qianru Wang, Zhaolong Sun, Jianping Guo, Ping Chen

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  9. Recent progress of thermocatalytic ammonia synthesis via an associative mechanism

    Fundamental Research · 2024-01-22

    Yangyu Zhang, Jiaxin Li, Yanliang Zhou, Chak‐Tong Au, Xiuyun Wang, Lilong Jiang

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  10. Cr5.7Si2.3P8N24—A Chromium(+IV) Nitridosilicate Phosphate with Amphibole‐Type Structure

    Angewandte Chemie · 2024-02-15

    Monika M. Pointner, Katherine R. Fisher, Martin L. Weidemann, Florian Wolf, Jonathan Paul Wright, Eleanor Lawrence Bright, Carlotta Giacobbe, Oliver Oeckler, Wolfgang Schnick

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  11. Cr5.7Si2.3P8N24—A Chromium(+IV) Nitridosilicate Phosphate with Amphibole‐Type Structure

    Angewandte Chemie International Edition · 2024-02-15

    Monika M. Pointner, Katherine R. Fisher, Martin L. Weidemann, Florian Wolf, Jonathan Paul Wright, Eleanor Lawrence Bright, Carlotta Giacobbe, Oliver Oeckler, Wolfgang Schnick

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  12. Promoting Effect of Bulk Cs+ over Cs0.68Ti1.83O4 for Ammonia Synthesis

    The Journal of Physical Chemistry C · 2024-06-10

    Fei‐Yang Tian, Jinkun Li, Fanyi Kong, Chunchen Zhang, Jiuhui Han, Ya Nan Tang, Xiangyu Xiao, Wenqian Chen, Liang Tang

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  13. Introduction of Synchrotron X-ray Powder Diffraction System and Demonstration of In-Situ Observation System

    Materia Japan · 2024-06-30

    Shogo Kawaguchi, Shintaro Kobayashi

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  14. Topochemical Synthesis and Formation Mechanism of Garnet Multimetal Fluorides

    ACS Materials Letters · 2024-10-31

    Keshav Kumar, Prabhat Thapliyal, Divya Bhutani, Rinya Rubu, Shubham Kumar Debadatta, Sheetal Jain, Premkumar Senguttuvan

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  15. Configuration and Dynamics of Hydride Ions in the Nitride-Hydride Catalyst Ca3CrN3H

    Chemistry of Materials · 2024-12-12

    Lucas Fine, Rasmus Lavén, Zefeng Wei, Tatsuya Tsumori, Hiroshi Kageyama, Ryoichi Kajimoto, Mónica Jiménez‐Ruiz, Michael Marek Koza, Maths Karlsson

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  16. Insight into the role of tunable nitrogen vacancies in transition metal nitrides for ammonia synthesis

    Nanoscale · 2025-01-01

    Shiqi Yu, Ziyu Mei, Luyuan Wang, Yuping Ren, Wu Wei, Mao Liu, Tianyi Wang, Chuangwei Liu

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  17. Progress of metal hydrides, amides and imides for ammonia synthesis and decomposition

    The Innovation Energy · 2025-01-01

    Sheng Feng, Wenbo Gao, Jianping Guo, Ping Chen

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  18. Spin Chains with Highly Quantum Character through Strong Covalency in Ca3CrN3

    Journal of the American Chemical Society · 2025-01-21

    Linus Kautzsch, Alexandru Bogdan Georgescu, Lin‐Ding Yuan, Keith M. Taddei, Aiden Reilly, Ram Seshadri, James M. Rondinelli, Stephen D. Wilson

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  19. Polymorphic YTiGe Intermetallic Electride Created by Hydrogenation and Dehydrogenation

    Chemistry of Materials · 2025-02-03

    Shuhao Chen, Siyuan Ren, Md Salman Khan, Dong Cheol Lim, Nahyun Lee, Hyungsub Kim, T. Thuy Hoang, Junhyeok Bang, Sung Wng Kim

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  20. Anion-Controlled Inorganic Materials as Catalysts for Small-Molecule Conversion Reactions

    ACS Applied Materials & Interfaces · 2025-04-17

    Megumi Okazaki, Yuta Tsuji, Daisuke Tanaka, Hiroshi Kageyama, Kazuhiko Maeda

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  21. Oxyhydride Synthesis through Facile Water Dissociation on the Electride Intermetallic LaScSi

    Journal of the American Chemical Society · 2025-06-13

    Khaled Alabd, Etienne Gaudin, Antoine Villesuzanne, Baptiste Vignolle, Étienne Durand, Nathalie Daro, Emmanuelle Suard, C. Ritter, Sophie Tencé

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  22. Design principles of metastable nanomaterials: A comprehensive review

    Progress in Natural Science Materials International · 2025-07-23

    Jincan Li, YiJing Zhang, YiJing Zhang, Huiyu Duan, Chen Quanzhan, Changyun Chen, Cheng Zhang, Changyun Chen, Kuaibing Wang

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  23. Hydrides for Dinitrogen Conversion

    ACS Catalysis · 2025-08-11

    Jianping Guo, Yongli Cai, Wenbo Gao, Ping Chen

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  24. Ultrastable One‐Dimensional Ti 2 S Electride Support for an Efficient and Durable Bifunctional Electrocatalyst

    Carbon Energy · 2025-09-11

    Siyuan Ren, Kyoung Ryeol Park, Binod Regmi, Wooseon Choi, Yun Seong Cho, Seon Je Kim, Seon Je Kim, Heechae Choi, Young‐Min Kim, Joohoon Kang, HyukSu Han, Seong‐Gon Kim, Seong‐Gon Kim, Sung Wng Kim, Sung Wng Kim

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  25. Simultaneous Formation of Arsenic Nitride Chalcogenides As 3 NS 3 and As 3 NSe 3 and Arsenic–Chalcogen Zintl Anions by Ammonothermal Reactions

    Zeitschrift für anorganische und allgemeine Chemie · 2026-01-22

    Frederik Hermann, Jörg Daniels, Gregor Schnakenburg, Thomas Bredow, Johannes Beck

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  26. Size-driven enhancement of coercivity in tetragonal FeCo nanocrystals

    Journal of Alloys and Compounds · 2026-04-01

    Xiaolei Shang, Jingzhen Zhou, Ruiqi Huang, Xiaoling Men, Qifeng Kuang, Desheng Pan, Da Li, Zhidong Zhang

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  27. Atomically Dispersed Mn Synergized With LiBaH 3 on MgO Enables Efficient Ammonia Synthesis via an H − Assisted N 2 Dissociation Mechanism

    Angewandte Chemie International Edition · 2026-05-15

    Yanbo Deng, Yaoqi Huang, Yongcheng Jin, Yue Wang, Runze Wang, Sheng Feng, Yongli Cai, Yeqin Guan, Qianru Wang, Xilun Zhang, Fei Chang, Shaojun Yuan, Gao W, Jianping Guo, P Chen

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  28. Reactive hydrogen in KH or KOH for catalytic NH3 synthesis

    The Innovation · 2026-05-29

    Peikun Wang, Wenbo Gao, Yanbo Deng, Fei Chang, Qi Wang, Sheng Feng, Jianping Guo, Ping Chen

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  29. Electride Formation of (Ca 1– x Sr x ) 3 CrN 3 Induced by Negative Chemical Pressure

    Angewandte Chemie International Edition · 2026-07-21

    Tatsuya Tsumori, Yu Cao, Daichi Kato, Suguru Yoshida, Yao Yuan, Hiroki Ubukata, Kantaro Murayama, Yuki Sasahara, Hiroshi Kageyama

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  30. Flexible hybridization of interstitial electrons with a transition metal center

    Cell Reports Physical Science · 2026-07-22

    Raza ullah shah Bacha, Nikita A. Kudriavykh, Yoji Kobayashi

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  31. Pressure-Induced Phase Transitions in Cr-Based Nitride Electrides

    Inorganic Chemistry · 2026-09-28

    Jacob A. Lafferty, Dawson M. Smith, Danna E. Freedman, Danilo Puggioni, James M. Rondinelli

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