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RESEARCH PAPER · European Journal of Inorganic Chemistry · 2021

A Simple Synthetic Route to Well‐Defined [Pd(NHC)Cl(1‐tBu‐indenyl)] Pre‐catalysts for Cross‐Coupling Reactions

Yaxu Liu, Thomas Scattolin, Alberto Gobbo, Marek Beliš, Kristof Van Hecke, Steven P. Nolan, Catherine S. J. Cazin

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A Simple Synthetic Route to Well‐Defined [Pd(NHC)Cl(1‐tBu‐indenyl)] Pre‐catalysts for Cross‐Coupling ReactionsOriginalCationic palladium( ii )-indenyl complexes bearing phosphines as ancillary ligands: synthesis, and study of indenyl amination and anticancer activity15Indenyl and Allyl Palladate Complexes Bearing N ‐Heterocyclic Carbene Ligands: an Easily Accessible Class of New Anticancer Drug Candidates38Versatile and Highly Efficient trans ‐[Pd(NHC)Cl 2 (DMS/THT)] Precatalysts for C−N and C−C Coupling Reactions in Green Solvents29Realizing 1,1‐Dehydration of Secondary Alcohols to Carbenes: Pyrrolidin‐2‐ols as a Source of Cyclic (Alkyl)(Amino)Carbenes6Realizing 1,1‐Dehydration of Secondary Alcohols to Carbenes: Pyrrolidin‐2‐ols as a Source of Cyclic (Alkyl)(Amino)Carbenes23A Second-Generation Palladacycle Architecture Bearing a N-Heterocyclic Carbene and Its Catalytic Behavior in Buchwald–Hartwig Amination Catalysis10N‐Heterocyclic Carbene‐Palladium Polymers Network: Recyclable Pre‐catalyst for Effective Suzuki–Miyaura Coupling Reaction in Water4Advances in the Synthesis and Applications of N-Heterocyclic Carbene Metal Complexes with a Focus on the Weak Base Route46The role of the stabilizing/leaving group in palladium catalysed cross-coupling reactions5Palladium N-Heterocyclic Carbene-Catalyzed Aminations: An Outline7Tailoring metal complexes with N-heterocyclic carbene ligands using Electron-Withdrawing Groups: Impact on catalytic activity and property development33Metal complexes of backbone-halogenated imidazol-2-ylidenes4Palladium(II)-Indenyl Complexes Bearing N-Heterocyclic Carbene (NHC) Ligands as Potent and Selective Metallodrugs toward High-Grade Serous Ovarian Cancer Models12A Well‐Defined Pd‐NHC Pre‐Catalyst for the Borylation of Aryl Chlorides4Metal–N-Heterocyclic Carbene Complexes in Buchwald–Hartwig Amination Reactions61Well‐Defined [Pd(NHC)(η3‐methylnaphthyl)Br] Complexes in Cross‐Coupling Reactions7Mechanochemical tuning of Pd(BIAN-NHC) allyl/cinnamyl complexes for enhanced cross-coupling0Research Progress on the Buchwald-Hartwig Amination Reactions Catalyzed by N-Heterocyclic Carbene Palladium Complexes1

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  1. Cationic palladium( ii )-indenyl complexes bearing phosphines as ancillary ligands: synthesis, and study of indenyl amination and anticancer activity

    Dalton Transactions · 2022-01-01

    Enrica Bortolamiol, Francesco Fama, Ziyun Zhang, Nicola Demitri, Luigi Cavallo, Isabella Caligiuri, Flavio Rizzolio, Thomas Scattolin, Fabiano Visentin

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  2. Indenyl and Allyl Palladate Complexes Bearing N ‐Heterocyclic Carbene Ligands: an Easily Accessible Class of New Anticancer Drug Candidates

    European Journal of Inorganic Chemistry · 2022-03-17

    Thomas Scattolin, Ilenia Pessotto, Enrico Cavarzerani, Vincenzo Canzonieri, Laura Orian, Nicola Demitri, Claudia S. Schmidt, Angela Casini, Enrica Bortolamiol, Fabiano Visentin, Flavio Rizzolio, Steven P. Nolan

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  3. Versatile and Highly Efficient trans ‐[Pd(NHC)Cl 2 (DMS/THT)] Precatalysts for C−N and C−C Coupling Reactions in Green Solvents

    European Journal of Organic Chemistry · 2022-03-22

    Yaxu Liu, Vladislav A. Voloshkin, Thomas Scattolin, Min Peng, Kristof Van Hecke, Steven P. Nolan, Catherine S. J. Cazin

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  4. Realizing 1,1‐Dehydration of Secondary Alcohols to Carbenes: Pyrrolidin‐2‐ols as a Source of Cyclic (Alkyl)(Amino)Carbenes

    Angewandte Chemie · 2022-04-01

    Ayan Das, Benedict J. Elvers, Mithilesh Kumar Nayak, Nicolas Chrysochos, Srinivas Anga, Amar Kumar, D. Krishna Rao, Tharangattu N. Narayanan, Carola Schulzke, Cem B. Yildiz, Anukul Jana

    Read original paper ↗ ·

  5. Realizing 1,1‐Dehydration of Secondary Alcohols to Carbenes: Pyrrolidin‐2‐ols as a Source of Cyclic (Alkyl)(Amino)Carbenes

    Angewandte Chemie International Edition · 2022-04-01

    Ayan Das, Benedict J. Elvers, Mithilesh Kumar Nayak, Nicolas Chrysochos, Srinivas Anga, Amar Kumar, D. Krishna Rao, Tharangattu N. Narayanan, Carola Schulzke, Cem B. Yildiz, Anukul Jana

    Read original paper ↗ ·

  6. A Second-Generation Palladacycle Architecture Bearing a N-Heterocyclic Carbene and Its Catalytic Behavior in Buchwald–Hartwig Amination Catalysis

    Catalysts · 2023-03-10

    Sylwia Ostrowska, Lorenzo Palio, Agnieszka Czapik, Subhrajyoti Bhandary, Marcin Kwit, Kristof Van Hecke, Steven P. Nolan

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  7. N‐Heterocyclic Carbene‐Palladium Polymers Network: Recyclable Pre‐catalyst for Effective Suzuki–Miyaura Coupling Reaction in Water

    Chemistry & Biodiversity · 2023-04-26

    Wei Huang, Huixian Ye, Xiaodan Li, Yuntong Li, Junyue Lin

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  8. Advances in the Synthesis and Applications of N-Heterocyclic Carbene Metal Complexes with a Focus on the Weak Base Route

    Organometallics · 2023-09-21

    Thomas Scattolin, Aleksei A. Logvinov, Nikolaos V. Tzouras, Catherine S. J. Cazin, Steven P. Nolan

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  9. The role of the stabilizing/leaving group in palladium catalysed cross-coupling reactions

    Dalton Transactions · 2024-01-01

    Lorenzo Palio, Francis Bru, Tommaso Ruggiero, Laurens Bourda, Kristof Van Hecke, Catherine S. J. Cazin, Steven P. Nolan

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  10. Palladium N-Heterocyclic Carbene-Catalyzed Aminations: An Outline

    Topics in Current Chemistry · 2024-01-24

    S. B. Umabharathi, Mohan Neetha, Gopinathan Nair Anilkumar

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  11. Tailoring metal complexes with N-heterocyclic carbene ligands using Electron-Withdrawing Groups: Impact on catalytic activity and property development

    Coordination Chemistry Reviews · 2024-05-28

    Roman O. Pankov, Darya Olegovna Prima, Valentine P. Ananikov

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  12. Metal complexes of backbone-halogenated imidazol-2-ylidenes

    Inorganica Chimica Acta · 2024-07-20

    Alejandro Bugarin, Siddappa A. Patil, Ryan Q Tran, Kostiantyn O. Marichev

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  13. Palladium(II)-Indenyl Complexes Bearing N-Heterocyclic Carbene (NHC) Ligands as Potent and Selective Metallodrugs toward High-Grade Serous Ovarian Cancer Models

    Journal of Medicinal Chemistry · 2024-08-09

    Enrica Bortolamiol, Matteo Mauceri, Rachele Piccolo, Enrico Cavarzerani, Nicola Demitri, Chiara Donati, Valentina Gandin, Simona Kranjc, Urška Kamenšek, Maja Čemažar, Vincenzo Canzonieri, Flavio Rizzolio, Fabiano Visentin, Thomas Scattolin

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  14. A Well‐Defined Pd‐NHC Pre‐Catalyst for the Borylation of Aryl Chlorides

    ChemCatChem · 2025-04-07

    Gianluca Carì, Leandros P. Zorba, Mathieu B. Plumereau, Marcel Matas, Tommaso Ruggiero, Kristof Van Hecke, Matthieu Jouffroy, Catherine S. J. Cazin, Steven P. Nolan

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  15. Metal–N-Heterocyclic Carbene Complexes in Buchwald–Hartwig Amination Reactions

    Chemical Reviews · 2025-06-06

    Sourav Sekhar Bera, Greta Utecht‐Jarzyńska, Shiyi Yang, Steven P. Nolan, Michal Szostak

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  16. Well‐Defined [Pd(NHC)(η3‐methylnaphthyl)Br] Complexes in Cross‐Coupling Reactions

    Chemistry - A European Journal · 2025-07-25

    Gianluca Carì, Riku Saito, Leandros P. Zorba, Tommaso Ruggiero, Kristof Van Hecke, Catherine S. J. Cazin, Steven P. Nolan

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  17. Mechanochemical tuning of Pd(BIAN-NHC) allyl/cinnamyl complexes for enhanced cross-coupling

    Organic & Biomolecular Chemistry · 2026-01-01

    Warda Parveen, Farhat Shakeel, Shehzad Muhammad Raffi, Xiangqun Chi, Bo Wang

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  18. Research Progress on the Buchwald-Hartwig Amination Reactions Catalyzed by N-Heterocyclic Carbene Palladium Complexes

    化学学报 · 2026-01-01

    Yanze Xu, Nannan Han, Xiaoqiong Diao, Jinwei Yuan, Yongmei Xiao, 杨亮茹, Lingbo Qu

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