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RESEARCH PAPER · Nature Catalysis · 2019

Structure of the catalytically active copper–ceria interfacial perimeter

Aling Chen, Xiaojuan Yu, Yan Zhou, Shu Miao, Yong Li, Sebastian Kuld, Jens Sehested, Jingyue Liu, Toshihiro Aoki, Song Ki Hong, Matteo Farnesi Camellone, Stefano Fabris, Jing Ning, Chuanchuan Jin, Chengwu Yang, Alexei Nefedov, Christof H. Wöll, Yuemin Wang, Wenjie Shen

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Structure of the catalytically active copper–ceria interfacial perimeterOriginalDesign strategies toward catalytic materials and cathode structures for emerging Li–CO 2 batteries104Insights into interface engineering in steam reforming reactions for hydrogen production166Oxygen Vacancy Generation and Stabilization in CeO 2– x by Cu Introduction with Improved CO 2 Photocatalytic Reduction Activity586New Strategies for the Preparation of Sinter‐Resistant Metal‐Nanoparticle‐Based Catalysts384Catalytic CO Oxidation by Gas-Phase Metal Oxide Clusters63Realizing Interfacial Electronic Interaction within ZnS Quantum Dots/N‐rGO Heterostructures for Efficient Li–CO 2 Batteries145In Situ FTIR-Assisted Synthesis of Nickel Hexacyanoferrate Cathodes for Long-Life Sodium-Ion Batteries77A Novel Approach to High‐Performance Aliovalent‐Substituted Catalysts—2D Bimetallic MOF‐Derived CeCuOx Microsheets64Controlling Dynamic Structural Transformation of Atomically Dispersed CuOx Species and Influence on Their Catalytic Performances85Selective Hydrogenation over Supported Metal Catalysts: From Nanoparticles to Single Atoms1609Unraveling the coordination structure-performance relationship in Pt1/Fe2O3 single-atom catalyst457Construction of Active Site in a Sintered Copper–Ceria Nanorod Catalyst172Polar surface structure of oxide nanocrystals revealed with solid-state NMR spectroscopy70Asymmetric Oxygen Vacancies: the Intrinsic Redox Active Sites in Metal Oxide Catalysts404Fabrication of layered double hydroxide microcapsules mediated by cerium doping in metal–organic frameworks for boosting water splitting219Theoretical insights into single-atom catalysts463Elucidating the Nature of the Cu(I) Active Site in CuO/TiO2 for Excellent Low-Temperature CO Oxidation93Electronic and geometric structure of the copper-ceria interface on Cu/CeO2 catalysts95Recent Advances on the Rational Design of Non-Precious Metal Oxide Catalysts Exemplified by CuOx/CeO2 Binary System: Implications of Size, Shape and Electronic Effects on Intrinsic Reactivity and Metal-Support Interactions87High-performance of Cu-TiO2 for photocatalytic oxidation of formaldehyde under visible light and the mechanism study165Heterostructured NiS 2 /ZnIn 2 S 4 Realizing Toroid-like Li 2 O 2 Deposition in Lithium–Oxygen Batteries with Low-Donor-Number Solvents159Highly efficient Cu/CeO2-hollow nanospheres catalyst for the reverse water-gas shift reaction: Investigation on the role of oxygen vacancies through in situ UV-Raman and DRIFTS131Electrocatalytic oxidation of methane to ethanol via NiO/Ni interface148Manipulating Atomic Structures at the Au/TiO2 Interface for O2 Activation139Copper-ceria solid solution with improved catalytic activity for hydrogenation of CO2 to CH3OH89Engineering Platinum–Oxygen Dual Catalytic Sites via Charge Transfer towards Highly Efficient Hydrogen Evolution86Metal-support interaction for heterogeneous catalysis: from nanoparticles to single atoms199Deep Understanding of Strong Metal Interface Confinement: A Journey of Pd/FeOx Catalysts151ZrO2-x modified Cu nanocatalysts with synergistic catalysis towards carbon-oxygen bond hydrogenation146Strong Oxide–Support Interactions Accelerate Selective Dehydrogenation of Propane by Modulating the Surface Oxygen68Coverage‐Dependent Behaviors of Vanadium Oxides for Chemical Looping Oxidative Dehydrogenation105Supported Metal Clusters: Fabrication and Application in Heterogeneous Catalysis505Surface Refaceting Mechanism on Cubic Ceria80Mechanism and Nature of Active Sites for Methanol Synthesis from CO/CO2 on Cu/CeO2240Tracking the formation, fate and consequence for catalytic activity of Pt single sites on CeO2415Hierarchical Echinus-like Cu-MFI Catalysts for Ethanol Dehydrogenation137Engineering Pt-Mn2O3 interface to boost selective oxidation of ethylene glycol to glycolic acid107Operando Investigation of Toluene Oxidation over 1D Pt@CeO 2 Derived from Pt Cluster-Containing MOF254Fully Exposed Cluster Catalyst (FECC): Toward Rich Surface Sites and Full Atom Utilization Efficiency305Atomic-level insight into reasonable design of metal-based catalysts for hydrogen oxidation in alkaline electrolytes143Lattice oxygen self-spillover on reducible oxide supported metal cluster: the water–gas shift reaction on Cu/CeO 2 catalyst62The catalytic dehydrogenation of ethanol by heterogeneous catalysts79Critical Roles of Surface Oxygen Vacancy in Heterogeneous Catalysis over Ceria-based Materials: A Selected Review63Enhanced Ammonia Synthesis Activity of Ceria-Supported Ruthenium Catalysts Induced by CO Activation114Controlled Synthesis of Cu 0 /Cu 2 O for Efficient Photothermal Catalytic Conversion of CO 2 and H 2 O86Improving the ammonia synthesis activity of Ru/CeO2 through enhancement of the metal–support interaction81Flame Synthesis of Cu/ZnO–CeO 2 Catalysts: Synergistic Metal–Support Interactions Promote CH 3 OH Selectivity in CO 2 Hydrogenation172Ru surface density effect on ammonia synthesis activity and hydrogen poisoning of ceria-supported Ru catalysts64Defect Engineering on CeO 2 ‐Based Catalysts for Heterogeneous Catalytic Applications244Boosting the Catalytic Performance of CeO 2 in Toluene Combustion via the Ce–Ce Homogeneous Interface149Uncovering the Promotion of CeO 2 /CoS 1.97 Heterostructure with Specific Spatial Architectures on Oxygen Evolution Reaction209Nanoscale Cerium Oxide: Synthesis, Biocatalytic Mechanism, and Applications60In Situ Raman Observation of Oxygen Activation and Reaction at Platinum–Ceria Interfaces during CO Oxidation156Understanding and Application of Strong Metal–Support Interactions in Conversion of CO 2 to Methanol: A Review88Engineering catalyst supports to stabilize PdOx two-dimensional rafts for water-tolerant methane oxidation229Engineering the Cu/Mo2CTx (MXene) interface to drive CO2 hydrogenation to methanol309Atomically Dispersed Heteronuclear Dual‐Atom Catalysts: A New Rising Star in Atomic Catalysis177Effect of the Configuration of Copper Oxide–Ceria Catalysts in NO Reduction with CO: Superior Performance of a Copper–Ceria Solid Solution60Regulating surface oxygen species on copper (I) oxides via plasma treatment for effective reduction of nitrate to ammonia282Boosting CO 2 electroreduction towards C 2+ products via CO* intermediate manipulation on copper-based catalysts66Optimization of nano-catalysts for application in compact reformers73Support stabilized PtCu single-atom alloys for propane dehydrogenation89Customizable CO2 Electroreduction to C1 or C2+ Products through Cuy/CeO2 Interface Engineering112Active Cu0–Cuσ+ Sites for the Hydrogenation of Carbon–Oxygen Bonds over Cu/CeO2 Catalysts175Selective and stable upgrading of biomass-derived furans into plastic monomers by coupling homogeneous and heterogeneous catalysis60The lanthanide doping effect on toluene catalytic oxidation over Pt/CeO2 catalyst70Interfacial compatibility critically controls Ru/TiO2 metal-support interaction modes in CO2 hydrogenation370Induced activation of the commercial Cu/ZnO/Al2O3 catalyst for the steam reforming of methanol516Co-promotion of two-type active sites: PtCu single-atom alloy and copper-ceria interface for preferential oxidation of CO64Partially sintered copper‒ceria as excellent catalyst for the high-temperature reverse water gas shift reaction370Designing Sites in Heterogeneous Catalysis: Are We Reaching Selectivities Competitive With Those of Homogeneous Catalysts?424Crystal-Phase-Mediated Restructuring of Pt on TiO 2 with Tunable Reactivity: Redispersion versus Reshaping99Supported Sub‐Nanometer Clusters for Electrocatalysis Applications74Defects engineering simultaneously enhances activity and recyclability of MOFs in selective hydrogenation of biomass109Identification of Active Sites in HCHO Oxidation over TiO2-Supported Pt Catalysts67Synergistic effect of Cu+ single atoms and Cu nanoparticles supported on alumina boosting water-gas shift reaction72Catalytically efficient Ni-NiOx-Y2O3 interface for medium temperature water-gas shift reaction84Selective CO 2 Photoreduction to CH 4 via Pd δ + ‐Assisted Hydrodeoxygenation over CeO 2 Nanosheets145Grain Boundary‐Derived Cu+/Cu0 Interfaces in CuO Nanosheets for Low Overpotential Carbon Dioxide Electroreduction to Ethylene131Defect Engineering of Ceria Nanocrystals for Enhanced Catalysis via a High-Entropy Oxide Strategy103Static and dynamic quantification tracking of asymmetric oxygen vacancies in copper-ceria catalysts with superior catalytic activity99Effective Ensemble of Pt Single Atoms and Clusters over the (Ni,Co)(OH) 2 Substrate Catalyzes Highly Selective, Efficient, and Stable Hydrogenation Reactions59Single-Atom Ce-Modified α-Fe 2 O 3 for Selective Catalytic Reduction of NO with NH 3153Homogeneity of Supported Single‐Atom Active Sites Boosting the Selective Catalytic Transformations115Boosting Electrochemical CO 2 Reduction to Methane via Tuning Oxygen Vacancy Concentration and Surface Termination on a Copper/Ceria Catalyst126Weakening the Metal–Support Interactions of M/CeO 2 (M = Co, Fe, Ni) Using a NH 3 -Treated CeO 2 Support for an Enhanced Water–Gas Shift Reaction73Ensemble effect for single-atom, small cluster and nanoparticle catalysts429Sustainable production of hydrogen with high purity from methanol and water at low temperatures163Ptn–Ov synergistic sites on MoOx/γ-Mo2N heterostructure for low-temperature reverse water–gas shift reaction155Engineering Cu+/CeZrO interfaces to promote CO2 hydrogenation to methanol92Tuning the C 1 /C 2 Selectivity of Electrochemical CO 2 Reduction on Cu–CeO 2 Nanorods by Oxidation State Control85Boosting the Activity of Pd Single Atoms by Tuning Their Local Environment on Ceria for Methane Combustion63Negatively Charged Single-Atom Pt Catalyst Shows Superior SO2 Tolerance in NOx Reduction by CO95Titania-Morphology-Dependent Pt–TiO2 Interfacial Catalysis in Water-Gas Shift Reaction64The Nature of Interfacial Catalysis over Pt/NiAl 2 O 4 for Hydrogen Production from Methanol Reforming Reaction103Construction of CuO/CeO 2 Catalysts via the Ceria Shape Effect for Selective Catalytic Oxidation of Ammonia296Reversible Transformation and Distribution Determination of Diverse Pt Single-Atom Species65Dynamic Reconstitution Between Copper Single Atoms and Clusters for Electrocatalytic Urea Synthesis364Scalable synthesis of Cu clusters for remarkable selectivity control of intermediates in consecutive hydrogenation93Gas-Dependent Active Sites on Cu/ZnO Clusters for CH3OH Synthesis106Adsorption of Molecules on Defective CeO 2 for Advanced Catalysis76Lamella-heterostructured nanoporous bimetallic iron-cobalt alloy/oxyhydroxide and cerium oxynitride electrodes as stable catalysts for oxygen evolution188Defects Tune the Strong Metal–Support Interactions in Copper Supported on Defected Titanium Dioxide Catalysts for CO 2 Reduction200Metal Oxide Aerogels: A New Horizon for Stabilizing Anodes in Rechargeable Zinc Metal Batteries69For more and purer hydrogen-the progress and challenges in water gas shift reaction81Interfacial Synergy between the Cu Atomic Layer and CeO 2 Promotes CO Electrocoupling to Acetate72Concerted oxygen diffusion across heterogeneous oxide interfaces for intensified propane dehydrogenation64Surface modification of Cu2O with stabilized Cu+ for highly efficient and stable CO2 electroreduction to C2+ chemicals69Mechanism of the Periodic Unsteady-State Water–Gas Shift Reaction on Highly Dispersed Cu-Loaded CeO2 Catalysts61Size of cerium dioxide support nanocrystals dictates reactivity of highly dispersed palladium catalysts327Recent Advances on Heterogeneous Non-noble Metal Catalysts toward Selective Hydrogenation Reactions164VOC Bonding of Heterointerface Boosting Kinetics of Free‐Standing Na5V12O32 Cathode for Ultralong Lifespan Sodium‐Ion Batteries81Asymmetric oxygen vacancy-enriched Mn2O3@CeO2 for NO oxidation with excellent low-temperature activity and boosted SO2-resistance74Tuning Oxygen Vacancies in Oxides by Configurational Entropy103Engineering metal-support interaction to construct catalytic interfaces and redisperse metal nanoparticles92Light-Reinforced Key Intermediate for Anticoking To Boost Highly Durable Methane Dry Reforming over Single Atom Ni Active Sites on CeO268Diving into the interface-mediated Mars-van Krevelen (M−vK) characteristic of CuOx-supported CeO2 catalysts63Photochromic single atom Ag/TiO 2 catalysts for selective CO 2 reduction to CH 4208Enhancement of Nitrate‐to‐Ammonia on Amorphous CeOx‐Modified Cu via Tuning of Active Hydrogen Supply122Highly Stable Pt/CeO 2 Catalyst with Embedding Structure toward Water–Gas Shift Reaction237Catalyst architecture for metal–support interactions and its effects on heterogeneous reactions72Understanding the Synergistic Catalysis in Hydrogenation of Carbonyl Groups on Cu-Based Catalysts87Insight into the extremely different catalytic behaviors of asymmetric and symmetric oxygen vacancies for peroxymonosulfate activation108Tuning oxidant and antioxidant activities of ceria by anchoring copper single-site for antibacterial application182Assembling an S-type heterojunction comprising vacancy-rich CeO2-x and CuBi2O4 for improved photocatalytic oxidation of gaseous toluene57A Ce-CuZn catalyst with abundant Cu/Zn-OV-Ce active sites for CO2 hydrogenation to methanol239Structured Catalysts and Catalytic Processes: Transport and Reaction Perspectives140Facilitating the dry reforming of methane with interfacial synergistic catalysis in an Ir@CeO2−x catalyst209Electrocatalysts with Highly Dispersed Cerium in Nickel Matrix for Hydrogen Evolution in Alkaline Electrolyte69Concentrated solar CO2 reduction in H2O vapour with >1% energy conversion efficiency102Strong metal-support interaction (SMSI) in environmental catalysis: Mechanisms, application, regulation strategies, and breakthroughs99Highly Selective Electrocatalytic CO2 Conversion to Tailored Products through Precise Regulation of Hydrogenation and C–C Coupling155Turning copper into an efficient and stable CO evolution catalyst beyond noble metals68Thermochemical CO 2 Reduction to Methanol over Metal-Based Single-Atom Catalysts (SACs): Outlook and Challenges for Developments101Atmosphere Induces Tunable Oxygen Vacancies to Stabilize Single‐Atom Copper in Ceria for Robust Electrocatalytic CO 2 Reduction to CH 4114Hydroxylated TiO2-induced high-density Ni clusters for breaking the activity-selectivity trade-off of CO2 hydrogenation91Inverse ceria-nickel catalyst for enhanced C–O bond hydrogenolysis of biomass and polyether61Direct cleavage of C=O double bond in CO2 by the subnano MoOx surface on Mo2N58Active Interfacial Perimeter in Pt/CeO 2 Catalysts with Embedding Structure for Water-Tolerant Toluene Combustion58Ru‐O V Site‐Mediated Product Selectivity Switch for Overall Photocatalytic CO 2 Reduction81Highly dispersed Cu on hollow spherical CeO2: An efficient and stable catalyst for the RWGS reaction66Cuproptosis: mechanisms and nanotherapeutic strategies in cancer and beyond90Interfacial Oxygen Vacancy‐Copper Pair Sites on Inverse CeO 2 /Cu Catalyst Enable Efficient CO 2 Electroreduction to Ethanol in Acid66Interfacial Catalysis at Atomic Level159Ultrastable supported oxygen evolution electrocatalyst formed by ripening-induced embedding378Manipulating hydrogenation pathways enables economically viable electrocatalytic aldehyde-to-alcohol valorization73Amyloid‐Templated Ceria Nanozyme Reinforced Microneedle for Diabetic Wound Treatments110Boosting ammonia electrosynthesis via interfacial tandem nitrate reduction enabled by an amorphous@crystalline electrocatalyst58Dynamic modulation of electron redistribution at the heterogeneous interface nickel hydroxides/platinum boosts acidic oxygen reduction reaction82Interfacial compatibility critically controls Ru/TiO2 metal-support interaction modes in CO2 hydrogenation281

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