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RESEARCH PAPER · Inorganic Chemistry · 2000

Syntheses and Structures of TcOF5and the Tc2O2F9+Cation and Formation of the TcOF4+Cation in Solution

Nicolas LeBlond, Hélène P. A. Mercier, David A. Dixon, Gary J. Schrobilgen

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Syntheses and Structures of TcOF5and the Tc2O2F9+Cation and Formation of the TcOF4+Cation in SolutionOriginal13 Manganese, technetium and rhenium421 New compounds and structures in the solid state1ChemInform Abstract: Syntheses and Structures of TcOF5 and the Tc2O2F9+ Cation and Formation of the TcOF4+ Cation in Solution.0Untitled work3X-ray Crystal Structures of α-KrF2, [KrF][MF6] (M = As, Sb, Bi), [Kr2F3][SbF6]·KrF2, [Kr2F3]2[SbF6]2·KrF2, and [Kr2F3][AsF6]·[KrF][AsF6]; Synthesis and Characterization of [Kr2F3][PF6]·nKrF2; and Theoretical Studies of KrF2, KrF+, Kr2F3+, and the [KrF][MF6] (M = P, As, Sb, Bi) Ion Pairs78The chemistry of krypton142Technetium24Noble‐Gas Compounds4MoF6 and WF6: Nonrigid Molecules?27Structural overview of technetium compounds (2000–2004)38Halogens and noble gases15High-Valent Technetium Fluorides. Does TcF7 Exist?18Applications in Inorganic Chemistry60Heterocations in Superacid Systems0The highest oxidation states of the transition metal elements216Density-functional computation of 99Tc NMR chemical shifts34Synthesis and X-ray Crystal Structure of (OsO3F2)2·2XeOF4 and the Raman Spectra of (OsO3F2)∞, (OsO3F2)2, and (OsO3F2)2·2XeOF410Fluoride Ion Donor Properties of cis-OsO2F4: Synthesis, Raman Spectroscopic Study, and X-ray Crystal Structure of [OsO2F3][Sb2F11]7Syntheses and Multi-NMR Study offac- andmer-OsO3F2(NCCH3) and the X-ray Crystal Structure (n= 2) and Raman Spectrum (n= 0) offac-OsO3F2(NCCH3)·nCH3CN6Preparation of Transition Metal Fluorides using ClF 34Noble‐Gas Compounds2High-Valent Fluorides and Fluoro-Oxidizers26Noble-Gas Chemistry41Hexafluoridotechnetate(IV) Revisited17Polar Alignment of Λ-Shaped Basic Building Units within Transition Metal Oxide Fluoride Materials15[XeOXeOXe]2+, the Missing Oxide of Xenon(II); Synthesis, Raman Spectrum, and X-ray Crystal Structure of [XeOXeOXe][μ-F(ReO2F3)2]218Trends in NMR chemical shifts of d0 transition metal compounds15The Reaction of Cs2[Tc(NO)F5] with BF3 in Acetonitrile: Formation and Structure of [{Tc(NO)(CH3CN)4}2(μ‐F)](BF4)37Chemistry at the Edge of the Periodic Table: The Importance of Periodic Trends on the Discovery of the Noble Gases and the Development of Noble-Gas Chemistry4Bis(tetraphenylarsonium) hexafluoridotechnetate(IV) dihydrate: preparation, structure and spectroscopic analysis3Fluoride ion donor ability of binary fluorides towards the Lewis acids AsF5 and SbF55Technetium ‐ The Unknown Center of the Periodic Table11

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  1. 13 Manganese, technetium and rhenium

    Annual Reports Section A (Inorganic Chemistry) · 2000-01-01

    PETER E. THORNTON

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  2. 21 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2000-01-01

    William T. A. Harrison

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  3. ChemInform Abstract: Syntheses and Structures of TcOF5 and the Tc2O2F9+ Cation and Formation of the TcOF4+ Cation in Solution.

    ChemInform · 2001-01-09

    Nicolas LeBlond, Hélène P. A. Mercier, David A. Dixon, Gary J. Schrobilgen

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  4. Untitled work

    Annual Reports Section A (Inorganic Chemistry) · 2001-01-28

    Paul F. Kelly

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  5. X-ray Crystal Structures of α-KrF2, [KrF][MF6] (M = As, Sb, Bi), [Kr2F3][SbF6]·KrF2, [Kr2F3]2[SbF6]2·KrF2, and [Kr2F3][AsF6]·[KrF][AsF6]; Synthesis and Characterization of [Kr2F3][PF6]·nKrF2; and Theoretical Studies of KrF2, KrF+, Kr2F3+, and the [KrF][MF6] (M = P, As, Sb, Bi) Ion Pairs

    Inorganic Chemistry · 2001-05-22

    John F. Lehmann, David A. Dixon, Gary J. Schrobilgen

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  6. The chemistry of krypton

    Coordination Chemistry Reviews · 2002-11-01

    John F. Lehmann

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  7. Technetium

    Elsevier eBooks · 2003-01-01

    Roger A. Alberto

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  8. Noble‐Gas Compounds

    Kirk-Othmer Encyclopedia of Chemical Technology · 2003-04-18

    Gary J. Schrobilgen, Matthew D. Moran

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  9. MoF6 and WF6: Nonrigid Molecules?

    Chemistry - A European Journal · 2004-08-13

    Gustavo Santiso Quiñones, Gerhard Hägele, Konrad Seppelt

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  10. Structural overview of technetium compounds (2000–2004)

    Coordination Chemistry Reviews · 2005-11-03

    Giuliano Bandoli, Francesco Tisato, Alessandro Dolmella, Stefania Agostini

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  11. Halogens and noble gases

    Annual Reports Section A (Inorganic Chemistry) · 2007-01-01

    Alan K. Brisdon

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  12. High-Valent Technetium Fluorides. Does TcF7 Exist?

    Inorganic Chemistry · 2007-06-15

    Sebastian Riedel, Manuel Renz, Martin Kaupp

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  13. Applications in Inorganic Chemistry

    Unknown journal · 2008-04-30

    Kazuo Nakamoto

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  14. Heterocations in Superacid Systems

    Unknown journal · 2008-06-19

    George Andrew Olah, G. K. Surya Prakash, Árpàd Molnár, Jean Sommer

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  15. The highest oxidation states of the transition metal elements

    Coordination Chemistry Reviews · 2008-07-31

    Sebastian Riedel, Martin Kaupp

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  16. Density-functional computation of 99Tc NMR chemical shifts

    Magnetic Resonance in Chemistry · 2008-10-14

    Michæl Bühl, Volodymyr Golubnychiy

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  17. Synthesis and X-ray Crystal Structure of (OsO3F2)2·2XeOF4 and the Raman Spectra of (OsO3F2)∞, (OsO3F2)2, and (OsO3F2)2·2XeOF4

    Inorganic Chemistry · 2009-04-14

    Michael J. Hughes, Hélène P. A. Mercier, Gary J. Schrobilgen

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  18. Fluoride Ion Donor Properties of cis-OsO2F4: Synthesis, Raman Spectroscopic Study, and X-ray Crystal Structure of [OsO2F3][Sb2F11]

    Inorganic Chemistry · 2009-12-01

    Michael J. Hughes, Hélène P. A. Mercier, Gary J. Schrobilgen

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  19. Syntheses and Multi-NMR Study offac- andmer-OsO3F2(NCCH3) and the X-ray Crystal Structure (n= 2) and Raman Spectrum (n= 0) offac-OsO3F2(NCCH3)·nCH3CN

    Inorganic Chemistry · 2010-04-12

    Michael J. Hughes, Michael Gerken, Hélène P. A. Mercier, Gary J. Schrobilgen

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  20. Preparation of Transition Metal Fluorides using ClF 3

    Unknown journal · 2012-10-14

    Ralf Haiges

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  21. Noble‐Gas Compounds

    Kirk-Othmer Encyclopedia of Chemical Technology · 2012-10-19

    Gary J. Schrobilgen, David S. Brock, Hélène P. A. Mercier

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  22. High-Valent Fluorides and Fluoro-Oxidizers

    Elsevier eBooks · 2013-01-01

    Sebastian Riedel

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  23. Noble-Gas Chemistry

    Elsevier eBooks · 2013-01-01

    David S. Brock, Gary J. Schrobilgen, Boris Žemva

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  24. Hexafluoridotechnetate(IV) Revisited

    Inorganic Chemistry · 2013-05-28

    Samundeeswari Mariappan Balasekaran, Matthias Johann Molski, Johann Spandl, Adelheid Hagenbach, Roger A. Alberto, Ulrich Abram

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  25. Polar Alignment of Λ-Shaped Basic Building Units within Transition Metal Oxide Fluoride Materials

    Inorganic Chemistry · 2013-12-12

    Michael A. Holland, Martin D. Donakowski, Eric A. Pozzi, Andrew M. Rasmussen, T. Thao Tran, Shannon E. Pease-Dodson, P. Shiv Halasyamani, Tamar Seideman, Richard P. Van Duyne, Kenneth Reinhard Poeppelmeier

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  26. [XeOXeOXe]2+, the Missing Oxide of Xenon(II); Synthesis, Raman Spectrum, and X-ray Crystal Structure of [XeOXeOXe][μ-F(ReO2F3)2]2

    Journal of the American Chemical Society · 2015-09-22

    Maria V. Ivanova, Hélène P. A. Mercier, Gary J. Schrobilgen

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  27. Trends in NMR chemical shifts of d0 transition metal compounds

    Journal of Organometallic Chemistry · 2017-03-31

    Zi‐Ling Xue, Tabitha M. Cook, Adam C. Lamb

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  28. The Reaction of Cs2[Tc(NO)F5] with BF3 in Acetonitrile: Formation and Structure of [{Tc(NO)(CH3CN)4}2(μ‐F)](BF4)3

    Zeitschrift für anorganische und allgemeine Chemie · 2017-08-24

    Samundeeswari Mariappan Balasekaran, Adelheid Hagenbach, Johann Spandl, Ulrich Abram

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  29. Chemistry at the Edge of the Periodic Table: The Importance of Periodic Trends on the Discovery of the Noble Gases and the Development of Noble-Gas Chemistry

    Structure and bonding · 2019-01-01

    Gary J. Schrobilgen

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  30. Bis(tetraphenylarsonium) hexafluoridotechnetate(IV) dihydrate: preparation, structure and spectroscopic analysis

    Acta Crystallographica Section C Structural Chemistry · 2019-11-14

    Samundeeswari Mariappan Balasekaran, Frédéric Poineau

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  31. Fluoride ion donor ability of binary fluorides towards the Lewis acids AsF5 and SbF5

    Journal of Fluorine Chemistry · 2022-12-10

    Zoran Mazej

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  32. Technetium ‐ The Unknown Center of the Periodic Table

    European Journal of Inorganic Chemistry · 2025-02-10

    Erik Strub, Désirée Badea, Jörn Bruns, Antonio Frontera, Natalia Mayordomo, A. P. Sakhonenkova, Maximilian Roca Jungfer, Mathias Siegfried Wickleder, Clarence Yong, Markus Zegke

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