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RESEARCH PAPER · ACS Omega · 2021

Effect of Drying on the Fabrication of MgAl Layered Double Hydroxides

Luiz Daniel da Silva Neto, Chayene Gonçalves Anchieta, José Leandro da Silva Duarte, Lucas Meili, José Teixeira Freire

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Effect of Drying on the Fabrication of MgAl Layered Double HydroxidesOriginalRevisiting the Structural Evolution of Hydrotalcite‐Derived Mixed Metal Oxides upon Alkali Metal Doping and Its Impact on Base Catalysis2The impact of drying temperature on the crystalline domain and the electrochemical performance of NiCoAl-LDH26Fundamentals of layered double hydroxides and environmental applications4Unveiling the Benefits of Dimethyl Sulfoxide as a Binder Solvent on the Electrochemical Performance of Layered Double Hydroxides0Investigating the Impact of the Washing Steps of Layered Double Hydroxides (LDH) on the Electrochemical Performance12Unveiling the benefits of dimethyl sulfoxide as a binder solvent on the electrochemical performance of layered double hydroxides10A facile synthesis of MgAl/layered double hydroxides from aluminum wastes19Synthesis and characterization of CdCr-NO3 layered double hydroxides nanostructures for Cr(VI) ions adsorption: factorial design and statistical analysis for multivariate sorption optimization0Photocatalytic Degradation of 2,4-Dichlorophenol in Water Using MgAl Activated Hydrotalcites as Photocatalyst4Advantage of Dimethyl Sulfoxide in the Fabrication of Binder-Free Layered Double Hydroxides Electrodes: Impacts of Physical Parameters on the Crystalline Domain and Electrochemical Performance2pH-Responsive Inorganic/Organic Nanohybrids System for Controlled Nicotinic Acid Drug Release11Determination of critical catalyst preparation factors (cCPF) influencing hydrogen evolution5Indulgent of the physiochemical features of MgCr-LDH nanosheets towards photodegradation process of methylene blue75Application of Clay-Biochar Composites as Adsorbents for Water Treatment5Layered double hydroxides: where should research stress on for massive scaling up?28Visible light photoreforming of greenhouse gases by nano Cu–Al LDH intercalated with urea-derived anions7Fabrication of nanostructured ZnNiBi-NO 3 layered double hydroxides for speciation and preconcentration/separation of chromium ions prior to MIS-FAAS determination3Recent advances of layered double hydroxide nanohybrids for photothermal therapy2NHC-heterocycle carbene gold catalyst intercalated in Layered Double Hydroxides as reusable hybrid catalyst in acidic medium5Influence of the synthesis method of layered double hydroxides on the textural properties and nitrate removal13Fluoride removal in drinking water using layered double hydroxide materials: Preparation, characterization and the current perspective on IR4.0 technologies36Engineering the Morphostructural Properties and Drug Loading Degree of Organic–Inorganic Fluorouracil–MgAl LDH Nanohybrids by Rational Control of Hydrothermal Treatment13Ternary MnFeZn layered double hydroxides as an efficient material for the electrochemical sensing of flutamide16Novel MIL-88B(Fe)/ZnTi-LDH high-low junctions for adsorption and photodegradation of tetracycline: Characteristics, performance, and mechanisms118Synergistic Effect of Bimetallic Ni-Based Catalysts Derived from Hydrotalcite on Stability and Coke Resistance for Dry Reforming of Methane5Nanoengineered injectable hydrogels derived from layered double hydroxides and alginate for sustained release of protein therapeutics in tissue engineering applications32Mechanism Insights into Customized Nanoconfined Catalyst Via Peroxymonosulfate Activation for Efficient Sulfamethoxazole Degradation: Key Roles of Electronic Structure and Non-Radical Pathway0Mg–Al LDH nanosheets as a nanotechnological tool in agriculture: an exploratory toxicity evaluation study8Unveiling a robust and high-temperature-stable two-dimensional ZnAl layered double hydroxide nanosheet based flexible triboelectric nanogenerator15A novel LDHs-VB3- inhibitor for rebar corrosion in simulated concrete pore solution: Synthesis, performance and mechanism24Production of MgAl/layered double hydroxide microspheres and investigation of the volumetric heat transfer coefficient in spray drying7Synthesis of biochar-ZnAl-layered double hydroxide composite for effective heavy metal adsorption: Exploring mechanisms and structural transformations36NA-ALGINATE BEADS OF CALCIUM / IRON-LAYERED DOUBLE HYDROXIDE FOR TREATING WATER CONTAMINATED WITH AMOXICILLIN ANTIBIOTIC0Facile and green hydrothermal synthesis of MgAl/NiAl/ZnAl layered double hydroxide nanosheets: a physiochemical comparison9Removal of Metribuzin and Bentazon by LDH-HA Modified Material: Kinetic and Equilibrium Study2Insights into cellular interactions of characterized Mg–Al Layered Double Hydroxide on L929 cells2Zinc-Copper-Nickel Mixed Metal Oxide as Heterogeneous Catalytic Material for the Reductive Degradation of Nitroarene and Azo Dye6Advanced Composite Triboelectric Nanogenerator from Bacterial Cellulose and MgAl-LDH Nanosheets: Synthesis, Performance, and Mechanistic insight0Synthesis and characterization of Ketotifen Fumarate Intercalated Zn–Al Layered Double Hydroxides as sustained-release carriers2Synthesis of LDH-MgAl and LDH-MgFe composites for the efficient removal of the antibiotic from water222D-1D Nanohybrids of CoCr-Layered Double Hydroxides Coupled with Carbon Nanotubes for High Performance Hybrid Supercapacitor9Humidity Effects on Sub-Ambient Direct Air Capture of CO 2 with Amine Functionalized Mg-Al LDHs and MMOs26Recent advances in CO2 capture and mineralization using layered double hydroxide-based materials: A review14Mechanism insights into customized 2D nanoconfined catalyst via peroxymonosulfate activation for efficient sulfamethoxazole degradation: Key roles of electronic structure and non-radical pathway9Enhanced removal of phosphate from aqueous solutions by MgAl-LDH impregnated with LaFeO 36Phosphate recovery using porous monolith MgAl-LDH: insights from NMR spectroscopy, physisorption and microscopy0Improving the Oxygen Evolution Reaction Performance of Ternary Layered Double Hydroxides by Tuning All Three Cations’ Electronic Structures4Preparation and Physicochemical Characterization of Layered Double Hydroxide MgAl‐LDHs/Celecoxib Hybrid Material1Al III - and Fe III -based layered double hydroxides: a review of their characterization techniques and formation mechanisms by co-precipitation with the variable pH method13Fabrication of flexible printed supercapacitor with high cycling stability using Cobalt-Cerium layered double hydroxide7Reactive Capture and Conversion of Carbon Dioxide to Methanol with ZnZrO2 and Alkali-Promoted Mg3AlOx Mixed Oxide Catalytic Sorbents6A composite of alginate impregnated with layer double hydroxide for extraction of sulfonamide antibiotics in honey samples4Optimizing celecoxib loading efficiency on MgAl-layered double hydroxide for enhanced dissolution: Response surface and genetic algorithm approach0Facile synthesis of MgFe-layered double hydroxides (LDHs) for adsorptive removal of malachite green dye from water6Efficient removal of triarylmethane biocide from aqueous solutions using ZnAl/LDH: Adsorption kinetics, isotherms, and thermodynamic insights9Synergistic Integration of MgAl-LDH Nanosheets into Bacterial Cellulose for High-Performance Triboelectric Nanogenerators10Electrochemical Characteristics of Magnesium–Aluminum Layered Double Hydroxide/Reduced Graphene Oxide Nanohybrids4LDH-chitosan bionanocomposites for oncologic applications: A refreshing perspective on the mutual influence through intermolecular forces toward controlled morphology and dispersion2Scheelite (CaWO4) leaching in mild conditions via heptatungstate sorption by MgAl– Layered Double Hydroxide0Magnesium – Aluminium – layered double hydroxides (Mg – Al – LDH) by MgCl2/Mg(NO3)2 mediated electrolysis using aluminium/vitreous carbon electrodes: Prominent in removing fluoride and nitrate from semiconductor wastewater1Fabrication of Mg/Al-LDH photocatalyst for solar-driven degradation of reactive red 120 and bacterial disinfection2Mathematical Modeling of LDH Nanoparticle Drying: Evaluating Effective Diffusivity and the Role of the Mass Biot Number0Reaction Pathways over ZnZrO 2 -Based Catalysts and Catalytic Sorbents1Constructing bifunctional Pd@CoAl-LDHs catalysts via metal-cation-confined in situ reduction for highly efficient reductive amination of biomass-derived cyclohexanone0MgAl-LDH Supported Ag3PO4 Composite for Oxygen Evolution Electrocatalysis: Structural, Electronic, and Interfacial Insights0Zn-Al layered double hydroxide-soy protein isolate biocomposite exhibits superior adsorption of tartrazine food dye and antimicrobial properties1NiAl–gC3N4 Heterocatalyst for Photocatalytic Degradation of Carcinogenic Textile Dyes: Synthesis, Thermal Stability, Dye Selectivity with Adsorption and Computational Insights3Layered double hydroxides intercalated with UV absorbers: preparation, characterisation, and application in UV-resistant asphalt1Multifunctional silver nanoparticles supported on ZnAl-LDH and ZnNiAl-LDH: Applications in reduction and ozonation reactions, and biological activity3Enhanced Selective Adsorption of Cadmium Ions by Lanthanum-Based Layered Double Hydroxide with Wide pH Adaptability1Innovative Formation of Exfoliated Polyethylene Terephthalate Nanocomposites Through Advanced Catalyst-Driven Polymerization1Study on mechanochemical-assisted denitrification of secondary aluminum dross0From rapid reduction to stable immobilization: A regenerative 4D FeMgAl layered double hydroxide–microbial strategy for chromium remediation1Effector dsRNA delivery via MgFe-layered double hydroxide nanocarriers confers prolonged protection against powdery mildew in pea2Aluminum-waste-derived MgAl–LDH for salicylic acid adsorption from water: Kinetics, isotherms and thermodynamic insights0Eco-friendly synthesis of Mg-Al-CO3 layered double hydroxides from seawater desalination brine and their high-efficiency adsorption of Congo Red dye from aqueous solutions0Evaluation of MCoAl-CO3 [M=Ni/Zn] ternary layered double hydroxides for dye-sensitized solar cells and environmental remediation applications0

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  1. Revisiting the Structural Evolution of Hydrotalcite‐Derived Mixed Metal Oxides upon Alkali Metal Doping and Its Impact on Base Catalysis

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  2. The impact of drying temperature on the crystalline domain and the electrochemical performance of NiCoAl-LDH

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  3. Fundamentals of layered double hydroxides and environmental applications

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  4. Unveiling the Benefits of Dimethyl Sulfoxide as a Binder Solvent on the Electrochemical Performance of Layered Double Hydroxides

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  5. Investigating the Impact of the Washing Steps of Layered Double Hydroxides (LDH) on the Electrochemical Performance

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  6. Unveiling the benefits of dimethyl sulfoxide as a binder solvent on the electrochemical performance of layered double hydroxides

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  7. A facile synthesis of MgAl/layered double hydroxides from aluminum wastes

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  8. Synthesis and characterization of CdCr-NO3 layered double hydroxides nanostructures for Cr(VI) ions adsorption: factorial design and statistical analysis for multivariate sorption optimization

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  9. Photocatalytic Degradation of 2,4-Dichlorophenol in Water Using MgAl Activated Hydrotalcites as Photocatalyst

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  10. Advantage of Dimethyl Sulfoxide in the Fabrication of Binder-Free Layered Double Hydroxides Electrodes: Impacts of Physical Parameters on the Crystalline Domain and Electrochemical Performance

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  12. Determination of critical catalyst preparation factors (cCPF) influencing hydrogen evolution

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  13. Indulgent of the physiochemical features of MgCr-LDH nanosheets towards photodegradation process of methylene blue

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  15. Layered double hydroxides: where should research stress on for massive scaling up?

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  16. Visible light photoreforming of greenhouse gases by nano Cu–Al LDH intercalated with urea-derived anions

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  17. Fabrication of nanostructured ZnNiBi-NO 3 layered double hydroxides for speciation and preconcentration/separation of chromium ions prior to MIS-FAAS determination

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  18. Recent advances of layered double hydroxide nanohybrids for photothermal therapy

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  19. NHC-heterocycle carbene gold catalyst intercalated in Layered Double Hydroxides as reusable hybrid catalyst in acidic medium

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  20. Influence of the synthesis method of layered double hydroxides on the textural properties and nitrate removal

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  21. Fluoride removal in drinking water using layered double hydroxide materials: Preparation, characterization and the current perspective on IR4.0 technologies

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  31. Production of MgAl/layered double hydroxide microspheres and investigation of the volumetric heat transfer coefficient in spray drying

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  45. Enhanced removal of phosphate from aqueous solutions by MgAl-LDH impregnated with LaFeO 3

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  47. Improving the Oxygen Evolution Reaction Performance of Ternary Layered Double Hydroxides by Tuning All Three Cations’ Electronic Structures

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  48. Preparation and Physicochemical Characterization of Layered Double Hydroxide MgAl‐LDHs/Celecoxib Hybrid Material

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  49. Al III - and Fe III -based layered double hydroxides: a review of their characterization techniques and formation mechanisms by co-precipitation with the variable pH method

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  50. Fabrication of flexible printed supercapacitor with high cycling stability using Cobalt-Cerium layered double hydroxide

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