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RESEARCH ARTICLE · ACS Central Science · 2020

A Modular Programmable Inorganic Cluster Discovery Robot for the Discovery and Synthesis of Polyoxometalates

Daniel Salley, Graham Keenan, De‐Liang Long, Nicola L. Bell, Leroy Cronin

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A Modular Programmable Inorganic Cluster Discovery Robot for the Discovery and Synthesis of PolyoxometalatesOriginalAdvances in gigantic polyoxomolybdate chemistry13Do robots dream of electronic structures?0Optimization of Formulations Using Robotic Experiments Driven by Machine Learning DoE69Quo Vadis, Polyoxometalate Chemistry?7Toward Machine Learning-Enhanced High-Throughput Experimentation155Expanding the Tool Kit of Automated Flow Synthesis: Development of In-line Flash Chromatography Purification22Robotic Stepwise Synthesis of Hetero-Multinuclear Metal Oxo Clusters as Single-Molecule Magnets62Chemputation and the Standardization of Chemical Informatics73Applied Machine Learning for Developing Next‐Generation Functional Materials72An integrated resource-efficient microfluidic device for parallelised studies of immobilised chiral catalysts in continuous flow via miniaturized LC/MS-analysis7Automated pH Adjustment Driven by Robotic Workflows and Active Machine Learning25An artificial intelligence enabled chemical synthesis robot for exploration and optimization of nanomaterials192Optimization of complex food formulations using robotics and active learning23Insights into the self-assembly of giant polyoxomolybdates from building blocks to supramolecular structures5The Application of Novel Functional Materials to Machine Learning0Automated Library Generation and Serendipity Quantification Enables Diverse Discovery in Coordination Chemistry12The rise of self-driving labs in chemical and materials sciences570Progress of Artificial Intelligence in Drug Synthesis and Prospect of Its Application in Nitrification of Energetic Materials8Population balance modeling of InP quantum dots: Experimentally enabled global optimization to identify unknown material parameters4Robotic Modules for the Programmable Chemputation of Molecules and Materials38Review of Low-cost Self-driving Laboratories: The "Frugal Twin" Concept3New insights on designing the next-generation materials for electrochemical synthesis of reactive oxidative species towards efficient and scalable water treatment: A review and perspectives16An Autonomous Electrochemical Discovery Robot that Utilises Probabilistic Algorithms: Probing the Redox Behaviour of Inorganic Materials16Automation and machine learning augmented by large language models in a catalysis study107Review of low-cost self-driving laboratories in chemistry and materials science: the “frugal twin” concept93The effect of ionic versus covalent functionalization of polyoxometalate hybrid materials with coordinating subunits on their stability and interaction with DNA3Algorithm-Driven Robotic Discovery of Polyoxometalate-Scaffolding Metal–Organic Frameworks34Nonzero-sum game-based decentralized approximate optimal control of modular robot manipulators with coordinate operation tasks using value iteration3An open-source peristaltic pump with multiple independent channels for laboratory automation1Robotic exploration of amino-acid functionalised molybdenum blue polyoxometalate nanoclusters3The emergence of automation in electrochemistry17Development of an Open-Source 3D-Printed Material Synthesis Robot FLUID: Hardware and Software Blueprints for Accessible Automation in Materials Science5Push button, automated flow synthesis of biaryls and stilbenes using palladium-catalysed cross-coupling reactions2Event-Triggered Mixed Nonzero-Sum Game Optimal Control for Modular Robotic Manipulator Performing Coordinated Operation Tasks24Machine learning in X-ray diffraction for materials discovery and characterization19A comprehensive understanding of the use of machine learning in polyoxometalates0A low-cost automated platform for fast and accurate pH control via physics-informed active learning0AI-driven robotic crystal explorer for rapid polymorph identification6Toward self-driving laboratory 2.0 for chemistry and materials discovery15Recent advances on the synthesis, structure and catalytic applications of Ru-OMs4Accelerated discovery of highly active enzyme nanohybrids with parallelized Bayesian optimization in hybrid space7SPACESHIP: Autonomous Mapping of Hardware-Dependent Synthesizable Space in Solution-Phase Gold Nanomaterials0Polyoxometalates for redox chemistry0Accelerating solid form discovery through an expert-guided, semi-automated workflow: Modular Multiwell Devices0

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