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RESEARCH PAPER · Angewandte Chemie International Edition · 2020

Optimization of Active Sites via Crystal Phase, Composition, and Morphology for Efficient Low‐Iridium Oxygen Evolution Catalysts

Hui Chen, Lei Shi, Xiao Liang, Lina Wang, Tewodros Asefa, Xiaoxin Zou

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Optimization of Active Sites via Crystal Phase, Composition, and Morphology for Efficient Low‐Iridium Oxygen Evolution CatalystsOriginalFabricating nano-IrO 2 @amorphous Ir-MOF composites for efficient overall water splitting: a one-pot solvothermal approach50Low-iridium electrocatalysts for acidic oxygen evolution31Iridium-based nanomaterials for electrochemical water splitting375Oxygen Reduction Reaction in the Field of Water Environment for Application of Nanomaterials33Boosting the electrocatalytic HER performance of Ni3N-V2O3 via the interface coupling effect128Direct Regulation of Double Cation Defects at the A1A2 Site for a High-Performance Oxygen Evolution Reaction Perovskite Catalyst31Multimetallic nanostructures for electrocatalytic oxygen evolution reaction in acidic media28Nanoporous ultra-high-entropy alloys containing fourteen elements for water splitting electrocatalysis200Regulating the adsorption behavior of intermediates on Ir–W@Ir–WO 3−x boosts acidic water oxidation electrocatalysis28Silver nanomaterials: synthesis and (electro/photo) catalytic applications230Prediction of Dual-Doped Integrated CsPbBr3–CsPbCl3 Perovskite Heterostructure for Practical Photocatalytic Water Splitting with a New Descriptor20Exclusive Strain Effect Boosts Overall Water Splitting in PdCu/Ir Core/Shell Nanocrystals260Exclusive Strain Effect Boosts Overall Water Splitting in PdCu/Ir Core/Shell Nanocrystals47Sustainable catalysts for water electrolysis: Selected strategies for reduction and replacement of platinum-group metals58Host Modification of Layered Double Hydroxide Electrocatalyst to Boost the Thermodynamic and Kinetic Activity of Oxygen Evolution Reaction146Iridium-containing water-oxidation catalysts in acidic electrolyte148SrIrO3 modified with laminar Sr2IrO4 as a robust bifunctional electrocatalyst for overall water splitting in acidic media55Discontinuous solid solutions of anthracene–phenanthrene: Thermodynamics and crystallization kinetics2Sodium‐Decorated Amorphous/Crystalline RuO 2 with Rich Oxygen Vacancies: A Robust pH‐Universal Oxygen Evolution Electrocatalyst680Sodium‐Decorated Amorphous/Crystalline RuO 2 with Rich Oxygen Vacancies: A Robust pH‐Universal Oxygen Evolution Electrocatalyst96Confined Ir single sites with triggered lattice oxygen redox: Toward boosted and sustained water oxidation catalysis554Monolayer Iridium Nanoparticles Coated TiO 2 Core‐Shell Architecture as Efficient Oxygen Evolution Reaction Electrocatalyst3IrRe-IrOx electrocatalysts derived from electrochemically oxidized IrRe thin films for efficient acidic oxygen evolution reaction7On the Durability of Iridium‐Based Electrocatalysts toward the Oxygen Evolution Reaction under Acid Environment255Promoting Electrocatalytic Oxygen Evolution of Ultrasmall NiFe (Hydr)oxide Nanoparticles by Graphene‐Support Effects17Role of surface steps in activation of surface oxygen sites on Ir nanocrystals for oxygen evolution reaction in acidic media69Structural Variations of Metal Oxide‐Based Electrocatalysts for Oxygen Evolution Reaction76In-situ reconstructed Ru atom array on α-MnO2 with enhanced performance for acidic water oxidation1221Tunable Surface Electric Field of Electrocatalysts via Constructing Schottky Heterojunctions for Selective Conversion of Trash Ions to Treasures7Highly active ruthenium sites stabilized by modulating electron-feeding for sustainable acidic oxygen-evolution electrocatalysis312Mitigation of RuO 6 octahedron distortion by enhanced A-site electronegativity in pyrochlore for acidic water oxidation33Nanostructured IrO x supported on N-doped TiO 2 as an efficient electrocatalyst towards acidic oxygen evolution reaction18Iridium‐based electrocatalysts toward sustainable energy conversion46Strategies for Electrochemically Sustainable H2 Production in Acid41The Pivotal Role of s‐, p‐, and f‐Block Metals in Water Electrolysis: Status Quo and Perspectives128Non-catalytic, instant iridium (Ir) leaching: A non-negligible aspect in identifying Ir-based perovskite oxygen-evolving electrocatalysts30Crystal facet engineering of perovskite cobaltite with optimized electronic regulation for water splitting27Single-Phase Perovskite SrIrO 3 Nanofibers as a Highly Efficient Electrocatalyst for a pH-Universal Oxygen Evolution Reaction27Promoting Oxygen Evolution Reaction Induced by Synergetic Geometric and Electronic Effects of IrCo Thin-Film Electrocatalysts34Development of New Mixed-Metal Ruthenium and Iridium Oxides as Electrocatalysts for Oxygen Evolution: Part I12Iridium Doped Pyrochlore Ruthenates for Efficient and Durable Electrocatalytic Oxygen Evolution in Acidic Media101Protonated Iridate Nanosheets with a Highly Active and Stable Layered Perovskite Framework for Acidic Oxygen Evolution75Crystal phase engineering of electrocatalysts for energy conversions53Nd6Ir2O13 as an Efficient Electrocatalyst Boosts the Oxygen Evolution Reaction in Acidic Media25Activation of iridium site by anchoring ruthenium atoms on defects for efficient anodic catalyst in polymer electrolyte membrane water electrolyzers25Regulating Ru-based double perovskite against lattice oxygen oxidation by incorporating Ir for efficient and stable acidic oxygen evolution reaction28Status and perspectives of key materials for PEM electrolyzer497Modulation of IrO6 Chemical Environment for Highly Efficient Oxygen Evolution in Acid25Theory-guided electrocatalyst engineering: From mechanism analysis to structural design188Effective regulation mechanisms of Fe-Ni(oxy)hydroxide: Ni-rich heteroatomic bonding (Ni-O-Fe-O-Ni) is essential23Molten salt assisted Co1−xAgxMoO4 with lattice Ag doping and oxygen vacancy for stable water oxidation11Decomposition of carbon-based catalysts in advanced oxidation processes: A neglected but noteworthy problem23Iridium-titanium oxides for efficient oxygen evolution reaction in acidic media22Acidic oxygen evolution reaction: Mechanism, catalyst classification, and enhancement strategies152Advances and status of anode catalysts for proton exchange membrane water electrolysis technology119Developments and Challenges of Catalytic Materials for Green Hydrogen Production12Efficient oxygen evolution reaction from iron-molybdenum nitride/molybdenum oxide heterostructured composites71Electronic perturbation by interfacial coupling of iridium cluster and Cu 3 P accelerates water splitting kinetics12Flow Cells for CO2 Reduction1Inorganic non-carbon supported Pt catalysts and synergetic effects for oxygen reduction reaction180Coordination Tailoring of Epitaxial Perovskite-Derived Iron Oxide Films for Efficient Water Oxidation Electrocatalysis23Iron-Doped Monoclinic Strontium Iridate as a Highly Efficient Oxygen Evolution Electrocatalyst in Acidic Media6Low-iridium doped single-crystalline hydrogenated titanates (H2Ti3O7) with large exposed {100} facets for enhanced oxygen evolution reaction under acidic conditions5Construction of amorphous/crystalline heterointerfaces for enhanced electrochemical processes257Eliminating over-oxidation of ruthenium oxides by niobium for highly stable electrocatalytic oxygen evolution in acidic media527Electronic and Lattice Engineering of Ruthenium Oxide towards Highly Active and Stable Water Splitting150Trojan strategy assisted phase-pure Fe-NiCo2S4 for industrial anion-exchange membrane water electrolyzer33Colossal Dielectric Perovskites of Calcium Copper Titanate (CaCu 3 Ti 4 O 12 ) with Low‐Iridium Dopants Enables Ultrahigh Mass Activity for the Acidic Oxygen Evolution Reaction35A Study on the Triangular-Wave Electrodeposition of Iridium Oxide on Ti3Phase engineering oriented defect-rich amorphous/crystalline RuO 2 nanoporous particles for boosting oxygen evolution reaction in acid media94Design strategies of electrocatalysts for acidic oxygen evolution reaction41Progress on the mechanisms of Ru-based electrocatalysts for the oxygen evolution reaction in acidic media77Electrocatalytic water splitting over perovskite oxide catalysts77Sol‐Gel‐Syntheses and Structural as well as Electrical Characterizations of Anatase‐ and Rutile‐Type Solid Solutions in the System IrO2−TiO29Amorphous‐Crystalline Interfaces on Hollow Nanocubes Derived from Ir‐Doped Ni–Fe–Zn Prussian Blue Analog Enables High Capability of Alkaline/Acidic/Saline Water Oxidations13Stabilizing the dissolution kinetics by interstitial Zn cations in CoMoO4 for oxygen evolution reaction at high potential6Spinel‐Structured High‐Entropy Oxide Nanofibers as Electrocatalysts for Oxygen Evolution in Alkaline Solution: Effect of Metal Combination and Calcination Temperature108Recent advances in Ru/Ir-based electrocatalysts for acidic oxygen evolution reaction190High Catalytic Activity of Co-centered 2D Metal Organic Frameworks toward Bifunctional Oxygen Evolution and Reduction Reactions: Rationalized by Spin Polarization Effect15Construction of Pd-doped RuO2 nanosheets for efficient and stable acidic water oxidation36Simultaneously Improved Activity and Stability for Acidic Water Oxidation of IrRu Oxides by a Dual Role of Tungsten Doping19Achieving superior oxygen evolution of perovskite via phase transition and electrochemical reconstruction strategy44Rational design of water splitting electrocatalysts through computational insights21Optimizing Edge Active Sites via Intrinsic In‐Plane Iridium Deficiency in Layered Iridium Oxides for Oxygen Evolution Electrocatalysis87The formation of unsaturated IrOx in SrIrO3 by cobalt-doping for acidic oxygen evolution reaction199Enhanced interfacial stability of Pt/TiO2/Ti via Pt-O bonding for efficient acidic electrolyzer20Designing 3d Transition Metal Cation-Doped MRuO x As Durable Acidic Oxygen Evolution Electrocatalysts for PEM Water Electrolyzers170An ink-free integrated dual electrode assembly for economical proton electrolyzer membrane water electrolysis at ultrahigh current densities12Advances in Noble Metal Electrocatalysts for Acidic Oxygen Evolution Reaction: Construction of Under‐Coordinated Active Sites53Ensuring Stability of Anode Catalysts in PEMWE: From Material Design to Practical Application19Unveiling the Activity Origin of Electrochemical Oxygen Evolution on Heteroatom‐Decorated Carbon Matrix10Unveiling the Activity Origin of Electrochemical Oxygen Evolution on Heteroatom‐Decorated Carbon Matrix6Copper Sulfide based Photocatalysts, Electrocatalysts and Photoelectrocatalysts: Innovations in Structural Modulation and Application53Highly dispersed Ir nanoparticles on Ti3C2Tx MXene nanosheets for efficient oxygen evolution in acidic media16Heterogeneous oxide/sulfide materials as superior bifunctional electrocatalysts for carbon-neutral green hydrogen production: A short review10Multiscale engineering of anode catalyst layers in proton exchange membrane water electrolyzers21High stability cubic perovskite Sr0.9Y0.1Co1-Fe O3- oxygen evolution by phase control and electrochemical reconstruction8Recent progress in advanced design of iridium‐based and ruthenium‐based perovskite catalysts for acidic oxygen evolution reaction47Utilizing cationic vacancy defects to switch oxygen evolution mechanisms on atomically dispersed ru for enhanced acidic catalytic performance53Interplay Between Calcination Temperature and Alkaline Oxygen Evolution of Electrospun High‐Entropy (Cr 1/5 Mn 1/5 Fe 1/5 Co 1/5 Ni 1/5 ) 3 O 4 Nanofibers21Iridium-based electrocatalysts for acidic oxygen evolution reaction58Recent Progress in Balancing the Activity, Durability, and Low Ir Content for Ir‐Based Oxygen Evolution Reaction Electrocatalysts in Acidic Media51Partial etching of ZIF-67 nanosheets for the fabrication of S-FeOx/ZIF-67/NF electrodes enabling highly efficient oxygen evolution reaction at large current densities0Electrospun noble metal-based nanofibers for water electrolysis11Interface engineering of RuO 2 /Ru–Co 3 O 4 heterostructures for high-efficiency oxygen evolution in acid0Mechanisms of Nanomaterials in Wastewater Treatment0Transition metal single-atom catalysts for water splitting: Unravelling coordination strategies and catalytic mechanisms for sustainable hydrogen generation12Self‐Healing Iridium‐Doped Manganese Oxide for Boosting Stability of Acidic Oxygen Evolution26Dispersing high loading and uniform IrO2 nanoparticles on acid-resistant oxides by combined ball milling and Adams fusion strategy for proton exchange membrane electrolyzer6Enhanced photoelectrocatalytic activity of IrO2-decorated nano-cuboidal SrTiO3 particles3Iridates for PEM water electrolysis0Mixed iridium-tungsten oxides as highly active and stable anode electrode for proton exchange membrane water electrolyzers7Metal‐Oxygen Octahedra Regulation of Iridium‐Based Perovskites for Efficient and Durable Acidic Water Oxidation19Low‐Ir‐Content Ir0.10Mn0.90O2 Solid Solution for Highly Active Oxygen Evolution in Acid Media18Correlation of Structure and Electrocatalytic Performance of Bulk Oxides for Water Electrolysis5Stability of Doped Ruthenium Oxide as Oxygen Evolution Reaction Electrocatalysts5Optimized Oxidation Temperature Enhances OER Performance of IrO₂‐Loaded SnO₂ Nanofibers – Role of Charge Carrier Percolation Pathways2Acid-Stable High-Entropy Oxide Nanoparticles for Electrochemical Water Oxidation10In situ anchoring RuO2 nanoparticles on δ-MnO2 ultrathin nanosheets for efficient simulated seawater oxidation3Strong Catalyst‐Support Interaction Stabilizes IrO x Nanoclusters for Efficient Acidic Oxygen Evolution7Regulation of Fe2O3@Co3O4 heterostructure for effective acidic oxygen evolution reaction5The Newly Discovered Pathway for Oxygen Evolution Reaction: In‐Situ/Operando Characterization Techniques for Catalyst Development13Facile access to amorphous NiCo2S4 hollow structure with high performance for supercapacitor7High-entropy alloy electrocatalysts for water splitting: A systematic review with perspectives on machine learning and future design strategies9DFT modeling of electrocatalytic water splitting for improvement of experimental relevance9Synthesis and catalytic behaviour of IrO2 nanostructures in acidic water oxidation4Surface hydroxyl participation enables efficient alkaline oxygen evolution on double perovskites for anion exchange membrane water electrolyzers3Sulfur substitution for lattice oxygen in Co(OH)2 activates the lattice oxygen-mediated mechanism for enhancing oxygen evolution reaction2Review of Supported Micro- and Nanometal Oxide Catalysts for Oxygen Evolution in Acidic Media0Unifying Scaling Relations and Multiple Reaction Mechanisms for Screening Transition Metal‐Doped Co 3 O 4 for Oxygen Evolution Reaction2Oxidized‐State Accumulation Controls Water Oxidation Kinetics on a Model Iridium Atomic Array2Oxidized‐State Accumulation Controls Water Oxidation Kinetics on a Model Iridium Atomic Array1The role of oxygen vacancies and metallic Ru in regulating oxide pathway mechanism for acidic water electrolysis1Single-atom catalyst with ion transport for next-generation energy conversion0Ce-doped ZnO@ZIF-8 core-shell nanotube mixed matrix membranes for CO2 separation0Electrospun Ti–Zr Oxide Heterostructures Enable Strongly Anchored Ultralow-Ir Anodes for Durable Acidic Oxygen Evolution0Tailoring electronic structure of electrocatalysts for efficient oxygen evolution reaction in proton exchange membrane electrolyzers0Boosting acidic oxygen evolution reaction through morphology and structure collaborative modulation of iridium-based catalysts0Supported Ir-based anode catalysts for proton exchange membrane water electrolysis: recent progress and perspectives0Dynamic Electron Redistribution on Rooted-Type High-Entropy Perovskite-Supported Ir Catalysts for Durable Proton-Exchange-Membrane Water Electrolysis0Electronic structure engineering of SrIrO3 via tailorable Turing pattern for efficient acidic OER0

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