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RESEARCH PAPER · ACS Catalysis · 2020

Recent Progresses on Structural Reconstruction of Nanosized Metal Catalysts via Controlled-Atmosphere Transmission Electron Microscopy: A Review

Min Tang, Wentao Yuan, Yang Ou, Guanxing Li, Ruiyang You, Songda Li, Hangsheng Yang, Ze Zhang, Yong Wang

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Recent Progresses on Structural Reconstruction of Nanosized Metal Catalysts via Controlled-Atmosphere Transmission Electron Microscopy: A ReviewOriginalIn situ observation of the crystal structure transition of Pt–Sn intermetallic nanoparticles during deactivation and regeneration7Tuning the shape and crystal phase of TiO 2 nanoparticles for catalysis39Nanocrystallites, adsorption, surface tension, and Wulff rule3In-situ/operando techniques to identify active sites for thermochemical conversion of CO2 over heterogeneous catalysts81Thermally stable single atom catalysts: From concept to in situ study7In situ atomic-scale studies of thermal stability and surface reconstruction of ZnO nanowires based Pd nanocatalysts10Deep reinforcement learning for predicting kinetic pathways to surface reconstruction in a ternary alloy29In-Situ Transmission Electron Microscopy: Electron Beam Effects in Carbon-based Nanomaterials2Facet‐Dependent Oxidative Strong Metal‐Support Interactions of Palladium–TiO 2 Determined by In Situ Transmission Electron Microscopy154Facet‐Dependent Oxidative Strong Metal‐Support Interactions of Palladium–TiO2 Determined by In Situ Transmission Electron Microscopy23A facile and green large-scale fabrication of single atom catalysts for high photocatalytic H2 evolution activity53Dynamics of Rh nanoparticle surface structure during NO reduction revealed by operando transmission electron microscopy14Surface reconstruction induced highly efficient N-doped carbon nanosheet supported copper cluster catalysts for dimethyl carbonate synthesis50A melamine-assisted pyrolytic synthesis of Ag-CeO2 nanoassemblys for CO oxidation: Activation of Ag-CeO2 interfacial lattice oxygen22Influence of Hydrogen Pressure on the Structure of Platinum–Titania Catalysts18Synthesis of Carbon Nanotubes by Floating Catalyst Chemical Vapor Deposition and Their Applications213Single-Atom Engineering to Ignite 2D Transition Metal Dichalcogenide Based Catalysis: Fundamentals, Progress, and Beyond272Confinement Effects in Individual Carbon Encapsulated Nonprecious Metal‐Based Electrocatalysts92Effects of Operation and Shutdown Parameters and Electrode Materials on the Reverse Current Phenomenon in Alkaline Water Analyzers0Surface morphology evolution of cobalt nanoparticles induced by hydrogen adsorption: a theoretical study2Tracking the redox reaction-induced reconstruction of NiAu nanoparticles via environmental scanning transmission electron microscopy4Direct surface functionalization with metal and metal oxide nanostructures6Induced activation of the commercial Cu/ZnO/Al2O3 catalyst for the steam reforming of methanol516Understanding the role of potassium incorporation in realizing transparent p-type ZnO thin films18Ionic liquid modified carbon nanotube supported palladium nanoparticles for efficient Sonogashira-Hagihara reaction20Ppm-level Cu dopant on ultrathin Pd nanosheets/TiO2 for highly enhanced photocatalytic alcoholysis of epoxides30Crystal-Phase-Mediated Restructuring of Pt on TiO 2 with Tunable Reactivity: Redispersion versus Reshaping99Atom‐Resolved Investigation on Dynamic Nucleation and Growth of Platinum Nanocrystals28Effects of operation and shutdown parameters and electrode materials on the reverse current phenomenon in alkaline water analyzers99The Significant Role of the Atomic Surface Structure of Support in Strong Metal‐Support Interaction5Revealing Surface Restraint-Induced Hexagonal Pd Nanocrystals via In Situ Transmission Electron Microscopy14Elucidation of Cu–Zn Surface Alloying on Cu(997) by Machine-Learning Molecular Dynamics9Reversible transformation between terrace and step sites of Pt nanoparticles on titanium under CO and O2 environments11Advanced Transmission Electron Microscopy for Identification of Atomic‐Scale Configurations of Zeolite‐Supported Metal Catalysts8In-situ transmission electron microscopy investigation on the evolution of Pt nanocrystals in oxidizing and reduicng atmospheres1Insights into Heterogeneous Catalysts under Reaction Conditions by In Situ/Operando Electron Microscopy65Atomic‐Scale Structure Dynamics of Nanocrystals Revealed By In Situ and Environmental Transmission Electron Microscopy106Sintering behavior of carbon-supported Pt nanoparticles and the effect of surface overcoating24Promoting n -Butane Dehydrogenation over PtMn/SiO 2 through Structural Evolution Induced by a Reverse Water-Gas Shift Reaction29Crystallization of SrAl12O19 Nanocrystals from Amorphous Submicrometer Particles3Microstructure study of YBa2Cu3O7-δ thin film with synchrotron-based three-dimensional reciprocal space mapping3The phenomenon of “dead” metal in heterogeneous catalysis: opportunities for increasing the efficiency of carbon-supported metal catalysts29Surface Hydroxyl-Determined Migration and Anchoring of Silver on Alumina in Oxidative Redispersion144Toward In Situ Atomistic Design of Catalytic Active Sites via Controlled Atmosphere Transmission Electron Microscopy30Visualizing Catalytic Dynamics Processes via Synchrotron Radiation Multitechniques43Insights into the Synthesis Mechanisms of Ag-Cu3P-GaP Multicomponent Nanoparticles7Particle Attachment Growth of Au@Ag Core–Shell Nanocuboids10In Situ Reconstruction of Electrocatalysts for Lithium–Sulfur Batteries: Progress and Prospects101Advanced In Situ TEM Microchip with Excellent Temperature Uniformity and High Spatial Resolution7Controlling the Strong Metal‐Support Interaction Overlayer Structure in Pt/TiO 2 Catalysts Prevents Particle Evaporation64Controlling the Strong Metal‐Support Interaction Overlayer Structure in Pt/TiO2 Catalysts Prevents Particle Evaporation3In Situ and Emerging Transmission Electron Microscopy for Catalysis Research123Dynamic evolution of metal nanoclusters revealed by in-situ electron microscopy11Revealing Temperature-Dependent Oxidation Dynamics of Ni Nanoparticles via Ambient Pressure Transmission Electron Microscopy29Insight into the Dynamic Evolution of Supported Metal Catalysts by In Situ/Operando Techniques and Theoretical Simulations56Multiscale CO 2 Electrocatalysis to C 2+ Products: Reaction Mechanisms, Catalyst Design, and Device Fabrication328Nucleation and Growth of Nanocrystals Investigated by In Situ Transmission Electron Microscopy42In Situ Transmission Electron Microscopy to Study the Location and Distribution Effect of Pt on the Reduction of Co3O4–SiO24Direct Observation of Sample Dynamics in the Gaseous Environment: A Perspective on Current Trends and Future Directions of In Situ Gas Cell Transmission Electron Microscopy14Selective Hydrogenation of Croton Aldehyde on Pt Nanoparticles Controlled by Tailoring Fraction of Well-Ordered Facets Under Different Pretreatment Conditions5Tuning Redistribution of CuOx Nanoparticles on TiO2 Support3Mechanism of the noncatalytic oxidation of soot using in situ transmission electron microscopy36Modelling of metal nanoparticles’ structures and dynamics under reaction conditions11Recent Developments in Revealing the Impact of Complex Metal Oxide Reconstruction on Catalysis19Nanoscale and ultrafast in situ techniques to probe plasmon photocatalysis19In Situ TEM Characterization and Modulation for Phase Engineering of Nanomaterials83Directional growth and reconstruction of ultrafine uranium oxide nanorods within single-walled carbon nanotubes6In situ analysis of a boron-based catalytic electrode with trace platinum for efficient hydrogen evolution in a wide pH range4In Situ Revealing the Dehydration and Atomic Structure Evolution of Protonated Titanate Nanotubes Via Environmental Transmission Electron Microscopy0Deep Insight into Characterizing the Metal–Support Interface in Heterogeneous Catalysis56Understanding and controlling the formation of single-atom site from supported Cu10 cluster by tuning CeO2 reducibility: Theoretical insight into the Gd-doping effect on electronic metal-support interaction6In situ Tracking the Constrained Reconstruction of Cu3Pd@SiO2 Nanoparticles Driven by Redox Atmospheres1Structural and chemical transformations of CuZn alloy nanoparticles under reactive redox atmospheres: An in situ TEM study29Hydroxide Structure-Dependent OH Promotion Mechanism over a Hydroxylated CoO x /Pt(111) Catalyst toward CO Oxidation36Anomalous Detachment Behavior and Directional Reconstruction Regulation of Leaching‐Type Precatalysts for Industrial Water Electrolyzers10In situ electron microscopy revealing dynamic structure–function relationship of heterogeneous catalyst6Atomically Resolved Transition Pathways of Iron Redox44Oscillatory Active State of a Pd Nanocatalyst Identified by In Situ Capture of the Instantaneous Structure–Activity Change at the Atomic Scale34Cycling and spiral-wave modes in an active cyclic Potts model7Constructing morphologically stable supported noble metal catalysts in heterogeneous catalysis: Mechanisms and strategies79Tracking the dynamics of catalytic Pt/CeO2 active sites during water-gas-shift reaction15Simultaneous 2D Projection and 3D Topographic Imaging of Gas-Dependent Dynamics of Catalytic Nanoparticles8Spatiotemporal patterns in the active cyclic Potts model6Reaction‐Driven Migration Dynamics of Nano‐Metal Particles Unraveled by Quantitative Electron Microscopies3Unraveling the catalytic redox mechanism of lithium–sulfur batteries through advanced in-situ/operando characterizations14Two-dimensional crystalline platinum oxide32Understanding the Dynamic Evolution of Active Sites among Single Atoms, Clusters, and Nanoparticles118Progress in in situ TEM investigations of halide perovskites6Ostwald ripening of supported metal nanoparticles: Role of dimers and other general trends22Imaging Gas‐Involved Structural Dynamics by Environmental Electron Microscopy3Super-dry reforming of methane using a tandem electro-thermocatalytic system85Transition metal oxide nanohybrid materials: A review of their structures, properties, and applications16Operando TEM Probes Dynamic Evolution of Transition Metal‐Based Catalysts and Their Heterostructures11Atmosphere-induced Ru-Ov-CeO2 interface for alleviating hydrogen inhibitory effect toward ammonia decomposition28Solar Flare Tracks: Unveiling Features and Their Impact on Distinct Lunar Soil Transformations0Bridging Structural and Chemical Insights: Integrating In Situ Electron Microscopy and X-ray Spectroscopy for Catalysis Research5A Scoring Model for Catalyst Informatics Based on Real-Time High-Throughput Fluorogenic Assay for Catalyst Discovery and Kinetic Profiling1Surface reconstruction of versatile perovskites via in situ nanoparticle engineering for solid oxide cells4Tracking Morphology Changes During Metal Oxidation Over a Broad Pressure Range Using ETEM With Simultaneous Secondary Electron and STEM Imaging0Advanced spectroscopic, microscopic, and compositional techniques in catalytic material characterization: Applications and progress3Machine Learning Potential Analysis of Structural Transition in Cu and Ag Nanoparticles: From Icosahedral to Face-Centered Cubic5Toward Rational Electrocatalyst Design: Dynamic Insights from Liquid Environmental Transmission Electron Microscopy1Recent advances of single-atom catalysts in the selective catalytic reduction of NO by CO1Integrative Approaches to Reveal Catalyst Dynamics: Bridging Operando Techniques, Theory, and Artificial Intelligence15Imaging nanoscale carrier, thermal, and structural dynamics with time-resolved and ultrafast electron energy-loss spectroscopy6Temporal Resolution of In Situ TEM Limits the Characterization of Catalyst Site Dynamics7Lifting the Fog: Graphene Gas Cell for In Situ (Scanning) Transmission Electron Microscopy with Robust Single-Atom Sensitivity2Gas-Mediated Dynamic Structure Evolution of Bimetallic Alloy Catalysts2Recent Advances in Strong Metal‐Support Interaction Engineering for Dry Reforming of Methane Catalysts14Chemical behaviors regulated by spatial dimensions and microenvironmental factors0Carbon-based atomically dispersed catalysts for enzyme catalysis applications2Dynamic Evolution of Catalyst Structure for Tuned Catalytic Performance in CO 2 Hydrogenation8Strong Metal–Support Interaction in Platinum Group Metal Heterostructured Catalysts5Tailoring the surface properties of catalytic nanomaterials for energy by atmosphere-induced modulation15D-STEM of energy materials: Recording real and reciprocal space dynamics via in situ 4D-STEM0Transient nanomaterials and stimuli-driven transformation pathways for clean energy applications and environmental remediation0A review of transition metal-based double perovskite oxides for photovoltaic applications0

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