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RESEARCH PAPER · ACS Central Science · 2019

3D Electron Diffraction: The Nanocrystallography Revolution

Mauro Gemmi, Enrico Mugnaioli, Tatiana E. Gorelik, Ute Kolb, Lukáš Palatinus, Philippe Boullay, Sven Hovmöller, Jan Pieter Abrahams

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3D Electron Diffraction: The Nanocrystallography RevolutionOriginalEvidence for subsolidus quartz-coesite transformation in impact ejecta from the Australasian tektite strewn field183D Electron Diffraction Unravels the New Zeolite ECNU‐23 from the “Pure” Powder Sample of ECNU‐2140Cs3Cu4In2Cl13 Nanocrystals: A Perovskite-Related Structure with Inorganic Clusters at A Sites25Polymorph evolution during crystal growth studied by 3D electron diffraction40MicroED methodology and development48Nanoscale tailoring of supramolecular crystals via an oriented external electric field21Structural analysis of metastable pharmaceutical loratadine form II, by 3D electron diffraction and DFT+D energy minimisation23A Compact Ultrafast Electron Diffractometer with Relativistic Femtosecond Electron Pulses14Fast-ADT: A fast and automated electron diffraction tomography setup for structure determination and refinement82Circumventing Wear and Tear of Adaptive Porous Materials18Serial protein crystallography in an electron microscope118Spiro-Conjugated Carbon/Heteroatom-Bridged p-Phenylenevinylenes: Synthesis, Properties, and Microcrystal Electron Crystallographic Analysis of Racemic Solid Solutions26New zeolite-like RUB-5 and its related hydrous layer silicate RUB-6 structurally characterized by electron microscopy22Donwilhelmsite, [CaAl4Si2O11], a new lunar high-pressure Ca-Al-silicate with relevance for subducted terrestrial sediments46Nanocrystals of Lead Chalcohalides: A Series of Kinetically Trapped Metastable Nanostructures67Racemic Conglomerate Formation via Crystallization of Metaxalone from Volatile Deep Eutectic Solvents19Beam-sensitive metal-organic framework structure determination by microcrystal electron diffraction28An Expandable Hydrogen-Bonded Organic Framework Characterized by Three-Dimensional Electron Diffraction110Advances in methods for atomic resolution macromolecular structure determination46Fragment-based determination of a proteinase K structure from MicroED data using ARCIMBOLDO_SHREDDER14Structure Determination from Lipidic Cubic Phase Embedded Microcrystals by MicroED29Visualizing drug binding interactions using microcrystal electron diffraction31Atomically Precise Nanocrystals75InsteaDMatic: towards cross-platform automated continuous rotation electron diffraction28Electron Diffraction on Flash-Frozen Cowlesite Reveals the Structure of the First Two-Dimensional Natural Zeolite28Color Differences Highlight Concomitant Polymorphism of Chalcones13Synthesis of Discrete CHA Zeolite Nanocrystals without Organic Templates for Selective CO2 Capture116Atoms and the void: modular construction of ordered porous solids30Synthesis of Discrete CHA Zeolite Nanocrystals without Organic Templates for Selective CO2 Capture13The structure of kaliophilite KAlSiO4, a long-lasting crystallographic problem16B/N-Doped p-Arylenevinylene Chromophores: Synthesis, Properties, and Microcrystal Electron Crystallographic Study57Two new minerals, badengzhuite, TiP, and zhiqinite, TiSi 2 , from the Cr-11 chromitite orebody, Luobusa ophiolite, Tibet, China: is this evidence for super-reduced mantle-derived fluids?28A new olanzapine cocrystal obtained from volatile deep eutectic solvents and determined by 3D electron diffraction23Microcrystal electron diffraction in macromolecular and pharmaceutical structure determination21Three-dimensional electron diffraction for porous crystalline materials: structural determination and beyond117Statistically correcting dynamical electron scattering improves the refinement of protein nanocrystals, including charge refinement of coordinated metals17Effect of pressure on the properties of a NASICON Li 1.3 Al 0.3 Ti 1.7 (PO 4 ) 3 nanofiber solid electrolyte28On the completeness of three-dimensional electron diffraction data for structural analysis of metal–organic frameworks23Reticular design and crystal structure determination of covalent organic frameworks106Structure determination of small molecule compounds by an electron diffractometer for 3D ED/MicroED106Local Crystallinity in Twisted Cellulose Nanofibers87Multiscale Assembly of [AgS4] Tetrahedrons into Hierarchical Ag–S Networks for Robust Photonic Water18Pair Distribution Function Obtained from Electron Diffraction: An Advanced Real-Space Structural Characterization Tool63Jingsuiite, TiB2, a new mineral from the Cr-11 podiform chromitite orebody, Luobusa ophiolite, Tibet, China: Implications for recycling of boron14Macromolecular crystallography using microcrystal electron diffraction17Surface characterization of pharmaceutical solids16Photoactive Heterostructures: How They Are Made and Explored22Three-Dimensional Electron Diffraction for Structural Analysis of Beam-Sensitive Metal-Organic Frameworks15High‐Throughput Electron Diffraction Reveals a Hidden Novel Metal–Organic Framework for Electrocatalysis54Alternating Heterochiral Supramolecular Copolymerization76Fluorescence-Based Sensing of Pesticides Using Supramolecular Chemistry69The Elusive Structure of Magadiite, Solved by 3D Electron Diffraction and Model Building48Combining X-rays, neutrons and electrons, and NMR, for precision and accuracy in structure–function studies17MyD88 TIR domain higher-order assembly interactions revealed by microcrystal electron diffraction and serial femtosecond crystallography99Dynamics of Supramolecular Crystal Growth at the Liquid–Solid Interface Studied via Scanning Tunneling Microscope and the Avrami Equation14Serial Electron Diffraction Data Processing With diffractem and CrystFEL23Synthesis and Structure of a 22 × 12 × 12 Extra-Large Pore Zeolite ITQ-56 Determined by 3D Electron Diffraction48Guidelines for the characterization of metal halide nanocrystals143D Electron Diffraction Structure Determination of Terrylene, a Promising Candidate for Intermolecular Singlet Fission14Design of metastable oxychalcogenide phases by topochemical (de)intercalation of sulfur in La2O2S224Integrative Structural Biology in the Era of Accurate Structure Prediction53Refinements on electron diffraction data of β-glycine in MoPro: a quest for an improved structure model16Establishing electron diffraction in chemical crystallography77A Close Look at Molecular Self-Assembly with the Transmission Electron Microscope73Structure determination, thermal stability and dissolution rate of δ-indomethacin38Comprehensive Study of Li+/Ni2+ Disorder in Ni-Rich NMCs Cathodes for Li-Ion Batteries69Toward Compositional Contrast by Cryo-STEM263D Electron Diffraction for Chemical Analysis: Instrumentation Developments and Innovative Applications91Measurement of Temporal Coherence of Free Electrons by Time-Domain Electron Interferometry21Revealing the early stages of carbamazepine crystallization by cryoTEM and 3D electron diffraction24Probing Molecular Motions in Metal–Organic Frameworks by Three-Dimensional Electron Diffraction34MicroED for the study of protein–ligand interactions and the potential for drug discovery17Chirality determination in crystals35Unraveling the Electrical and Magnetic Properties of Layered Conductive Metal‐Organic Framework With Atomic Precision80Unraveling the Electrical and Magnetic Properties of Layered Conductive Metal‐Organic Framework With Atomic Precision18Structure and Surface Passivation of Ultrathin Cesium Lead Halide Nanoplatelets Revealed by Multilayer Diffraction48Indomethacin Polymorph δ Revealed To Be Two Plastically Bendable Crystal Forms by 3D Electron Diffraction: Correcting a 47‐Year‐Old Misunderstanding**54Electron Microscopy of Nanoporous Crystals21Rare earth nanominerals in bentonite deposits of the Eocene Texas coastal plains17A structure determination protocol based on combined analysis of 3D-ED data, powder XRD data, solid-state NMR data and DFT-D calculations reveals the structure of a new polymorph of l -tyrosine45Organic Cocrystals of TCNQ and TCNB Based on an Orthocetamol Backbone Solved by Three-Dimensional Electron Diffraction13SCM-25: A Zeolite with Ordered Meso-cavities Interconnected by 12 × 12 × 10-Ring Channels Determined by 3D Electron Diffraction17Characterization of metal-organic frameworks by transmission electron microscopy16Microscopic Insights into Cation-Coupled Electron Hopping Transport in a Metal–Organic Framework64Structure of the active pharmaceutical ingredient bismuth subsalicylate41Electron Diffraction Enables the Mapping of Coke in ZSM‐5 Micropores Formed during Methanol‐to‐Hydrocarbons Conversion33Phosphinate MOFs Formed from Tetratopic Ligands as Proton-Conductive Materials143D electron diffraction for structure determination of small‐molecule nanocrystals: A possible breakthrough for the pharmaceutical industry20Halide perovskites as disposable epitaxial templates for the phase-selective synthesis of lead sulfochloride nanocrystals50Single-crystal structure determination of nanosized metal–organic frameworks by three-dimensional electron diffraction99Direct Location of Organic Molecules in Framework Materials by Three-Dimensional Electron Diffraction27Electron Diffraction of 3D Molecular Crystals98In Situ Three-Dimensional Electron Diffraction for Probing Structural Transformations of Single Nanocrystals13Accurate lattice parameters from 3D electron diffraction data. I. Optical distortions58Selective and Reversible Solvent Uptake in Tetra‐4‐(4‐pyridyl)phenylmethane‐based Supramolecular Organic Frameworks15Atomic-level structural responsiveness to environmental conditions from 3D electron diffraction34Structure and function tailored metal-organic frameworks for heterogeneous catalysis28Authigenic clays as precursors to carbonate precipitation in saline lakes of Salar de Llamara, Northern Chile23Microcrystal electron diffraction (MicroED) structure determination of a mechanochemically synthesized co-crystal not affordable from solution crystallization27Hydrogen atoms in supramolecular chemistry: a structural perspective. Where are they, and why does it matter?25Massive Accumulation of Strontium and Barium in Diplonemid Protists25A 3D extra-large-pore zeolite enabled by 1D-to-3D topotactic condensation of a chain silicate172Direct structure determination of vemurafenib polymorphism from compact spherulites using 3D electron diffraction14High-throughput phase elucidation of polycrystalline materials using serial rotation electron diffraction33Electron-Beam- and Thermal-Annealing-Induced Structural Transformations in Few-Layer MnPS318One-step preparation of photoresponsive microcapsules based on the interfacial self-assembly of an azopyridine coordination polymer14Catching a New Zeolite as a Transition Material during Deconstruction17Electron crystallography and dedicated electron-diffraction instrumentation27The Elusive Structure of Levocetirizine Dihydrochloride Determined by Electron Diffraction27Accurate structure models and absolute configuration determination using dynamical effects in continuous-rotation 3D electron diffraction data131Jana2020 – a new version of the crystallographic computing system Jana505Stable Sn-Based Hybrid Perovskite-Related Structures with Tunable Color Coordinates via Organic Cations in Low-Temperature Synthesis20Structure Elucidation of Secondary Metabolites: Current Frontiers and Lingering Pitfalls24Research Progress on Metal–Organic Frameworks by Advanced Transmission Electron Microscopy27Structure determination of a low-crystallinity covalent organic framework by three-dimensional electron diffraction21In Situ and Emerging Transmission Electron Microscopy for Catalysis Research123Locating Hydrogen Positions for COF‐300 by Cryo‐3D Electron Diffraction23A robust ultra-microporous cationic aluminum-based metal-organic framework with a flexible tetra-carboxylate linker20Making the Most of 3D Electron Diffraction: Best Practices to Handle a New Tool43Atomic-level structure determination of amorphous molecular solids by NMR60Stimuli‐Responsive, Dynamic Supramolecular Organic Frameworks34Scaling up cryo-EM for biology and chemistry: The journey from niche technology to mainstream method17Quantitative three-dimensional local order analysis of nanomaterials through electron diffraction21Reticular Synthesis of Highly Crystalline Three-Dimensional Mesoporous Covalent–Organic Frameworks for Lipase Inclusion61STEM SerialED: achieving high-resolution data for ab initio structure determination of beam-sensitive nanocrystalline materials27Unveiling the topology of partially disordered micro-crystalline nitro-perylenediimide with X-aggregate stacking: an integrated approach16High-Throughput Identification of Crystalline Natural Products from Crude Extracts Enabled by Microarray Technology and microED28Discovery of new cocrystals beyond serendipity: lessons learned from successes and failures28Electron diffraction and solid-state NMR reveal the structure and exciton coupling in a eumelanin precursor25Structure Determination of Biogenic Crystals Directly from 3D Electron Diffraction Data22Topological Analysis and Structural Determination of 3D Covalent Organic Frameworks48Single crystal perovskite an emerging photocatalytic and storage material: Synthesis to applications via theoretical insight20Comprehensive Application of XFEL Microcrystallography for Challenging Targets in Various Organic Compounds14Controlling Phase in Colloidal Synthesis39Mechanochemical Synthesis and Three-Dimensional Electron Diffraction Structure Solution of a Novel Cu-Based Protocatechuate Metal–Organic Framework17Structure Low Dimensionality and Lone-Pair Stereochemical Activity: the Key to Low Thermal Conductivity in the Pb–Sn–S System57Current trends and advancements in crystallization and single-crystal structural analysis of small molecules45High-speed imaging and quantitative analysis of nonequilibrium stochastic processes using atomic resolution electron microscopy28Cryo-tomography and 3D Electron Diffraction Reveal the Polar Habit and Chiral Structure of the Malaria Pigment Crystal Hemozoin15Atomic-level structure of the amorphous drug atuliflapon via NMR crystallography17Single Entity Electrocatalysis58In Situ Study of the Activation Process of MOF-74 Using Three-Dimensional Electron Diffraction29Single-Crystal Structural Analysis of 2D Metal–Organic Frameworks and Covalent Organic Frameworks by Three-Dimensional Electron Diffraction27Spiers Memorial Lecture: NMR crystallography19Defining, designing and determining the structure of supramolecular frameworks17Atomic-scale insights into topotactic transformations in an extra-large-pore zeolite using time-resolved 3D electron diffraction22A Novel Ti 12 ‐Based Metal‐Organic Framework for Photocatalytic Hydrogen Evolution21Retrospective Review on Reticular Materials: Facts and Figures Over the Last 30 Years21Single-crystalline covalent organic frameworks: Synthesis, characterizations, and functions312D Open Framework Materials: Chemistry, Materials, and Applications34

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  1. Evidence for subsolidus quartz-coesite transformation in impact ejecta from the Australasian tektite strewn field

    Geochimica et Cosmochimica Acta · 2019-08-21

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  2. 3D Electron Diffraction Unravels the New Zeolite ECNU‐23 from the “Pure” Powder Sample of ECNU‐21

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  3. 3D Electron Diffraction Unravels the New Zeolite ECNU‐23 from the “Pure” Powder Sample of ECNU‐21

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  4. Synthèse et étude structurale de nanozeolites à petits micropores pour la capture du CO2

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  5. Microcrystal electron diffraction methodology and applications

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  6. Cs3Cu4In2Cl13 Nanocrystals: A Perovskite-Related Structure with Inorganic Clusters at A Sites

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  7. Polymorph evolution during crystal growth studied by 3D electron diffraction

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  10. Nanoscale tailoring of supramolecular crystals via an oriented external electric field

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  12. Structural analysis of metastable pharmaceutical loratadine form II, by 3D electron diffraction and DFT+D energy minimisation

    CrystEngComm · 2020-01-01

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  14. Fast-ADT: A fast and automated electron diffraction tomography setup for structure determination and refinement

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  16. Serial protein crystallography in an electron microscope

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  17. Spiro-Conjugated Carbon/Heteroatom-Bridged p-Phenylenevinylenes: Synthesis, Properties, and Microcrystal Electron Crystallographic Analysis of Racemic Solid Solutions

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  18. New zeolite-like RUB-5 and its related hydrous layer silicate RUB-6 structurally characterized by electron microscopy

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  19. Donwilhelmsite, [CaAl4Si2O11], a new lunar high-pressure Ca-Al-silicate with relevance for subducted terrestrial sediments

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  20. Nanocrystals of Lead Chalcohalides: A Series of Kinetically Trapped Metastable Nanostructures

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  21. Orientational disorder of monomethyl-quinacridone investigated by Rietveld refinement, structure refinement to the pair distribution function and lattice-energy minimizations

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  22. Racemic Conglomerate Formation via Crystallization of Metaxalone from Volatile Deep Eutectic Solvents

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  23. Beam-sensitive metal-organic framework structure determination by microcrystal electron diffraction

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  24. Exotic compositional ordering in Mn-Ni-As intermetallics

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  30. Electron Diffraction as a Tool for Hydrogen Atom Localization and Absolute Structure Determination of Nanocrystals Containing Organic Molecules

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  31. Structural Characterization of Beam Sensitive Pharmaceutical Compounds Using 3D Electron Diffraction-Micro-ED at Low Dose with Pixelated Detectors

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  32. Structure Determination from Lipidic Cubic Phase Embedded Microcrystals by MicroED

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  33. Visualizing drug binding interactions using microcrystal electron diffraction

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  34. The Effect of the Starting Mineralogical Mixture on the Nature of Fe-Serpentines Obtained during Hydrothermal Synthesis AT 90°C

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  35. Atomically Precise Nanocrystals

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  36. InsteaDMatic: towards cross-platform automated continuous rotation electron diffraction

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  37. Electron Diffraction on Flash-Frozen Cowlesite Reveals the Structure of the First Two-Dimensional Natural Zeolite

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  38. Color Differences Highlight Concomitant Polymorphism of Chalcones

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  39. Exotic Compositional Ordering in Manganese–Nickel–Arsenic (Mn‐Ni‐As) Intermetallics

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  40. Exotic Compositional Ordering in Manganese–Nickel–Arsenic (Mn‐Ni‐As) Intermetallics

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  41. Research progress on the crystal structure determination using electron diffraction

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  42. Synthesis of Discrete CHA Zeolite Nanocrystals without Organic Templates for Selective CO2 Capture

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  43. Atoms and the void: modular construction of ordered porous solids

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  44. Synthesis of Discrete CHA Zeolite Nanocrystals without Organic Templates for Selective CO2 Capture

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  45. The structure of kaliophilite KAlSiO4, a long-lasting crystallographic problem

    IUCrJ · 2020-09-28

    Enrico Mugnaioli, Elena Bonaccorsi, Arianna Lanza, Erik Elkaı̈m, Virginia Diez-Gómez, Isabel Sobrados, Mauro Gemmi, Michele Gregorkiewitz

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  46. Fabrication of low aspect ratio three-element Boersch phase shifters for voltage-controlled three electron beam interference

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  47. The structure of a new nano-phase of lanthanum-doped strontium titanate

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    Ercin Cagan Duran, Alexander S. Eggeman

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  48. B/N-Doped p-Arylenevinylene Chromophores: Synthesis, Properties, and Microcrystal Electron Crystallographic Study

    Journal of the American Chemical Society · 2020-10-22

    Hua Lü, Takayuki Nakamuro, Keitaro Yamashita, Haruaki Yanagisawa, Osamu Nureki, Masahide Kikkawa, Han Gao, Jiangwei Tian, Rui Shang, Eiichi Nakamura

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  49. Structural study of decrespignyite-(Y), a complex yttrium rare earth copper carbonate chloride, by three-dimensional electron and synchrotron powder diffraction

    European Journal of Mineralogy · 2020-10-23

    Jordi Rius, Fernando Colombo, Oriol Vallcorba, X. Torrelles, Mauro Gemmi, Enrico Mugnaioli

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  50. Two new minerals, badengzhuite, TiP, and zhiqinite, TiSi 2 , from the Cr-11 chromitite orebody, Luobusa ophiolite, Tibet, China: is this evidence for super-reduced mantle-derived fluids?

    European Journal of Mineralogy · 2020-11-02

    Fahui Xiong, Xiangzhen Xu, Enrico Mugnaioli, Mauro Gemmi, Richard Wirth, Edward S. Grew, Paul T. Robinson, Jingsui Yang

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