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RESEARCH PAPER · Angewandte Chemie International Edition · 2017

Activation and Deactivation of Gold/Ceria–Zirconia in the Low‐Temperature Water–Gas Shift Reaction

James Carter, Xi Liu, Qian He, Sultan M. Althahban, Ewa Nowicka, Simon J. Freakley, Liwei Niu, David John Morgan, Yongwang Li, J. W. Niemantsverdriet, Stanislaw E. Golunski, Christopher J. Kiely, Graham John Hutchings

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Activation and Deactivation of Gold/Ceria–Zirconia in the Low‐Temperature Water–Gas Shift ReactionOriginalMetal Catalysts for Heterogeneous Catalysis: From Single Atoms to Nanoclusters and Nanoparticles4774Dynamic behavior of metal nanoparticles for catalysis157Quantitative Effect of Zr Content on the Structure and Water–Gas Shift Reaction Activities of Gold Supported on Ceria–Zirconia9Ultrastable bimetallic catalyst with tuned surface electronic properties for highly selective oxidation of cyclohexane26Adsorption, Dissociation, and Spillover of Hydrogen over Au/TiO2 Catalysts: The Effects of Cluster Size and Metal–Support Interaction from DFT69Engineering Stable Surface Oxygen Vacancies on ZrO2 by Hydrogen-Etching Technology: An Efficient Support of Gold Catalysts for Water-Gas Shift Reaction72Identification of the Au/ZnO interface as the specific active site for the selective oxidation of the secondary alcohol group in glycerol91Recent Advances in the Gold-Catalysed Low-Temperature Water–Gas Shift Reaction36Average and local structures of κ-phase CeZrO 4 crystals by neutron powder diffraction1Insights into interface engineering in steam reforming reactions for hydrogen production166Visualizing Formation of Intermetallic PdZn in a Palladium/Zinc Oxide Catalyst: Interfacial Fertilization by PdH x95Visualizing Formation of Intermetallic PdZn in a Palladium/Zinc Oxide Catalyst: Interfacial Fertilization by PdH x9A DFT and microkinetic study of HCHO catalytic oxidation mechanism over Pd/Co3O4 catalysts: The effect of metal-oxide interface41How Do Structurally Distinct Au/α‐Fe2O3 Interfaces Determine Surface OH/H2O reactivity, Intermediate Evolution, and Product Formation in Low‐temperature Water‐gas Shift Reaction?6Enhanced Activity and Stability of Gold/Ceria-Titania for the Low-Temperature Water-Gas Shift Reaction21Stable Multimetallic Nanoparticles for Oxygen Electrocatalysis135Construction of stabilized bulk-nano interfaces for highly promoted inverse CeO2/Cu catalyst134Thermally induced sintering and redispersion of Au nanoparticles supported on Ce1-xEuxO2 nanocubes and their influence on catalytic CO oxidation12Construction of Active Site in a Sintered Copper–Ceria Nanorod Catalyst172The Success Story of Gold-Based Catalysts for Gas- and Liquid-Phase Reactions: A Brief Perspective and Beyond7Well-Defined Materials for Heterogeneous Catalysis: From Nanoparticles to Isolated Single-Atom Sites1242Praseodymium hydroxide/gold-supported precursor: a new strategy for preparing stable and active catalyst for the water-gas shift reaction21CO 2 Reduction to Methanol on Au/CeO 2 Catalysts: Mechanistic Insights from Activation/Deactivation and SSITKA Measurements89Evolution of Isolated Atoms and Clusters in Catalysis217Kinetics of Water Gas Shift Reaction on Au/CeZrO4: A Comparison Between Conventional Heating and Dielectric Barrier Discharge (DBD) Plasma Activation14Bifunctional Silicotungstic Acid and Tungstophosphoric Acid Impregnated Cu–Zn–Al & Cu–Zn–Zr Catalysts for Dimethyl Ether Synthesis from Syngas10Supported Metal Clusters: Fabrication and Application in Heterogeneous Catalysis505Confining isolated atoms and clusters in crystalline porous materials for catalysis476Crystallographic Visualization of a Double Water Molecule Addition on a Pt1‐MOF during the Low‐temperature Water‐Gas Shift Reaction8Direct and oxidative dehydrogenation of propane: from catalyst design to industrial application244Fundamental Aspects of Ceria Supported Au Catalysts Probed by In Situ/Operando Spectroscopy and TAP Reactor Studies18Toward an Atomic-Level Understanding of Ceria-Based Catalysts: When Experiment and Theory Go Hand in Hand111Data-driven simulation and characterisation of gold nanoparticle melting71Elucidating the mechanism of the reverse water–gas shift reaction over Au/CeO2 catalysts using operando and transient spectroscopies69Alleviating inhibitory effect of H2 on low-temperature water-gas shift reaction activity of Pt/CeO2 catalyst by forming CeO2 nano-patches on Pt nano-particles32Control-Synthesized Ultrafine AU Nanoparticles by Aspergillus Niger Extracellular Metabolites from Sim Cards as High-Effective 4-Nitrophenol Degradation Catalyst9Kinetic and Thermodynamic Factors Influencing Palladium Nanoparticle Redispersion into Mononuclear Pd(II) Cations in Zeolite Supports25Highly efficient CeO2-supported noble-metal catalysts: From single atoms to nanoclusters173Reversible Growth of Gold Nanoparticles in the Low-Temperature Water–Gas Shift Reaction25Rational design and synthesis of cerium dioxide-based nanocomposites20Size Effects in Gas‐phase C−H Activation5STEM imaging and spectroscopy studies of Au and Au-based catalysts0Spectroscopic investigation of the structural transformation of Ru in the Ru/CeO 2 catalyst18Interfaces and Oxygen Vacancies-Enriched Catalysts Derived from Cu-Mn-Al Hydrotalcite towards High-Efficient Water–Gas Shift Reaction8For more and purer hydrogen-the progress and challenges in water gas shift reaction81Environmental TEM Study of the Dispersion of Au/α-MoC: From Nanoparticles to Two-Dimensional Clusters21Intercalated Borate Anions Modulation of Layered Double Hydroxide by Alkali Treating for Improving Water-Gas Shift Catalytic Performance of Au-Based Catalysts0Active nanointerfaces sites for low-temperature water-gas shift reaction over inverse configuration Nb–CeO2/Cu catalysts7Environmental Catalysis by Gold Nanoparticles1Abundance of Low-Energy Oxygen Vacancy Pairs Dictates the Catalytic Performance of Cerium-Stabilized Zirconia21Alkali treatment modulated borate anions in layered double hydroxides as precursors of highly efficient Au-based catalysts for water-gas shift reaction1Structure and Chemical Reactivity of Y‐Stabilized ZrO2 Surfaces: Importance for the Water‐Gas Shift Reaction13Struktur und chemische Reaktivität von Yttrium‐stabilisierten ZrO2‐Oberflächen: Zur Bedeutung für die Wassergas‐Shift‐Reaktion3Selectively located Pt clusters on Au/CeO2 for highly robust water-gas shift reaction via atomic layer deposition5The evolution of model Rh/Fe3O4(001) catalysts in hydrogen environments4Hydrogen production by the water-gas shift reaction: A comprehensive review on catalysts, kinetics, and reaction mechanism69Understanding the Dynamic Evolution of Active Sites among Single Atoms, Clusters, and Nanoparticles118The Simultaneous Total Oxidation of Toluene, Propene, and CO Environmental Pollutants Using Bimetallic Au‐Pt/ZrO 2 /UVM‐7 Catalysts1Formation of hydrided Pt-Ce-H sites in efficient, selective oxidation catalysts71Atomically dispersed Pt and Pt clusters on CeO2 supports for H2 production via low-temperature water-gas shift reaction6Active Site Evolution during Formic Acid Conversion on Rh-Substituted Fe3O4(001)2NiO (H) locked Au clusters against CO-induced aggregation for robust water-gas shift catalysis7Electronic and magnetic properties of nanomaterials0Enhanced activity and stability of Ni/ceria-titania in hydrogen production from the hydrolysis of ammonia-borane0Gold-Modified Rare Earth Oxides with Tunable Lattice Oxygen Reactivity for N 2 O Synthesis0Silica encapsulation in Cu-exsoluted phyllosilicate toward robust Cu–Si interfaces for the water-gas shift reaction0Alkali Metal-Promoted Au/TS-1 Bifunctional Catalyst for Highly Efficient and Stable Gas-Phase Propylene Epoxidation with H2 and O2 via In Situ-Generated H2O20

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  3. Quantitative Effect of Zr Content on the Structure and Water–Gas Shift Reaction Activities of Gold Supported on Ceria–Zirconia

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  4. Ultrastable bimetallic catalyst with tuned surface electronic properties for highly selective oxidation of cyclohexane

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  5. Adsorption, Dissociation, and Spillover of Hydrogen over Au/TiO2 Catalysts: The Effects of Cluster Size and Metal–Support Interaction from DFT

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  6. Engineering Stable Surface Oxygen Vacancies on ZrO2 by Hydrogen-Etching Technology: An Efficient Support of Gold Catalysts for Water-Gas Shift Reaction

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  7. Identification of the Au/ZnO interface as the specific active site for the selective oxidation of the secondary alcohol group in glycerol

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  8. Recent Advances in the Gold-Catalysed Low-Temperature Water–Gas Shift Reaction

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  9. Average and local structures of κ-phase CeZrO 4 crystals by neutron powder diffraction

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  11. Visualizing Formation of Intermetallic PdZn in a Palladium/Zinc Oxide Catalyst: Interfacial Fertilization by PdH x

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  13. A DFT and microkinetic study of HCHO catalytic oxidation mechanism over Pd/Co3O4 catalysts: The effect of metal-oxide interface

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  14. How Do Structurally Distinct Au/α‐Fe2O3 Interfaces Determine Surface OH/H2O reactivity, Intermediate Evolution, and Product Formation in Low‐temperature Water‐gas Shift Reaction?

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  17. Construction of stabilized bulk-nano interfaces for highly promoted inverse CeO2/Cu catalyst

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  19. Construction of Active Site in a Sintered Copper–Ceria Nanorod Catalyst

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