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RESEARCH PAPER · Journal of the American Chemical Society · 2020

Elucidating the Weakly Reversible Cs–Pb–Br Perovskite Nanocrystal Reaction Network with High-Throughput Maps and Transformations

Jakob C. Dahl, Xingzhi Wang, Xiao Huang, Emory M. Chan, A. Paul Alivisatos

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Elucidating the Weakly Reversible Cs–Pb–Br Perovskite Nanocrystal Reaction Network with High-Throughput Maps and TransformationsOriginalBandgap determination from individual orthorhombic thin cesium lead bromide nanosheets by electron energy-loss spectroscopy12Hybrid nanocapsules for in situ TEM imaging of gas evolution reactions in confined liquids7How can we predict and determine the ecological carrying capacity of a predator species in an enclosed wildlife protected area?1Alloy CsCd x Pb1– x Br3 Perovskite Nanocrystals: The Role of Surface Passivation in Preserving Composition and Blue Emission72Water Triggered Synthesis of Highly Stable and Biocompatible 1D Nanowire, 2D Nanoplatelet, and 3D Nanocube CsPbBr3 Perovskites for Multicolor Two-Photon Cell Imaging77Machine Learning Accelerated Insights of Perovskite Materials3Surface modification of all-inorganic lead halide perovskite nanocrystals1Multilayer Diffraction Reveals That Colloidal Superlattices Approach the Structural Perfection of Single Crystals62Advanced Multi-laser-beam Parallel Heating System for Rapid High Temperature Treatment2Demystifying the Formation of Colloidal Perovskite Nanocrystals via Controlling Stepwise Synthesis13Highly stable cesium lead bromide perovskite nanocrystals for ultra-sensitive and selective latent fingerprint detection44Combined NMR and Isothermal Titration Calorimetry Investigation Resolves Conditions for Ligand Exchange and Phase Transformation in CsPbBr3 Nanocrystals27High‐Throughput Robotic Synthesis and Photoluminescence Characterization of Aqueous Multinary Copper–Silver Indium Chalcogenide Quantum Dots22Direct Optical Lithography of CsPbX 3 Nanocrystals via Photoinduced Ligand Cleavage with Postpatterning Chemical Modification and Electronic Coupling96The making of a reconfigurable semiconductor with a soft ionic lattice37Nanocristaux semi-conducteurs colloïdaux pour dispositifs opto-électroniques : synthèse et stabilité sous contraintes thermiques et optiques0Vacuum-evaporated lead halide perovskite LEDs [Invited]13Structure and Surface Passivation of Ultrathin Cesium Lead Halide Nanoplatelets Revealed by Multilayer Diffraction48Equilibriums in Formation of Lead Halide Perovskite Nanocrystals34Research Group-Led Undergraduate Research Program: Analyzing and Improving a Versatile Springboard for First-Year Undergraduates8Inverse size-dependent Stokes shift in strongly quantum confined CsPbBr 3 perovskite nanoplates15Multivariate analysis of peptide-driven nucleation and growth of Au nanoparticles12Programmable precise kinetic control over crystal phase, size, and equilibrium in spontaneous metathesis reaction for Cs–Pb–Br nanostructure patterns at room temperature6Development and Prospects of Halide Perovskite Single Crystal Films19Dimensional Control over Metal Halide Perovskite Crystallization Guided by Active Learning32Active meta-learning for predicting and selecting perovskite crystallization experiments24The role of organic ligand shell structures in colloidal nanocrystal synthesis223Transformation of Metal Halides to Facet-Modulated Lead Halide Perovskite Platelet Nanostructures on A-Site Cs-Sublattice Platform15Stable CsPbBr3 Nanoclusters Feature a Disk-like Shape and a Distorted Orthorhombic Structure38Dynamics of Polymer Nanocapsule Buckling and Collapse Revealed by In Situ Liquid-Phase TEM12Stabilizing and accessing across ternary phase cesium lead bromide perovskite nanocrystals: thermodynamic and kinetic controls4How a Facet of a Nanocrystal Is Formed: The Concept of the Symmetry Based Kinematic Theory8Optical Memory, Switching, and Neuromorphic Functionality in Metal Halide Perovskite Materials and Devices77Machine Learning‐Assisted Microfluidic Synthesis of Perovskite Quantum Dots34Big Data in a Nano World: A Review on Computational, Data-Driven Design of Nanomaterials Structures, Properties, and Synthesis83Collective Diffraction Effects in Perovskite Nanocrystal Superlattices57Molecular insights into the growth and time evolution of surface states of CsPbBr 3 nanoparticles synthesized using a scalable room temperature approach10Stability Effects of Selective Anion Abstraction from Cesium Lead Halide Perovskite Nanocrystals2Functional organic cation induced 3D-to-0D phase transformation and surface reconstruction of CsPbI3 inorganic perovskite27Using Data-Driven Learning to Predict and Control the Outcomes of Inorganic Materials Synthesis33Scientific Machine Learning of 2D Perovskite Nanosheet Formation31Exploration of Solution-Processed Bi/Sb Solar Cells by Automated Robotic Experiments Equipped with Microwave Conductivity18Influence of Binary Ligands in Designing Cesium Lead Halide (CsPbX3, X = Cl, Br, I) Perovskite Nanocrystals-Oleic Acid and Oleylamine15Multi-dimensional Data Visualization for Analyzing Materials0Designing semiconductor materials and devices in the post-Moore era by tackling computational challenges with data-driven strategies33Ultrasmall 2D Sn‐Doped MAPbBr 3 Nanoplatelets Enable Bright Pure‐Blue Emission9Reaction-controlled shape evolution and insights into the growth mechanism of CsPbBr3 nanocrystals3Precursor Chemistry of Lead Bromide Perovskite Nanocrystals18The Role of Alkylammonium Bromides on the Surface Passivation of Stable Alcohol‐Dispersed CsPbX3 Nanocrystals and on the Stability Enhancement in Light‐Emitting Applications10Chemical Instability of CsPbBr 3 Nanocrystals and the Reversible Transformation between CsPbBr 3 and Cs 4 PbBr 6 Nanocrystals as Driven by Synthetic Precursors8Machine learning applications in nanomaterials: Recent advances and future perspectives94High-throughput reaction discovery for Cs–Pb–Br nanocrystal synthesis5Automated Gold Nanorod Spectral Morphology Analysis Pipeline12One Pot Synthesis of Cyan Emitting CdZnSSe Quantum Dots for Human Centric Lighting1Optimizing CsPbBr 3 nanowires for high-performance optoelectronics: focusing on blue shift and superfast kinetics through amine-rich synthesis10Unraveling the myths and mysteries of photon avalanching nanoparticles16Elemental Reaction Steps between Elemental Sulfur and Metal Carboxylate during the Synthesis of Metal Sulfide Nanocrystals in Hydrocarbon Solvents1Systematic Study of the Synthesis of Monodisperse CsPbI 3 Perovskite Nanoplatelets for Efficient Color‐Pure Light Emitting Diodes12Metal Doping of Strongly Confined Halide Perovskite Nanocrystals under Ambient Conditions15High-quality and stable perovskite nanocrystals with enhanced properties via photo-brightening3Artificial Intelligence‐Driven Approaches in Semiconductor Research44Thiol ligands engineering for long-term luminescence efficiency of perovskite nanocrystals1Design Principles in Engineering of Multigrain Nanocatalysts via Multiscale Electronic Structure Characterization1Diameter Control and Optical Properties of CsPbBr 3 Nanowires Based on the Oleylamine–Octylamine System2Synthesizer: Chemistry‐Aware Machine Learning for Precision Control of Nanocrystal Growth5Automated Nanocrystal Synthesis: Lessons from 25 Years of Robots, Microfluidics, and Machine Learning7Morphology-Dependent Optical Properties and Exciton Dynamics of CsPbBr 3 Nanowires and Nanoplatelets0Understanding Synthesis Space in Ligand-Assisted Reprecipitated CsPb(Br x I 1– x ) 3 Perovskite Nanocrystals3Unlocking Subunit Cell Precision Overgrowth in CsPbBr 3 Quantum Dots1Effect of concentrations of block copolymer micelles in the synthesis of CsPbBr3 perovskite nanoparticles0Machine Learning‐Guided Elucidation of Spacer‐Dependent Crystallization Pathways in Quasi‐2D Perovskites: Linear vs. Branched Spacer Cations0Machine Learning‐Guided Elucidation of Spacer‐Dependent Crystallization Pathways in Quasi‐2D Perovskites: Linear vs. Branched Spacer Cations0Tuning the Optoelectronic Properties of Wide Bandgap Perovskites: Data‐Driven Insights from Combinatorial Synthesis and High‐Throughput Experimentation0

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  2. Hybrid nanocapsules for in situ TEM imaging of gas evolution reactions in confined liquids

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  3. How can we predict and determine the ecological carrying capacity of a predator species in an enclosed wildlife protected area?

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  4. Alloy CsCd x Pb1– x Br3 Perovskite Nanocrystals: The Role of Surface Passivation in Preserving Composition and Blue Emission

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  5. Water Triggered Synthesis of Highly Stable and Biocompatible 1D Nanowire, 2D Nanoplatelet, and 3D Nanocube CsPbBr3 Perovskites for Multicolor Two-Photon Cell Imaging

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  6. Machine Learning Accelerated Insights of Perovskite Materials

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  7. Surface modification of all-inorganic lead halide perovskite nanocrystals

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  8. Multilayer Diffraction Reveals That Colloidal Superlattices Approach the Structural Perfection of Single Crystals

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  9. Advanced Multi-laser-beam Parallel Heating System for Rapid High Temperature Treatment

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  10. Demystifying the Formation of Colloidal Perovskite Nanocrystals via Controlling Stepwise Synthesis

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  11. Highly stable cesium lead bromide perovskite nanocrystals for ultra-sensitive and selective latent fingerprint detection

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  12. Combined NMR and Isothermal Titration Calorimetry Investigation Resolves Conditions for Ligand Exchange and Phase Transformation in CsPbBr3 Nanocrystals

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  13. High‐Throughput Robotic Synthesis and Photoluminescence Characterization of Aqueous Multinary Copper–Silver Indium Chalcogenide Quantum Dots

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  14. Direct Optical Lithography of CsPbX 3 Nanocrystals via Photoinduced Ligand Cleavage with Postpatterning Chemical Modification and Electronic Coupling

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  16. Nanocristaux semi-conducteurs colloïdaux pour dispositifs opto-électroniques : synthèse et stabilité sous contraintes thermiques et optiques

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  17. Vacuum-evaporated lead halide perovskite LEDs [Invited]

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  18. Structure and Surface Passivation of Ultrathin Cesium Lead Halide Nanoplatelets Revealed by Multilayer Diffraction

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  19. Equilibriums in Formation of Lead Halide Perovskite Nanocrystals

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  21. Inverse size-dependent Stokes shift in strongly quantum confined CsPbBr 3 perovskite nanoplates

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  23. Programmable precise kinetic control over crystal phase, size, and equilibrium in spontaneous metathesis reaction for Cs–Pb–Br nanostructure patterns at room temperature

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  25. Dimensional Control over Metal Halide Perovskite Crystallization Guided by Active Learning

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  38. Stability Effects of Selective Anion Abstraction from Cesium Lead Halide Perovskite Nanocrystals

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  39. Functional organic cation induced 3D-to-0D phase transformation and surface reconstruction of CsPbI3 inorganic perovskite

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  43. Influence of Binary Ligands in Designing Cesium Lead Halide (CsPbX3, X = Cl, Br, I) Perovskite Nanocrystals-Oleic Acid and Oleylamine

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