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RESEARCH PAPER · Science · 2022

Dynamic interplay between metal nanoparticles and oxide support under redox conditions

Hannes Frey, Arik Beck, Xing Huang, Jeroen A. van Bokhoven, Marc‐Georg Willinger

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Dynamic interplay between metal nanoparticles and oxide support under redox conditionsOriginalDynamics of metal-support interface revealed by environmental transmission electron microscopy15Strong Metal–Support Interaction in Heterogeneous Catalysts469New routes for the construction of strong metal—support interactions55Insights into Heterogeneous Catalysts under Reaction Conditions by In Situ/Operando Electron Microscopy65Recent progress in electrochemical reduction of carbon monoxide toward multi-carbon products50Tuning Strong Metal–Support Interaction Kinetics on Pt-Loaded TiO 2 (110) by Choosing the Pressure: A Combined Ultrahigh Vacuum/Near-Ambient Pressure XPS Study41Insight into the transient inactivation effect on Au/TiO2 catalyst by in-situ DRIFT and UV–vis spectroscopy26Particle Size Effects of Carbon Supported Nickel Nanoparticles for High Pressure CO2 Methanation47Atomic‐Scale Structure Dynamics of Nanocrystals Revealed By In Situ and Environmental Transmission Electron Microscopy106Selective oxidation of methane to CO on Ni@BOx via reaction-induced vapor migration of boron-containing species onto Ni30Metal–Metal Oxide Catalytic Interface Formation and Structural Evolution: A Discovery of Strong Metal–Support Bonding, Ordered Intermetallics, and Single Atoms37Hydrogen Interaction with Oxide Supports in the Presence and Absence of Platinum37Direct environmental TEM observation of silicon diffusion-induced strong metal-silica interaction for boosting CO2 hydrogenation38Engineering Heterogeneous Catalysis with Strong Metal–Support Interactions: Characterization, Theory and Manipulation303Engineering Heterogeneous Catalysis with Strong Metal–Support Interactions: Characterization, Theory and Manipulation28Not Just Another Methanation Catalyst: Depleted Uranium Meets Nickel for a High‐Performing Process Under Autothermal Regime2Bionic structural design of Pt nanozymes with the nano-confined effect for the precise recognition of copper ion24Catalytic modification of corn straw facilitates the remediation of Cd contaminated water and soil23Unveiling the nucleation and evolution of twinned intermetallic nanocrystals for CO-tolerant selective hydrogenation6Chemical Electron Microscopy (CEM) for Heterogeneous Catalysis at Nano: Recent Progress and Challenges11Metal–support interactions for heterogeneous catalysis: mechanisms, characterization techniques and applications163On-chip gas reaction nanolab for in situ TEM observation7Recent progress in porous catalysts for dehydrogenation of ammonia borane28Semi-quantitative determination of active sites in heterogeneous catalysts for photo/electrocatalysis26Support-facet-dependent morphology of small Pt particles on ceria25Understanding the complexity in bridging thermal and electrocatalytic methanation of CO 2105Wet-chemical synthesis of two-dimensional metal oxide-based nanoarchitectures for electrochemical energy conversion0Approaching Elaborate Control of the Nano‐Products of Carbothermal Reduction Reaction Through In Situ Identification3Equilibrium Shapes of Ag, Ni, and Ir Nanoparticles under CO Conditions2Colloidally Engineered Pd and Pt Catalysts Distinguish Surface- and Vapor-Mediated Deactivation Mechanisms25Boosting Chemoselective Hydrogenation of Nitroaromatic via Synergy of Hydrogen Spillover and Preferential Adsorption on Magnetically Recoverable Pt@Fe2O340Studying, Promoting, Exploiting, and Predicting Catalyst Dynamics: the Next Frontier in Heterogeneous Catalysis41Controllable CO2 Reduction or Hydrocarbon Oxidation Driven by Entire Solar via Silver Quantum Dots Direct Photocatalysis17Cooperative Characterization of In Situ TEM and Cantilever-TGA to Optimize Calcination Conditions of MnO2 Nanowire Precursors27Toward In Situ Atomistic Design of Catalytic Active Sites via Controlled Atmosphere Transmission Electron Microscopy30Atomistic Origins of Reversible Noncatalytic Gas–Solid Interfacial Reactions11Enhanced Alkene Selectivity for Transfer Semihydrogenation of Alkynes over Electron-Deficient Pt Nanoparticles Encapsulated in Hollow Silica Nanospheres14Single-atom catalysts for hydroformylation of olefins52Nonclassical Strong Metal–Support Interactions for Enhanced Catalysis28An odyssey to operando environmental transmission electron microscopy: What’s next?7Pt3Ti Intermetallic Alloy Formed by Strong Metal–Support Interaction over Pt/TiO2for the Selective Hydrogenation of Acetophenone60Mesoporous Pt@Pt-skin Pt3Ni core-shell framework nanowire electrocatalyst for efficient oxygen reduction229One positive part of copper ion on biocatalysts: CNPs@Cu-Trypsin-assisted aqueous extraction technique for simultaneous exploration of edible insect oil and protein11Operando Photoelectron Photoion Coincidence Spectroscopy to Detect Short-lived Intermediates in Catalysis4Reduction‐induced metal/oxide interfacial sites for selective CO2 hydrogenation25Shape-Controlled Synthesis of Platinum-Based Nanocrystals and Their Electrocatalytic Applications in Fuel Cells106Microstructure regulation of graphitic carbon nitride nanotubes via quick thermal polymerization process for photocatalytic hydrogen evolution13Oxidative-Atmosphere-Induced Strong Metal–Support Interaction and Its Catalytic Application72Defects Tune the Strong Metal–Support Interactions in Copper Supported on Defected Titanium Dioxide Catalysts for CO 2 Reduction200Insights into the Synthesis Mechanisms of Ag-Cu3P-GaP Multicomponent Nanoparticles7Does Cluster Encapsulation Inhibit Sintering? Stabilization of Size-Selected Pt Clusters on Fe 3 O 4 (001) by SMSI36Thermodynamically and Kinetically Stabilized Pt Clusters Against Sintering on CeO 2 Nanofibers Through Enclosing CeO 2 Nanocubes21Controlling the Strong Metal‐Support Interaction Overlayer Structure in Pt/TiO 2 Catalysts Prevents Particle Evaporation64Controlling the Strong Metal‐Support Interaction Overlayer Structure in Pt/TiO2 Catalysts Prevents Particle Evaporation3Memory-dictated dynamics of single-atom Pt on CeO2 for CO oxidation161Metal-anchoring, metal oxidation-resistance, and electron transfer behavior of oxygen vacancy-rich TiO2 in supported noble metal catalyst for room temperature HCHO conversion26Restructuring of titanium oxide overlayers over nickel nanoparticles during catalysis287In‐Situ Gas–Solid Interactions0PdGa Alloying-Dealloying Processes under Reducing and CO2 Hydrogenation Reaction Conditions from Metadynamics Simu-lations2Imaging Interface and Particle Size Effects by In Situ Correlative Microscopy of a Catalytic Reaction7Atomic Scale Observation of the Structural Dynamics of Supported Gold Nanocatalysts under 1,3‐Butadiene by in situ Environmental Transmission Electron Microscopy5A strong bimetal-support interaction in ethanol steam reforming112Recent advances in in-situ transmission electron microscopy techniques for heterogeneous catalysis54Dynamic Metal–Support Interaction-Activated Sub-Nanometer Pt Clusters on FeOx Supports for Aqueous Phase Reforming and Hydrogenolysis of Glycerol26In Situ and Emerging Transmission Electron Microscopy for Catalysis Research123Oxygen‐Saturated Strong Metal‐Support Interactions Triggered by Water on Titania Supported Catalysts43Phase Segregation in PdCu Alloy Nanoparticles During CO Oxidation Reaction at Atmospheric Pressure17Nickel Nanoparticles Supported on Carbon Cloth via Pulsed Laser Deposition as an Effective Catalyst for Urea Electro-oxidation Reaction5Dynamic evolution of metal nanoclusters revealed by in-situ electron microscopy11Defect‐Mediated Growth of Crystallographic Shear Plane7Depleted uranium oxide supported nickel catalyst for autothermal CO2 methanation in non-adiabatic reactor under induction heating20Cerium-modified Pt/Al2O3 for NH3 synthesis by NO reduction with H212Oscillatory behavior of Ni/TiO2 catalyst during partial oxidation of methane: Understanding the role of strong metal-support interaction11Two-Dimensional Geometry-Dependent Interfaces for Enhanced Water Splitting Kinetics12Effects of Membrane Thickness, Gas Pressure and Electron Dose in Gas Cell Transmission Electron Microscopy2Low Ruthenium Content Confined on Boron Carbon Nitride as an Efficient and Stable Electrocatalyst for Acidic Oxygen Evolution Reaction88Low Ruthenium Content Confined on Boron Carbon Nitride as an Efficient and Stable Electrocatalyst for Acidic Oxygen Evolution Reaction2Direct Observation of Ni Nanoparticle Growth in Carbon-Supported Nickel under Carbon Dioxide Hydrogenation Atmosphere29Enhancing catalytic performance and hot electron generation through engineering metal-oxide and oxide-oxide interfaces10From atomistic to collective dynamics: Bridging gaps in gas-phase electron microscopy for catalysis6Operando investigations of strong metal-support interaction during catalysis2The role of surface hydroxyls in the entropy-driven adsorption and spillover of H2 on Au/TiO2 catalysts157Electrochemical and microscopic characterization of titanium dioxide electrodes modified with platinum nanoparticles4Nanotechnology-based mRNA vaccines163The Effect of Chemical Environment and Temperature on the Domain Structure of Free‐Standing BaTiO3 via In Situ STEM14Nucleation and Growth of Nanocrystals Investigated by In Situ Transmission Electron Microscopy42Quantitative Analysis of the Interface between Titanium Dioxide Support and Noble Metal by Electron Energy Loss Spectroscopy10Metadynamics Simulations Reveal Alloying-Dealloying Processes During CO2 Hydrogenation with Bimetallic PdGa Nanoparticle Catalysts1Double-Edged Sword Effect of Classical Strong Metal–Support Interaction in Catalysts for CO2 Hydrogenation to CO, Methane, and Methanol43Constructing Nanoporous Ir/Ta2O5 Interfaces on Metallic Glass for Durable Acidic Water Oxidation39Oxygen Vacancy-Induced Metal–Support Interactions in AuPd/ZrO 2 Catalysts for Boosting 5-Hydroxymethylfurfural Oxidation39Visualizing interfacial collective reaction behaviour of Li–S batteries576Effects of CO and NO atmospheres on the morphology of Ag, Ni, and Ir nanoparticles1Spinel‐Type Oxides for Acidic Oxygen Evolution Reaction: Mechanism, Modulation, and Perspective30Direct Evidence of Dynamic Metal Support Interactions in Co/TiO2 Catalysts by Near-Ambient Pressure X-ray Photoelectron Spectroscopy10Probing Functional Structures, Defects, and Interfaces of 2D Transition Metal Dichalcogenides by Electron Microscopy42Generation of oxide surface patches promoting H-spillover in Ru/(TiOx)MnO catalysts enables CO2 reduction to CO262Strong Metal–Support Interaction Facilitated Multicomponent Alloy Formation on Metal Oxide Support53Identifying and avoiding dead ends in the characterization of heterogeneous catalysts at the gas–solid interface42Direct Operando Visualization of Metal Support Interactions Induced by Hydrogen Spillover During CO2 Hydrogenation30Alloy strategy to synthesize Pt-early transition metal oxide interfacial catalysts7Atomic Dynamics of Multi‐Interfacial Migration and Transformations8Electronic Phosphide–Support Interactions in Carbon-Supported Molybdenum Phosphide Catalysts Derived from Metal–Organic Frameworks32Recent advances in the engineering and electrochemical applications of amorphous-based nanomaterials: A comprehensive review45Carbon Encapsulation of Supported Metallic Iridium Nanoparticles: An in Situ Transmission Electron Microscopy Study and Implications for Hydrogen Evolution Reaction53Catalytic oxidation of lignite by Pt/TiO2 can enhance cadmium adsorption capacity25Enhanced Methanol Synthesis over Self‐Limited ZnOx Overlayers on Cu Nanoparticles Formed via Gas‐Phase Migration Route49Enhanced Methanol Synthesis over Self‐Limited ZnOx Overlayers on Cu Nanoparticles Formed via Gas‐Phase Migration Route34D Catalysis Concept Enabled by Multilevel Data Collection and Machine Learning Analysis21Exploration of Strong Metal‐Support Interaction in Heterogeneous Catalysts by in situ Transmission Electron Microscopy12In Situ Visualization and Mechanistic Understandings on Facet-Dependent Atomic Redispersion of Platinum on CeO240Water-assisted generation of catalytic interface: The case of interfacial Pt-FeOx(OH)y sites active in preferential carbon monoxide oxidation9A well-defined supported Pt nanoparticle catalyst for heterogeneous catalytic surface science2Catalyst architecture for metal–support interactions and its effects on heterogeneous reactions72Directional growth and reconstruction of ultrafine uranium oxide nanorods within single-walled carbon nanotubes6Dynamics at phase boundaries of active catalyst studied by multi-scale operando EM0Electronic perturbation-promoted interfacial pathway for facile C–H dissociation13Hollow metal-organic frameworks and derivatives1Influences of Ru and ZrO 2 interaction on the hydroesterification of styrene12Metadynamics simulations reveal alloying-dealloying processes for bimetallic PdGa nanoparticles under CO 2 hydrogenation13Metal–support interactions in metal oxide-supported atomic, cluster, and nanoparticle catalysis414Nanoscale chemical characterization of materials and interfaces by tip-enhanced Raman spectroscopy49Organic Synthesis Catalyzed by Metal Nanoparticles0The influence of bulk stoichiometry on near-ambient pressure reactivity of bare and Pt-loaded rutile TiO 2 (110)7Effect of Gas Environment on Metal‐Support Interactions of Supported Metal Catalysts13Spontaneous Formation of Ultrasmall Noble Metal Nanoparticles on Cobalt‐Based Layered Double Hydroxide for Electrochemical and Environmental Catalysis8Fabrication of NiTi-MMO supported on in-situ generated TiO2 for dioctyl phthalate hydrogenation: A strategy for improving the utilization efficiency of Ni0Renaissance of Strong Metal–Support Interactions381Deep Insight into Characterizing the Metal–Support Interface in Heterogeneous Catalysis56Strong Metal‐Support Interactions: From Characterization, Manipulation to Application in Fischer‐Tropsch Synthesis and Atmospheric CO2 hydrogenation19Significance of Epitaxial Growth of PtO 2 on Rutile TiO 2 for Pt/TiO 2 Catalysts117Construction of a Metal–Silica Interface for Semihydrogenation of Alkynes8Microenvironmental regulation of covalent organic frameworks for photocatalytic hydrogen peroxide production70Tuning the CO 2 Hydrogenation Activity via Regulating the Strong Metal–Support Interactions of the Ni/Sm 2 O 3 Catalyst63The relationship between structure and performance of Mo-ZrO2 catalysts in CO2 hydrogenation6Tuning the metal loading of Pt/CeO2 catalysts for the water-gas shift reaction11A Data and DFT-Driven Framework for Predicting the Microstructure of Submonolayer Inverse Metal Oxide on Metal Catalysts10Recent Advances in Coke Management for Dry Reforming of Methane over Ni-Based Catalysts86Tri-system integration in metal-oxide nanocomposites via in-situ solution-processed method for ultrathin flexible transparent electrodes20Structural and chemical transformations of CuZn alloy nanoparticles under reactive redox atmospheres: An in situ TEM study29Strong Interactions between Au Nanoparticles and BiVO4 Photoanode Boosts Hole Extraction for Photoelectrochemical Water Splitting8Strong Interactions between Au Nanoparticles and BiVO4 Photoanode Boosts Hole Extraction for Photoelectrochemical Water Splitting89Reverse water gas-shift reaction product driven dynamic activation of molybdenum nitride catalyst surface77Atomic controlled shell thickness on Pt@Pt3Ti core-shell nanoparticles for efficient and durable oxygen reduction44Heterostructured Catalytic Materials as Advanced Electrocatalysts: Classification, Synthesis, Characterization, and Application149In situ surface etching strategy for bimetallic MOFs-derived oxides and their catalytic properties6Dynamic Active Sites In Situ Formed in Metal Nanoparticle Reshaping under Reaction Conditions34Tuning Adsorbate‐Mediated Strong Metal‐Support Interaction by Oxygen Vacancy: A Case Study in Ru/TiO 264Tuning Adsorbate‐Mediated Strong Metal‐Support Interaction by Oxygen Vacancy: A Case Study in Ru/TiO216How interfacial electron-donating defects influence the structure and charge of gold nanoparticles on TiO2 support7

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