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RESEARCH PAPER · Nature Reviews Materials · 2022

Nanostructuring versus microstructuring in battery electrodes

Rishabh Jain, Aniruddha S. Lakhnot, Kevin Bhimani, Shyam Sharma, Varad Mahajani, Reena A. Panchal, Mithil Kamble, Fudong Han, Chunsheng Wang, Nikhil A. Koratkar

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Nanostructuring versus microstructuring in battery electrodesOriginalEmerging two-dimensional nanostructured manganese-based materials for electrochemical energy storage: recent advances, mechanisms, challenges, and prospects105Li/Na Ion Storage Performance of a FeOF Nano Rod with Controllable Morphology0Inner wrinkled mesoporous hollow carbon spheres with nanopillars connected to double shells for excellent potassium storage14High specific energy and power sodium-based dual-ion supercabatteries by pseudocapacitive Ni-Zn-Mn ternary perovskite fluorides@reduced graphene oxides anodes with conversion-alloying-intercalation triple mechanisms36NiMn-based metal-organic framework with optimized eg orbital occupancy as efficient bifunctional electrocatalyst for lithium-oxygen batteries67Coal tar pitch-based carbon composited Sb2Se3 microrod anode toward superior sodium storage performance20Solid electrolyte interphase layer induced electrochemical behavior diversity of aluminum foil anode for lithium ion batteries26Practical assessment of the energy density of potassium-ion batteries36MnS nanoparticles embedded uniformly in sulfur/nitrogen-doped porous carbon spheres enhancing lithium-storage performance9Intercalation Hosts for Multivalent‐Ion Batteries25Al-based materials for advanced lithium rechargeable batteries: recent progress and prospects10Defect engineering of two-dimensional materials for advanced energy conversion and storage417Elucidating the electrochemical reaction mechanism of lithium-rich antiperovskite cathodes for lithium-ion batteries as exemplified by (Li 2 Fe)SeO9EXPLORING THERMAL TRANSPORT IN ELECTROCHEMICAL ENERGY STORAGE SYSTEMS UTILIZING TWO-DIMENSIONAL MATERIALS: PROSPECTS AND HURDLES2Scalable engineering of hierarchical layered micro-sized silicon/graphene hybrids via direct foaming for lithium storage15Two-dimensional nitrogen and phosphorus co-doped mesoporous carbon-graphene nanosheets anode for high-performance potassium-ion capacitor18Electrochemical Reactivation of Dead Li 2 S for Li−S Batteries in Non‐Solvating Electrolytes64Electrochemical Reactivation of Dead Li2S for Li−S Batteries in Non‐Solvating Electrolytes1Lithium-rich antiperovskite (Li 2 Fe)SeO: A high-performance cathode material for lithium-ion batteries13Three-dimensional structure S-SnS2/NSG with sulfur vacancies for high-performance lithium-ion batteries24Electrochemically Induced Crystalline‐to‐Amorphous Transition of Dinuclear Polyoxovanadate for High‐Rate Lithium‐Ion Batteries19On-site conversion reaction enables ion-conducting surface on red phosphorus/carbon anode for durable and fast sodium-ion batteries34Composite cathode for all-solid-state lithium batteries: Progress and perspective65High-rate and excellent-cycle performance Li4Ti5O12 electrodes with 3D porous copper foils as current collectors fabricated using a femtosecond laser processing strategy25Controlled Isotropic Canalization of Microsized Silicon Enabling Stable High‐Rate and High‐Loading Lithium Storage57Fast-charging cathode materials for lithium & sodium ion batteries272Pyramid-Patterned Germanium Composite Film Anode for Rechargeable Lithium-Ion Batteries Prepared Using a One-Step Physical Method6Monodisperse MoS2/Graphite Composite Anode Materials for Advanced Lithium Ion Batteries14Constructing a conductive and buffer network on microscale silicon-based anodes for high-performance lithium-ion batteries10Covalent Organic Frameworks (COFs)/MXenes Heterostructures for Electrochemical Energy Storage59Ion transport phenomena in electrode materials11Gradient-distributed NiCo2O4 nanorod electrode for redox flow batteries: Establishing the ordered reaction interface to meet the anisotropic mass transport57In Situ Raman Spectroscopy of Li+ and Na+ Storage in Anodic TiO2 Nanotubes: Implications for Battery Design18Heat‐Up Process: Road to Synthesizing Monodisperse Nanoparticles8Advanced Materials to Support Sustainable Power Infrastructure0Approaching Microsized Alloy Anodes via Solid Electrolyte Interphase Design for Advanced Rechargeable Batteries73Design of Gradient Ti Reconstituted Fe2O3 Anodes with Enhanced Lithium Affinity Modulated Electronic Structures: First-Principles Calculations and Experiment Verification5A Self‐Powered Body Motion Sensing Network Integrated with Multiple Triboelectric Fabrics for Biometric Gait Recognition and Auxiliary Rehabilitation Training190Polyimide-engineered sodium titanate anode for sodium storage with improved structure and interface stability6Designable air-stable and dendrite-free Li metal anode via the oligomer layer for in-situ gel polymer batteries5Coupling between cathode and anode in hybrid charge storage39Prelithiated, Multiscale Nickel Phosphate Octahydrate Platelets by a Tailored Nanoarchitectonics Approach3Covalent Coating of Micro‐Sized Silicon With Dynamically Bonded Graphene Layers Toward Stably Cycled Lithium Storage108Design, fabrication and assembly considerations for electronic systems made of fibre devices154Micro-sized porous bulk bismuth caged by carbon for fast charging and ultralong cycling in sodium-ion batteries29Operando Raman and DFT Analysis of (De)lithiation in Fast-Charging, Shear-Phase H-Nb2O528Radiation effects on lithium metal batteries18Polymers for flexible energy storage devices119High sulfur-doped microporous carbon for high-rate potassium ion storage: Interspace design and solvent effect19Toward Achieving High Areal Capacity in Silicon-Based Solid-State Battery Anodes: What Influences the Rate-Performance?84Review of regulating Zn2+ solvation structures in aqueous zinc-ion batteries40Better engineering layered vanadium oxides for aqueous zinc‐ion batteries: Going beyond widening the interlayer spacing67Rapid single pot synthesis of hierarchical Bi2WO6 microspheres/RGO nanocomposite and its application in energy storage: A supercritical water approach35A 3D Multilevel Heterostructure Containing 2D Vertically Aligned MoS2 Nanosheets and 1D Sandwich C-MoS2-C Nanotubes to Enhance the Storage of Li+ Ions4A Steric-Hindrance-Induced Weakly Solvating Electrolyte Boosting the Cycling Performance of a Micrometer-Sized Silicon Anode73Tight Binding and Dual Encapsulation Enabled Stable Thick Silicon/Carbon Anode with Ultrahigh Volumetric Capacity for Lithium Storage35Two Birds with One Stone: Micro/Nanostructured SiO x C y Composites for Stable Li‐Ion and Li Metal Anodes23Designing highly packed silicon anode slurries for high capacity and prolonged lifespan of lithium-ion batteries29Coordination-Assisted Construction of Ultra-Fine Metal Nanoparticle Composites for Stable Sodium-Ion Battery Anodes4Doping of group IVB elements for nickel-rich cobalt-free cathodes25Tunable 1D and 2D Polyacrylonitrile Nanosheet Superstructures23Structure–performance relationship of nanomaterials13A Multiscale, Dynamic Elucidation of Li Solubility in the Alloy and Metallic Plating Process23Recent advances on electrode/electrolyte interfacial modulation in rechargeable magnesium batteries2In-situ construction of a hybrid interfacial protective layer for highly stable Li metal anodes7Covalent Bond Hybrid Nanostructure of N-doped rGO and Ultrathin SnS2 with High Porosity for Lithium-Ion Batteries6Differentiating Cyclability and Kinetics of Na+ Ions in Surface-Functionalized and Nanostructured Graphite Using Electrochemical Impedance Spectroscopy8Bi-layer graphite felt as the positive electrode for zinc-bromine flow batteries: Achieving efficient redox reaction and stable mass transport21Cation-deficient perovskite Li0.35Nd0.55TiO3 as a high-performance anode for lithium-ion batteries15Recent advances in synthesis of metal-organic frameworks (MOFs)-derived metal oxides and its composites for electrochemical energy storage applications73Comprehensive Study of Lithium Diffusion in Si/C-Layer and Si/C3N4 Composites in a Faceted Crystalline Silicon Anode for Fast-Charging Lithium-Ion Batteries16Alkali‐Ion Batteries by Carbon Encapsulation of Liquid Metal Anode37A-site deficient perovskite lithium praseodymium titanate as a high-rate anode for lithium-ion batteries10Hybrid Metal‐Ion Capacitors Based on Carbon Nanospheres8Synthetic brochosomes: design, synthesis, and applications7Toward Practical Alloy Anode Based Solid State Batteries11Discovery of fast and stable proton storage in bulk hexagonal molybdenum oxide75Tailoring Three-Dimensional Cross-Linked Networks Based on Water-Soluble Polymeric Materials for Stable Silicon Anode22Quasi‐Solid‐State All‐V2O5 Battery4Frameworked Electrolytes: A Pathway Towards Solid Future of Batteries11Understanding How the Suppression of Insertion-Induced Phase Transitions Leads to Fast Charging in Nanoscale LixMoO29Active nanomaterials for Li-ion batteries and advanced nanomaterials for supercapacitors19Integrated technologies and novel nanostructured materials for energy storage2Kinetically controlled synthesis of low-strain disordered micro–nano high voltage spinel cathodes with exposed {111} facets22Manipulating non-equilibrium diffusion-controlled reaction toward reversible alloying reactions in alkali ion batteries5One-step chemical vapor deposition synthesis of Si NWs@C core/shell anodes without additional catalysts by the oxide-assisted growth mechanism for lithium-ion batteries17Possibilities and challenges of cathode materials for Zn-ion batteries17Strategies to enable microsized alloy anodes for high-energy and long-life alkali-ion batteries39Tuning lithium–yttrium chloride local structure through coordination control and mixing during synthesis8Unlocking the potential of open-tunnel oxides: DFT-guided design and machine learning-enhanced discovery for next-generation industry-scale battery technologies7Wadsley–Roth phase CoNb 11 O 29 as a high-performance anode for lithium-ion batteries11Dynamic Behavior of Spatially Confined Sn Clusters and Its Application in Highly Efficient Sodium Storage with High Initial Coulombic Efficiency19Application of Recycled Battery-Graphite Electrode Decorated with Polyglutamic Acid/Au Nanoparticles for Detection of Nalbuphine Drug Abuse1Plasma-Induced Defect Engineering in TiNb2O7 for Boosting Lithium-Ion Diffusion12Dual regulation of polysulfides redox kinetics and lithium deposition with ultrafine Co–Mo2C nanocrystals confined in 2D nitrogen-doped carbon sheets for Li–S batteries7High-Rate SiO Lithium-Ion Battery Anode Enabled by Rationally Interfacial Hybrid Encapsulation Engineering25Evaluating the Impact of Conjugation Break Spacer Incorporation in Poly(3,4-propylenedioxythiophene)-Based Cathode Binders for Lithium-Ion Batteries12Insights on advanced g‐C 3 N 4 in energy storage: Applications, challenges, and future79Micelle-directed self-assembly of single-crystal-like mesoporous stoichiometric oxides for high-performance lithium storage14Multiscale Micro‐Nano Hierarchical Porous Germanium with Self‐Adaptive Stress Dispersion for Highly Robust Lithium‐Ion Batteries Anode30MoS2-carbon based nanocomposites as anodes for lithium-ion batteries: A review56Synthesis of submicron-sized LiNi0.5Co0.2Mn0.3O2 cathode particles via reverse microemulsion method: Tailoring size, interfacial properties, and enhanced electrochemical performance for lithium-ion battery9Magnetic Force Dilatometry of Silicon-NMC622 Lithium-Ion Coin Cells: The Effects of Binder, Capacity Ratio, and Electrolyte Selection2Recent Progress in Improving Rate Performance of Cellulose-Derived Carbon Materials for Sodium-Ion Batteries102Interfacial carbon tailoring of porous SiOx/carbon nanotube hybrids towards high-rate lithium storage3Micron-Sized Cobalt Niobium Oxide with Multiscale Porous Sponge-Like Structure Boosting High-Rate and Long-Life Lithium Storage9Sea urchin-inspired VS4 morphology for superior electrochemical performance in high-energy batteries6Enhanced Fast‐Charging and Longevity in Sodium‐Ion Batteries through Nitrogen‐Doped Carbon Frameworks Encasing Flower‐Like Bismuth Microspheres130Reduced Volume Expansion of Micron‐Sized SiOx via Closed‐Nanopore Structure Constructed by Mg‐Induced Elemental Segregation43Reduced Volume Expansion of Micron‐Sized SiOx via Closed‐Nanopore Structure Constructed by Mg‐Induced Elemental Segregation4Addressing Irreversibility and Structural Distortion in WS2 Inorganic Fullerene-Like Nanoparticles: Effects of Voltage Cutoff Experiments in Beyond Li+-Ion Storage Applications3The impact of carbon material microstructure on li-ion storage behaviors of Si in Si/C anodes39Femtosecond laser fabrication of 3D vertically aligned micro-pore network on thick-film Li4Ti5O12 electrode for high-performance lithium storage25Facile Magnetite Coating for Stable High‐Voltage Cycling of Nickel‐Rich Cathodes in Conventional Liquid and All‐Solid‐State Lithium‐Ion Batteries3Advanced Micro/Nanostructure Silicon-Based Anode Materials for High-Energy Lithium-Ion Batteries: From Liquid- to Solid-State Batteries93Understanding and Enhancing Silicon Nanoparticle Distribution during Electrode Processing3Development of Si-Based Anodes for All-Solid-State Li-Ion Batteries9Materials for 3D Printed Metal and Metal‐Ion Batteries3All-Textile Piezoelectric Nanogenerator Based on 3D Knitted Fabric Electrode for Wearable Applications43Recent advances in pulsed electrochemical techniques: Synthesis of electrode materials and electrocatalytic reactions25Assembled MXene–Liquid Metal Cages on Silicon Microparticles as Self-Healing Battery Anodes26Metallic Sb‐stabilized porous silicon with stable SEI and high electron/ion conductivity boosting lithium‐ion storage performance22Enhanced lithium storage performance of MoS2/C3N4 composites based on the structure design by controlling the amount of C3N46Structural engineering of Sb‐based electrode materials to enhance advanced sodium‐ion batteries20Controllable Synthesis of Sub‐10 nm ZnS Nanograins Confined in Micro‐Size Carbon Skeleton for Aqueous Zn–S Batteries34Progress in modification of micron silicon-based anode materials for lithium-ion battery54Thermal vapor sulfurization modified micro-sized red phosphorus/activated carbon composite anode for sodium-ion batteries6Standalone Stretchable Biophysical Sensing System Based on Laser Direct Write of Patterned Porous Graphene/Co3O4 Nanocomposites16Construction of WSSe2/C anode with enlarged layer spacing for efficient Na+ storage by anion synergistic strategy6Precise characterization of thermal conductivity and interfacial thermal resistance of individual polymer microparticle3Hierarchical Nanoporous N-Doped Carbon for Enhanced Rate Performance of Lithium-Ion Battery Anodes10Mo2C-Co heterostructure with carbon nanosheets decorated carbon microtubules: Different means for high-performance lithium-sulfur batteries20Dynamic evolution of zinc directional deposition: Toward precise interface manipulation for reversible zinc metal anodes28Emerging paradigms in two-dimensional materials: Classification, synthesis, and the role of defects in electrocatalysis for water splitting and oxygen reduction reaction22C60 Fullerene-Reinforced Silicon Oxycarbide Composite Fiber Mats: Performance as Li-Ion Battery Electrodes10Rigid-flexible coupling multistage carbon composite materials based on hybrid crosslinking as anodes for ultra long-cycling lithium-ion batteries11Sustainable organic electrodes using black soldier fly-derived melanin for zinc-ion hybrid capacitors14Are Sulfide‐Based Solid‐State Electrolytes the Best Pair for Si Anodes in Li‐Ion Batteries?52Application of neutron transmutation technology to control the physical properties of nanoparticles at the atomic scale44State-of-the-Art Electric Vehicle Modeling: Architectures, Control, and Regulations19A voltage-decoupled Zn-Br2 flow battery for large-scale energy storage1The preparation of SnS2@NxC electrodes and its exceptional performance in energy storage usages4Boosting the potassium storage property of spongia-like copper phosphide anode via nano-in-micro construction3Graphite/Nanosilicon Composite Anode for Lithium‐Ion Capacitors with Improved Energy Density and Cyclability6Controllable Synthesis of Hollow Dodecahedral Si@C Core–Shell Structures for Ultrastable Lithium‐Ion Batteries39Constructing LiF‐Enriched Solid Electrolyte Interface on Graphene Arrays with Abundant Edges on Microscale Si‐C Anodes Toward High‐Energy Lithium‐Ion Batteries60Nanoscale precision welding-enabled quasi-3D conductive carbon blacks for fast-charging and long-lasting secondary batteries9Nanoelectrochemistry in next generation lithium batteries0Pyrolytic Carbon: An Inexpensive, Robust, and Versatile Electrode for Synthetic Organic Electrochemistry4Pyrolytic Carbon: An Inexpensive, Robust, and Versatile Electrode for Synthetic Organic Electrochemistry13

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