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RESEARCH PAPER · ACS Omega · 2018

Lepidocrocite-Type Titanate Formation from Isostructural Prestructures under Hydrothermal Reactions: Observation by Synchrotron X-ray Total Scattering Analyses

Satoshi Tominaka, Hiroki Yamada, Satoshi Hiroi, Saori Imada Kawaguchi, Koji Ohara

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Lepidocrocite-Type Titanate Formation from Isostructural Prestructures under Hydrothermal Reactions: Observation by Synchrotron X-ray Total Scattering AnalysesOriginalZeolitic intralayer microchannels of magadiite, a natural layered silicate, to boost green organic synthesis43Time-resolved pair distribution function analysis of disordered materials on beamlines BL04B2 and BL08W at SPring-861Condensed ferric dimers for green photocatalytic synthesis of nylon precursors20Electrical Conduction in Curved Hexagonal Borophane0Mechanisms for Tungsten Oxide Nanoparticle Formation in Solvothermal Synthesis: From Polyoxometalates to Crystalline Materials51Structural Evolution of Amorphous Precursors toward Crystalline Zeolites Visualized by an in Situ X-ray Pair Distribution Function Approach41Geometrical Frustration of B-H Bonds in Layered Hydrogen Borides Accessible by Soft Chemistry77In situ synchrotron pair distribution function analysis to monitor synthetic pathways under electromagnetic excitation16Structural Analysis of Sucrose-Derived Hard Carbon and Correlation with the Electrochemical Properties for Lithium, Sodium, and Potassium Insertion313Observation of Liquid Phase Synthesis of Sulfide Solid Electrolytes Using Time‐Resolved Pair Distribution Function Analysis7Phase Identification of Crystal Precipitated from Molten CaO–SiO2–FeOx–P2O5 Slag by High Temperature In-situ X-ray Diffraction17Far-from-equilibrium effects of electric and electromagnetic fields in ceramics synthesis and processing19Bridging Structural Inhomogeneity to Functionality: Pair Distribution Function Methods for Functional Materials Development102In situ Blue titania via band shape engineering for exceptional solar H2 production in rutile TiO278High-energy x-ray diffraction study on phase transition asymmetry of plastic crystal neopentylglycol3In situ scattering studies of material formation during wet-chemical syntheses1Sodium insertion and de-insertion mechanism of spinel-type sodium titanium oxide studied by in situ XRD9Local structure determination using total scattering data12Distinctive Ce 3+ luminescence from single-crystalline and glassy Ce:LaB 3 O 64On the Structure of One-Dimensional TiO 2 Lepidocrocite1Solvothermal synthesis of soluble, surface modified anatase and transition metal doped anatase hybrid nanocrystals5Effect of Glass Composition on Luminescence and Structure of CsPbBr3 Quantum Dots in an Amorphous Matrix12Ultrafast Nanocrystallization of BaF2 in Oxyfluoride Glasses with Crystal-like Nanostructures: Implications for Upconversion Fiber Devices16Self‐Straining Nanocrystals Strategy: Temperature and Pressure Co‐Induced Phase Transitions of CsPbBr3 in Amorphous Matrices11On the structure of one-dimensional TiO2 lepidocrocite49Improving Electrochemical Activity of P2‐type Na2/3Mn2/3Ni1/3O2 by Controlling its Crystallinity2Tracking Sub-Nano-Scale Structural Evolution in Zeolite Synthesis by In Situ High-Energy X-ray Total Scattering Measurement with Pair Distribution Function Analysis45Influence of precursor structure on the formation of tungsten oxide polymorphs0In situ Raman and X-ray scattering of a single supersaturated aqueous Mg(NO3)2 droplet ultrasonically levitated5Atom-Selective Analyses Reveal the Structure-Directing Effect of Cs Cation on the Synthesis of Zeolites12Influence of precursor structure on the formation of tungsten oxide polymorphs1One-dimensional, titania-based lepidocrocite nanofilaments and their self-assembly33Structure of Single Aqueous MgSO4 Droplets Ultrasonically Levitated in the Air: Supersaturation and Crystallization3Origin of High Activity and Durability of Confined Ordered Intermetallic PtCo Catalysts for the Oxygen Reduction Reaction in Rotating Disk Electrode and Fuel Cell Operating Conditions35Influence of the Precursor Structure on the Formation of Tungsten Oxide Polymorphs14Development of negative TiO2-based electrodes by soft chemistry for aqueous proton ions batteries0Structural insights and electronic state analysis of PtNi nanowire catalysts by operando high-energy resolution fluorescence detection X-ray absorption spectroscopy11In situ structural characterization of Li3PS4 solid electrolytes under high pressure4Experimental Elucidation of a Cubane Water Cluster in the Hydrophobic Cavity of UiO‐662A Modified Galvanic Cell Synthesis of Pd@Pt Core–Shell Nanowire Catalysts: Structural Insights and Enhanced ORR Performance5Application of X‐ray Pair Distribution Function to Batteries3Structure–Activity Relationship in PtCo L10 Ordered Phase ORR Catalysts: Pt-Rich Shell Having Anisotropic Lattice Distortion Revealed by PDF and XAS Analysis16Impact of Temperature on Zeolitization Elucidated by In Situ High-Energy X-ray Total Scattering Measurement9Stepwise Topochemical Linkage of Zirconium Oxo Clusters to Yield Black Zirconia Nanocrystals1Local structural evolutions of the Na 2 / 3 (Mn 2 / 3 Ni 1 / 3 )O 2 with two different crystallinities during Na extraction/insertion using in situ PDF analysis4Comparison of the Arrhenius parameters between conventional hydrothermal and microwave-assisted synthesis methods for tin oxide nanoparticles0Impact of ZnO on CsPbBr3 nanocrystals in fluorophosphate glasses by in situ multi-spectroscopy measurement1Antibacterial Activity of Quantum-Confined One-Dimensional Titanate Nanofilaments0Configurational Entropy Engineering of Bi‑Doped Glass Fiber Enabling Ultrabroadband Emission0Unveiling the Structure and Properties Evolution of Nd 3+ ‐Doped Phosphate Glass with Substitution of SiO 2 by P 2 O 50

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  1. Zeolitic intralayer microchannels of magadiite, a natural layered silicate, to boost green organic synthesis

    Chemical Science · 2018-01-01

    Yusuke Ide, Satoshi Tominaka, Hiroyuki Kono, Rahul Ram, Akihiko Machida, Nao Tsunoji

    Read original paper ↗ ·

  2. Time-resolved pair distribution function analysis of disordered materials on beamlines BL04B2 and BL08W at SPring-8

    Journal of Synchrotron Radiation · 2018-09-26

    Koji Ohara, Satoshi Tominaka, Hiroki Yamada, Masakuni Takahashi, Hiroshi Yamaguchi, Futoshi Utsuno, Takashi Umeki, Atsushi Yao, Kengo Nakada, Michitaka Takemoto, Satoshi Hiroi, Naruki Tsuji, Toru Wakihara

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  3. Condensed ferric dimers for green photocatalytic synthesis of nylon precursors

    Chemical Science · 2019-01-01

    Yusuke Ide, Satoshi Tominaka, Yumi Yoneno, Kenji Komaguchi, Toshiaki Takei, Hidechika Nishida, Nao Tsunoji, Akihiko Machida, Tsuneji Sano

    Read original paper ↗ ·

  4. Electrical Conduction in Curved Hexagonal Borophane

    SSRN Electronic Journal · 2019-01-01

    Satoshi Tominaka, Ryota Ishibiki, Asahi Fujino, Kohsaku Kawakami, Koji Ohara, Iwao Matsuda, Hideo Hosono, Takahiro Kondo

    Read original paper ↗ ·

  5. Mechanisms for Tungsten Oxide Nanoparticle Formation in Solvothermal Synthesis: From Polyoxometalates to Crystalline Materials

    The Journal of Physical Chemistry C · 2019-02-06

    Mikkel Juelsholt, Troels Lindahl Christiansen, Kirsten M. Ø. Jensen

    Read original paper ↗ ·

  6. Structural Evolution of Amorphous Precursors toward Crystalline Zeolites Visualized by an in Situ X-ray Pair Distribution Function Approach

    The Journal of Physical Chemistry C · 2019-10-21

    Hiroki Yamada, Satoshi Tominaka, Koji Ohara, Zhendong Liu, Tatsuya Okubo, Toru Wakihara

    Read original paper ↗ ·

  7. Geometrical Frustration of B-H Bonds in Layered Hydrogen Borides Accessible by Soft Chemistry

    Chem · 2019-12-09

    Satoshi Tominaka, Ryota Ishibiki, Asahi Fujino, Kohsaku Kawakami, Koji Ohara, Takuya Masuda, Iwao Matsuda, Hideo Hosono, Takahiro Kondo

    Read original paper ↗ ·

  8. In situ synchrotron pair distribution function analysis to monitor synthetic pathways under electromagnetic excitation

    Journal of Materials Chemistry A · 2020-01-01

    Nathan Nakamura, Laisuo Su, Jianming Bai, Sanjit Ghose, B. Reeja‐Jayan

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  9. Structural Analysis of Sucrose-Derived Hard Carbon and Correlation with the Electrochemical Properties for Lithium, Sodium, and Potassium Insertion

    Chemistry of Materials · 2020-03-03

    Kei Kubota, Saori Shimadzu, Naoaki Yabuuchi, Satoshi Tominaka, Soshi Shiraishi, Maria A. Abreu-Sepulveda, Ayyakkannu Manivannan, Kazuma Gotoh B, Mika Fukunishi, Mouad Dahbi, Shinichi Komaba

    Read original paper ↗ ·

  10. Observation of Liquid Phase Synthesis of Sulfide Solid Electrolytes Using Time‐Resolved Pair Distribution Function Analysis

    physica status solidi (b) · 2020-06-09

    Koji Ohara, Naoya Masuda, Hiroshi Yamaguchi, Atsushi Yao, Satoshi Tominaka, Hiroki Yamada, Satoshi Hiroi, Masakuni Takahashi, Kentaro Yamamoto, Toru Wakihara, Yoshiharu Uchimoto, Futoshi Utsuno, Shigeru Kimura

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  11. Phase Identification of Crystal Precipitated from Molten CaO–SiO2–FeOx–P2O5 Slag by High Temperature In-situ X-ray Diffraction

    ISIJ International · 2020-12-15

    Masanori Suzuki, Honami Serizawa, Norimasa Umesaki

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  12. Far-from-equilibrium effects of electric and electromagnetic fields in ceramics synthesis and processing

    MRS Bulletin · 2021-01-01

    B. Reeja‐Jayan, Jian Luo

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  13. Bridging Structural Inhomogeneity to Functionality: Pair Distribution Function Methods for Functional Materials Development

    Advanced Science · 2021-01-22

    He Sun Zhu, Yalan Huang, Jincan Ren, Binghao Zhang, Yubin Ke, Alex K.‐Y. Jen, Qiang Zhang, Xun‐Li Wang, Qi Liu

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  14. In situ Blue titania via band shape engineering for exceptional solar H2 production in rutile TiO2

    Applied Catalysis B: Environmental · 2021-05-19

    Esmail Doustkhah, M. Hussein N. Assadi, Kenji Komaguchi, Nao Tsunoji, Mohamed Esmat, Naoki Fukata, Osamu Tomita, Ryu Abe, Bunsho Ohtani, Yusuke Ide

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  15. High-energy x-ray diffraction study on phase transition asymmetry of plastic crystal neopentylglycol

    Chinese Physics B · 2021-07-14

    Zhe Zhang, Yanna Chen, Ji Qi, Zhao Zhang, Koji Ohara, Osami Sakata, Zhang Zhi-dong, Bing Li

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  16. In situ scattering studies of material formation during wet-chemical syntheses

    Elsevier eBooks · 2021-08-04

    Susanne Linn Skjærvø, Mikkel Juelsholt, Kirsten M. Ø. Jensen

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  17. Sodium insertion and de-insertion mechanism of spinel-type sodium titanium oxide studied by in situ XRD

    Journal of Alloys and Compounds · 2021-08-30

    Riki Kataoka, Toshikatsu Kojima, Mitsunori Kitta, Akihiko Machida

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  18. Local structure determination using total scattering data

    Elsevier eBooks · 2021-10-28

    Simon J. L. Billinge, Sandra Helen Skjærvø, Maxwell W. Terban, Songsheng Tao, Long Yang, Yevgeny Rakita, Benjamin A. Frandsen

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  19. Distinctive Ce 3+ luminescence from single-crystalline and glassy Ce:LaB 3 O 6

    Journal of Materials Chemistry C · 2022-01-01

    Dongsheng Yuan, Encarnación G. Vı́llora, Satoshi Tominaka, Kiyoshi Shimamura

    Read original paper ↗ ·

  20. On the Structure of One-Dimensional TiO 2 Lepidocrocite

    SSRN Electronic Journal · 2022-01-01

    Hussein O. Badr, Francisco Lagunas, Daniel Autry, Jacob H. Cope, Takayuki Kono, Robert F. Klie, Yong‐Jie Hu, Michel W. Barsoum

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  21. Solvothermal synthesis of soluble, surface modified anatase and transition metal doped anatase hybrid nanocrystals

    Nanoscale Advances · 2022-01-01

    A. S. Bathe, Adrián Sanz Arjona, Annie Regan, C. Wallace, C. R. Nerney, Niaobh M. O'Donoghue, James M. Crosland, Tigran Simonian, Richard I. Walton, Peter W. Dunne

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  22. Effect of Glass Composition on Luminescence and Structure of CsPbBr3 Quantum Dots in an Amorphous Matrix

    Materials · 2022-02-23

    Ruilin Zheng, Jumpei Ueda, Kenji Shinozaki, Setsuhisa Tanabe

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  23. Ultrafast Nanocrystallization of BaF2 in Oxyfluoride Glasses with Crystal-like Nanostructures: Implications for Upconversion Fiber Devices

    ACS Applied Nano Materials · 2022-03-02

    Kenji Shinozaki, Yoshiki Ishii, Sohei Sukenaga, Koji Ohara

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  24. Self‐Straining Nanocrystals Strategy: Temperature and Pressure Co‐Induced Phase Transitions of CsPbBr3 in Amorphous Matrices

    Advanced Optical Materials · 2022-05-20

    Ruilin Zheng, Jumpei Ueda, Jiyao Li, Kenji Shinozaki, Zeyu Fan, Satoshi Horike, Setsuhisa Tanabe

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  25. On the structure of one-dimensional TiO2 lepidocrocite

    Matter · 2022-11-02

    Hussein O. Badr, Francisco Lagunas, Daniel Autrey, Jacob H. Cope, Takayuki Kono, Takeshi Torita, Robert F. Klie, Yong‐Jie Hu, Michel W. Barsoum

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  26. Improving Electrochemical Activity of P2‐type Na2/3Mn2/3Ni1/3O2 by Controlling its Crystallinity

    Batteries & Supercaps · 2022-12-01

    Riki Kataoka, Noboru Taguchi, Kohei Tada, Akihiko Machida, Nobuhiko Takeichi

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  27. Tracking Sub-Nano-Scale Structural Evolution in Zeolite Synthesis by In Situ High-Energy X-ray Total Scattering Measurement with Pair Distribution Function Analysis

    Journal of the American Chemical Society · 2022-12-16

    Ayano Minami, Peidong Hu, Yuki Sada, Hiroki Yamada, Koji Ohara, Yasuo Yonezawa, Yukichi Sasaki, Yutaka Yanaba, Masanori Takemoto, Yuki Yoshida, Tatsuya Okubo, Toru Wakihara

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  28. Influence of precursor structure on the formation of tungsten oxide polymorphs

    ChemRxiv · 2023-02-10

    Mikkel Juelsholt, Olivia Aalling‐Frederiksen, Troels Lindahl Christiansen, Emil T. S. Kjær, Niels Lefeld, Andrea Kirsch, Kirsten M. Ø. Jensen

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  29. In situ Raman and X-ray scattering of a single supersaturated aqueous Mg(NO3)2 droplet ultrasonically levitated

    Analytical Sciences · 2023-03-01

    Toshio Yamaguchi, Natsuki Hata, Shun-ichiro Matsuo, Kōji Yoshida, Tsutomu Kurisaki, Shoji Ishizaka, Koji Ohara

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  30. Atom-Selective Analyses Reveal the Structure-Directing Effect of Cs Cation on the Synthesis of Zeolites

    The Journal of Physical Chemistry Letters · 2023-04-05

    Hiroki Yamada, Hirofumi Horikawa, Chokkalingam Anand, Koji Ohara, Toshiaki Ina, Akihiko Machida, Satoshi Tominaka, Tatsuya Okubo, Zhendong Liu, Kenta Iyoki, Toru Wakihara

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  31. Influence of precursor structure on the formation of tungsten oxide polymorphs

    ChemRxiv · 2023-04-11

    Mikkel Juelsholt, Olivia Aalling‐Frederiksen, Troels Lindahl Christiansen, Emil T. S. Kjær, Niels Lefeld, Andrea Kirsch, Kirsten M. Ø. Jensen

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  32. One-dimensional, titania-based lepidocrocite nanofilaments and their self-assembly

    Matter · 2023-07-05

    Kaustubh Sudhakar, Avishek Karmakar, Hussein O. Badr, Tarek Ali El-Melegy, Mary Qin Hassig, Michael S. Carey, Stefan Masiuk, Liyan Wu, Qian Qian, Takayuki Kono, Christopher Y. Li, Michel W. Barsoum

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  33. Structure of Single Aqueous MgSO4 Droplets Ultrasonically Levitated in the Air: Supersaturation and Crystallization

    Journal of Solution Chemistry · 2023-08-01

    Toshio Yamaguchi, Shun-ichiro Matsuo, Kōji Yoshida, Tsutomu Kurisaki, Shoji Ishizaka, Koji Ohara

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  34. Origin of High Activity and Durability of Confined Ordered Intermetallic PtCo Catalysts for the Oxygen Reduction Reaction in Rotating Disk Electrode and Fuel Cell Operating Conditions

    ACS Catalysis · 2023-08-04

    Yunfei Gao, Tomoki Uchiyama, Kentaro Yamamoto, Toshiki Watanabe, Satoshi Tominaka, Neha Thakur, Ryota Sato, Toshiharu Teranishi, Hideto Imai, Y. Sakurai, Yoshiharu Uchimoto

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  35. Influence of the Precursor Structure on the Formation of Tungsten Oxide Polymorphs

    Inorganic Chemistry · 2023-09-01

    Mikkel Juelsholt, Olivia Aalling‐Frederiksen, Troels Lindahl Christiansen, Emil T. S. Kjær, Niels Lefeld, Andrea Kirsch, Kirsten M. Ø. Jensen

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  36. Development of negative TiO2-based electrodes by soft chemistry for aqueous proton ions batteries

    Unknown journal · 2023-11-20

    Milad Toorabally

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  37. Structural insights and electronic state analysis of PtNi nanowire catalysts by operando high-energy resolution fluorescence detection X-ray absorption spectroscopy

    Journal of Materials Chemistry A · 2024-01-01

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  38. In situ structural characterization of Li3PS4 solid electrolytes under high pressure

    Journal of Solid State Electrochemistry · 2024-04-15

    Atsushi Yao, Shogo Kadota, Satoshi Hiroi, Hiroki Yamada, Jochi Tseng, Seiya Shimono, Futoshi Utsuno, Koji Ohara

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  39. Experimental Elucidation of a Cubane Water Cluster in the Hydrophobic Cavity of UiO‐66

    ChemPhysChem · 2024-08-26

    Kazutaka Sonobe, Satoshi Tominaka, Akihiko Machida

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  40. A Modified Galvanic Cell Synthesis of Pd@Pt Core–Shell Nanowire Catalysts: Structural Insights and Enhanced ORR Performance

    ACS Applied Energy Materials · 2024-09-13

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  41. Application of X‐ray Pair Distribution Function to Batteries

    Unknown journal · 2024-12-13

    Chong Chen

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  42. Structure–Activity Relationship in PtCo L10 Ordered Phase ORR Catalysts: Pt-Rich Shell Having Anisotropic Lattice Distortion Revealed by PDF and XAS Analysis

    ACS Applied Materials & Interfaces · 2025-05-16

    Yunfei Gao, Mukesh Kumar, Neha Thakur, Weijie Cao, Toshiki Watanabe, Satoshi Tominaka, Kazutaka Sonobe, Akihiko Machida, Ryota Sato, Toshiharu Teranishi, Masashi Matsumoto, Hideto Imai, Tomoya Uruga, Yoshiharu Sakurai, Yoshiharu Uchimoto

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  43. Impact of Temperature on Zeolitization Elucidated by In Situ High-Energy X-ray Total Scattering Measurement

    Journal of the American Chemical Society · 2025-07-05

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  44. Stepwise Topochemical Linkage of Zirconium Oxo Clusters to Yield Black Zirconia Nanocrystals

    Crystal Growth & Design · 2025-12-01

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  45. Local structural evolutions of the Na 2 / 3 (Mn 2 / 3 Ni 1 / 3 )O 2 with two different crystallinities during Na extraction/insertion using in situ PDF analysis

    Electrochimica Acta · 2025-12-19

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  46. Comparison of the Arrhenius parameters between conventional hydrothermal and microwave-assisted synthesis methods for tin oxide nanoparticles

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  47. Impact of ZnO on CsPbBr3 nanocrystals in fluorophosphate glasses by in situ multi-spectroscopy measurement

    Journal of Non-Crystalline Solids · 2026-03-25

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  48. Antibacterial Activity of Quantum-Confined One-Dimensional Titanate Nanofilaments

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  49. Configurational Entropy Engineering of Bi‑Doped Glass Fiber Enabling Ultrabroadband Emission

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  50. Unveiling the Structure and Properties Evolution of Nd 3+ ‐Doped Phosphate Glass with Substitution of SiO 2 by P 2 O 5

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